CAS: 613-37-6; 4-Methoxybiphenyl

该化合物是一种有机化合物,其特征为联苯结构,其联苯结构与一个苯环的某一个基体相连,其分子式为CHO分子,分子重量约为198.25克/摩尔.该化合物一般无色,可视温度和纯度而定,为黄色液体或固态;已知其芳香特性,并用于各种用途,包括作为有机合成的中间体以及染料和药品的生产. 4-MethoxyBy联苯在乙醇和醚等有机溶剂中表现出中等溶性,但水溶性较低,其化学行为受可参与电药用芳香替代反应的甲氧组的存在影响.安全数据表明,应谨慎处理该化合物,因为它在接触时可能构成健康风险.建议采取适当的安全措施,包括使用个人防护设备.

结构式图片

物理性质

MSDS等安全信息

上下游产品

diazomethane 4-Phenylphenol iodobenzene para-iodoanisole 4-(4'-methoxy-biphenyl-4-yl)-4-oxo-butyric acid 4-(4-methoxy-biphenyl-3-yl)-4-oxo-butyric acid 4-methoxy-4'-nitrobiphenyl 3-nitro-4-methoxybiphenyl

合成工艺路线路线简述

  • 合成目标产物 4-Methoxybiphenyl 主要起始原料 4-Methoxyphenylboronic Acid And Aniline
  • 98-80-6 = 613-37-6
    反应条件:1.1 Reagents: Potassium Carbonate Catalysts: (3-Aminopropyl)Triethoxysilane (Bound To Graphene Oxide And Silica),Palladium,Silica (Bound To Graphene Oxide Via Aptes),Graphene (Oxide,Grafted With Aptes) Solvents: Ethanol; 2 H,80 °C
    标题:Self-Assembly Strategies For Graphene Oxide/silica Nanostructures: Synthesis And Structural Analysis
    作者:Takeuchi,Yuki; Ohkura,Kentaro; Nishina,Yuta
    参考文献:Bulletin Of The Chemical Society Of Japan 日期:2023 卷标:96(2) 页码:113-119]

    98-80-6 + 586-76-5 = 613-37-6 + 92-92-2 + 586-76-5
    反应条件:1.1 Reagents: Potassium Carbonate Catalysts: Palladium Solvents: Dimethylformamide,Water; Rt1.2 Reagents: Potassium Hydroxide Solvents: Ethanol,Water; 12 H,Rt
    标题:Efficient Catalytic Activation Of Suzuki-Miyaura C-C Coupling Reactions With Recyclable Palladium Nanoparticles Tailored With Sterically Demanding Di-N-Alkyl Sulfides
    作者:Kumar,Satyendra; Rao,G. K.; Kumar,Arun; Singh,Mahabir P.; Saleem,Fariha; Et Al
    参考文献:Rsc Advances 日期:2015 卷标:5(26) 页码:20081-20089
对羟基联苯置于sodium Hydroxide,硫酸二甲酯体系中,化学反应生成 4-甲氧基联苯
参考文献:Mesomorphic Compound Having Alkyl Beta-Hydroxycarboxylate As Chiral Group And Liquid Crystal Composition Containing Same
标题:Mesomorphic Compound Having Alkyl Beta-Hydroxycarboxylate As Chiral Group And Liquid Crystal Composition Containing Same

海关参考信息

专利信息


专利号:US-9315483-B2
优先权日:2007-09-13
标题 :Synthesis of deuterated catechols and benzo[D][1,3]dioxoles and derivatives thereof
发明人：JONES ANDREW D; ZELLE ROBERT E; SILVERMAN I ROBERT
权利人:CONCERT PHARMACEUTICALS INC
摘要:The present invention provides a convenient and efficient process for the synthesis of d 2 -benzo[d][1,3]dioxoles.

专利号:US-7250510-B2
优先权日:2005-08-24
标 题:Transition metal complexes of N-heterocyclic carbenes, method of preparation and use in transition metal catalyzed organic transformations
发明人：ORGAN MICHAEL G; O'BRIEN CHRISTOPHER J; KANTCHEV ASSAM ERIC B
权利人:TOTAL SYNTHESIS LTD
摘要:The present invention relates to catalysts of transition metal complexes of N-heterocyclic carbenes, their methods of preparation and their use in chemical synthesis. The synthesis, ease-of-use, and activity of the compounds of the present invention are substantial improvements over in situ catalyst generation. Further, the transition metal complexes of N-heterocyclic carbenes of the present invention may be used as precatalysts in metal-catalyzed cross-coupling reactions.

专利号:US-9428524-B2
优先权日:2010-05-25
标 题:Synthetic process for the manufacture of ecteinascidin compounds
发明人：MARTIN LÓPEZ MA JESÚS; FRANCESCH SOLLOSO ANDRÉS; CUEVAS MARCHANTE MARIA DEL CARMEN
权利人:MARTIN LÓPEZ MA JESÚS; FRANCESCH SOLLOSO ANDRÉS; CUEVAS MARCHANTE MARIA DEL CARMEN; PHARMA MAR SA
摘要:This invention relates to compounds of formula II: wherein R 1 , R 2 , Prot SH , and Prot NH are as defined, to processes for the synthesis of ecteinascidins of formula I from compounds of formula II, and to processes for the synthesis of compounds of formula II.

专利号:US-6891059-B2
优先权日:2000-01-27
标题:Asymmetric synthesis of pregabalin
发明人：BURK MARK JOSEPH; GOEL OM PRAKASH; HOEKSTRA MARVIN SIMON; MICH THOMAS FREDERICK; MULHERN THOMAS; RAMSDEN JAMES A
权利人:WARNER LAMBERT CO
摘要:This invention provides a method of making (S)-(+)-3-(aminomethyl)-5-methylhexanoic acid (pregabalin) or a salt thereof via an asymmetric hydrogenation synthesis. Pregabalin is useful for the treatment and prevention of seizure disorders, pain, and psychotic disorders. The invention also provides intermediates useful in the production of pregabalin.

专利号:US-8212056-B2
优先权日:2008-06-30
标 题 :Ligands for transition-metals and methods of use
发明人：KWONG FUK YEE; SO CHAU MING
权利人:KWONG FUK YEE; SO CHAU MING; UNIV HONG KONG POLYTECHNIC
摘要:The present invention relates to indolyl phosphine ligands, and methods of making such ligands utilizing phenyl hydrazines and aryl ketones as the starting material. The present invention further includes uses of the ligands in the synthesis of pharmaceuticals, materials, and agriculture.

专利号:US-5098602-A
优先权日:1988-05-11
标题 :Novel halogen-containing ester compounds, and their intermediates, and method of producing the same as well as liquid crystal compositions containing the same and light switching elements
发明人：HIRAI TOSHIHIRO; YOSHIZAWA ATSUSHI; NISHIYAMA ISA; FUKUMASA MITSUO; SHIRATORI NOBUYUKI; YOKOYAMA AKIHISA
权利人:NIPPON MINING CO
摘要:This invention provides a novel halogen-containing ester compound represented by the following general formula (I): ##STR1## (wherein R is an alkyl group, A is selected from a single bond, --O--, --COO-- and --CO--, both of X and Y are halogen atoms or either one of X and Y is a halogen atom and the other is a hydrogen atom, each of m and n is 0 or 1, m+n=0 or 1, each of k and l is an integer of 1 or more, provide k

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主要参考文献


1: Lau PL, Allen RW, Styring P. Continuous-flow Heck synthesis of 4-methoxybiphenyl and methyl 4-methoxycinnamate in supercritical carbon dioxide expanded solvent solutions. Beilstein J Org Chem. 2013 Dec 17;9:2886-97. doi: 10.3762/bjoc.9.325. eCollection 2013.
2: Tsutsumi T, Amakura Y, Okuyama A, Tanioka Y, Sakata K, Sasaki K, Maitani T. Application of an ELISA for PCB 118 to the screening of dioxin-like PCBs in retail fish. Chemosphere. 2006 Oct;65(3):467-73. Epub 2006 Mar 10.
4: Lehmler HJ, Parkin S, Robertson LW. The three-dimensional structure of 3, 3', 5'-trichloro-4-methoxybiphenyl, a "coplanar" polychlorinated biphenyl (PCB) derivative. Chemosphere. 2002 Jan;46(3):485-8.

合成参考文献


摘要:Black, D. A.; Fagnou, K., Science of Synthesis, (2010) 45, 591.
摘要:Black, D. A.; Fagnou, K., Science of Synthesis, (2010) 45, 602.
摘要:Black, D. A.; Fagnou, K., Science of Synthesis, (2010) 45, 550.
摘要:Black, D. A.; Fagnou, K., Science of Synthesis, (2010) 45, 562.
摘要:Black, D. A.; Fagnou, K., Science of Synthesis, (2010) 45, 567.
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