专利号:US-2024116890-A1 优先权日:2022-09-28 标 题 :Large scale synthesis of cannabinol 发明人:COLLINS ARIANNA C; CRUCES IVAN; RAY KYLE; CRUCES WESTLEY 权利人:COLORADO CHROMATOGRAPY LLC 摘要:Methods for producing cannabinol, cannabivarin, or derivatives thereof are disclosed. The methods disclosed herein can be employed for large scale synthesis or semi-synthesis of the compounds, including multi-kilogram quantities of the compounds.
专利号:US-2023002312-A1 优先权日:2019-11-20 标题:A continuous flow process for the synthesis of hydroxamic acid 发明人:PIMPALE MILIND JAGANNATH; KINI PRASHANT VASANT 权利人:UPL LTD 摘要:The present invention relates to a process for the synthesis of hydroxamic acids by continuous flow process wherein said process comprising reacting alkyl ester with hydroxyl amine salt in presence of base in a microreactor system and continuously producing hydroxamic acid.
专利号:US-8785656-B2 优先权日:2012-02-16 标 题:Telescoping synthesis of 5-amino-4-nitroso-1-alkyl-1H-pyrazole salt 发明人:GEIBEL WOLFRAM; WEBER INGO; OSAN ARMIN; SPECKBACHER MARKUS 权利人:PROCTER & GAMBLE 摘要:A telescoping synthesis of 5-amino-4-nitroso-1-alkyl-1H-pyrazole salt derivatives of formula (I), the compound (I) itself, and its use as an intermediate in the fabrication of 1-alkyl-4,5-diaminopyrazole salts of general formula (IX). The compounds of formula (IX) can be used as precursor dyes in oxidative hair dye compositions. n n n n n n n n n n R is a mono- or poly-substituted or unsubstituted, straight or branched, saturated or mono- or poly-unsaturated, alkyl group. HZ and HZ′ are organic or mineral acids.
专利号:US-11554348-B2 优先权日:2016-11-10 标 题 :Method of preparing hierarchical porous channel molecular sieve membrane and application thereof 发明人:GU XUEHONG; YAO XUN; PENG LI 权利人:NANJING UNIVERSITY OF TECHNOLOGY 摘要:The invention relates to a method for preparing a hierarchical porous zeolite membrane and an application thereof, comprising the following steps: a mesoporous structure-directing agent is added to limit the growth of zeolite crystals, and self-assembled in the crystallization process to generate a mesoporous structure. Based on a seed crystal induced secondary nucleation mechanism, this method can realize one-step hydrothermal synthesis of hierarchical porous zeolite membrane with the advantages of mild and controllable synthesis conditions, simple process, good repeatability, reduced energy consumption and cost savings. The hierarchical porous zeolite membrane prepared by the method has good cut-off performance, and the cut-off molecular weight is adjustable between 200 to 500,000 Da.
专利号:US-9359318-B2 优先权日:2010-08-06 标 题:Process for the synthesis of 2,5-furandicarboxylic acid 发明人:BORSOTTI GIAMPIETRO; DIGIOIA FRANCESCA 权利人:BORSOTTI GIAMPIETRO; DIGIOIA FRANCESCA; NOVAMONT SPA 摘要:Process for the synthesis of 2,5-furandicarboxylic acid through the oxidation of -hydroxymethylfurfural in a flow of oxygenor a compound containing oxygen, catalyzed by a supported catalyst containing a metal of the platinum group, carried out in aqueous solution in which the pH is maintained higher than 7 and lower than 12 through the addition of a weak base.
专利号:US-2025214851-A1 优先权日:2023-12-28 标 题 :SYNTHESIS OF POROUS CRYSTALLINE MATERIALS IN THE PRESENCE OF FLUORIDE MINERALIZER AND pH-MODIFIED WATER-SOLUBLE OXIDIZED DISULFIDE OIL 发明人:HODGKINS ROBERT PETER; KOSEOGLU OMER REFA 权利人:SAUDI ARABIAN OIL CO 摘要:Methods are provided for hydrothermal synthesis of porous crystalline materials. The method generally comprises forming a solution of precursors and reagents in effective ratios for a porous crystalline material including a fluoride-containing mineralizer, and a pH-modified water-soluble oxidized disulfide oil composition. The solution is hydrothermally treated under effective conditions and for an effective time to synthesize porous crystalline materials.
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