CAS: 6920-22-5; Hexane-1,2-Diol

上下游产品

1,2-Epoxyhexane 4-butyl-2,2-dimethyl-[1,3]dioxolane 1-hexene rac-2-hydroxyhexanoic acid 20H20N6O12C20H20N6O12 -OtBuZ-Glu(2S,2R)-2-hydroxyhexyl-OtBu (R)-3-benzyloxy-1,2-propanediol

1-己烯置于ruthenium Trichloride Sodium Periodate体系中,用 乙酸乙酯,乙腈 作为反应溶剂,化学反应 0.05H,以100%的收率获得产物dl-1,2-己二醇
参考文献:Enhancing Selectivity In Oxidation Catalysis With Sol-gel Nanocomposites
标题:Enhancing Selectivity In Oxidation Catalysis With Sol-gel Nanocomposites
摘要:使用掺入有机催化剂 Tempo 的溶胶疏水纳米结构二氧化硅基质,可以轻松合成δ-羟基酸等有价值的有机化合物,并提高了相关的选择性:这是一种基于材料科学的合成路线,无法通过经典的均相合成实现.
DOI:10.1039/b505949F

专利信息

专利号:US-2018297857-A1
优先权日:2015-06-02
标 题:Aqueous Synthesis of Polyhedral 'Brick-Like' Iron Oxide Nanoparticles for Hyperthermia and T2 MRI Contrast Enhancement, and for Targeting Endothelial Cells for Therapeutic Delivery
发明人：HEGMANN TORSTEN; WORDEN MATTHEW; MILLER DONALD W
权利人:UNIV KENT STATE OHIO
摘要:A low temperature, aqueous synthesis of polyhedral iron oxide nanoparticles (IONPs) is presented. The modification of the co-precipitation hydrolysis method with Triton X surfactants results in the formation of crystalline polyhedral particles. The particles are herein termed iron oxide “nanobricksâ€? (IONBs), as the varieties of particles made are all variations on a simple “brick-likeâ€?, polyhedral shape such as rhombohedral shape or parallelogram as evaluated by TEM. These IONBs can be easily coated with hydrophilic silane ligands, allowing them to be dispersed in aqueous media. The dispersed particles are investigated for potential applications as hyperthermia and T 2 MRI contrast agents. The results demonstrate that the IONBs perform better than comparable spherical IONPs in both applications, and show r 2 values amongst the highest for iron oxide based materials reported in the literature.

专利号:US-2025214849-A1
优先权日:2023-12-28
标 题:Synthesis of porous crystalline materials in the presence of water-soluble oxidized disulfide oil and fluoride mineralizer
发明人：HODGKINS ROBERT PETER; KOSEOGLU OMER REFA
权利人:SAUDI ARABIAN OIL CO
摘要:Methods are provided for hydrothermal synthesis of porous crystalline materials. The method generally comprises forming a solution of precursors and reagents in effective ratios for a porous crystalline material including a fluoride-containing mineralizer, and water-soluble oxidized disulfide oil. The solution is hydrothermally treated under effective conditions and for an effective time to synthesize porous crystalline materials.

专利号:US-2025214851-A1
优先权日:2023-12-28
标 题 :SYNTHESIS OF POROUS CRYSTALLINE MATERIALS IN THE PRESENCE OF FLUORIDE MINERALIZER AND pH-MODIFIED WATER-SOLUBLE OXIDIZED DISULFIDE OIL
发明人：HODGKINS ROBERT PETER; KOSEOGLU OMER REFA
权利人:SAUDI ARABIAN OIL CO
摘要:Methods are provided for hydrothermal synthesis of porous crystalline materials. The method generally comprises forming a solution of precursors and reagents in effective ratios for a porous crystalline material including a fluoride-containing mineralizer, and a pH-modified water-soluble oxidized disulfide oil composition. The solution is hydrothermally treated under effective conditions and for an effective time to synthesize porous crystalline materials.

专利号:US-6939962-B2
优先权日:2000-07-31
标题:Method for the synthesis of sucrose-6-esters
发明人：CLARK JASON D; LEMAY JR RICHARD R
权利人:TATE & LYLE PLC
摘要:There is described a process for the synthesis of a sucrose-6-ester comprising: (a) reacting a mixture comprising sucrose and a polar aprotic solvent with an organotin-based acylation promoter, while adding a solvent capable of removing water by co-distillation, and removing water by co-distillation, to afford a first reaction mixture which is substantially free from water, followed by (b) adding a carboxylic anhydride to said first reaction mixture to afford a second reaction mixture, and maintaining said second reaction mixture at a temperature and for a period of time sufficient to produce a sucrose-6-ester, characterised in that step (a) is performed at a temperature of from 85 to 125° C. and at a pressure of from 20 to 80 kPa. In the most preferred embodiment, the polar aprotic solvent is DMF, the solvent capable of removing water by co-distillation is cyclohexane, the organotion-based acylation promoter is a 1,3-diacyloxy-1,1,3,3-tetrabutyldistannoxane, and step (a) is performed at approximately 97° C., and approximately 50 kpa, until the weight ratio of tin to water in the first reaction mixture is greater than about 26, when the tin content is measured by X-Ray Fluoresence Analyzer, and the water content is measured by the Karl-Fischer method.

专利号:US-11958751-B2
优先权日:2022-06-27
标 题:Method of synthesizing materials integrating supernatant recycle
发明人：HODGKINS ROBERT P; KOSEOGLU OMER REFA
权利人:SAUDI ARABIAN OIL CO
摘要:Methods are disclosed for synthesizing materials, including an initial synthesis in the presence of WS-ODSO (which can include a pH-modified WS-ODSO composition, in certain embodiments a neutralized WS-ODSO composition), and one or more subsequent syntheses using supernatant (“mother liquorâ€?) from a previous synthesis of the same or different materials. The synthesized materials in the initial synthesis and in subsequent synthesis can be the same or different inorganic oxide materials including amorphous oxides, crystalline oxides or oxides of metals. The methods advantageously reduce the amount of utility water required for synthesizing a material and reduce the water waste, and reduce the DSO waste from a refinery and discharge into the environment. In certain embodiments the methods reduce the requirements to procure an alkaline reagent required for synthesizing materials. In certain embodiments, supernatant can be recycled over multiple synthesis batches of the same or different type of materia.

专利号:EP-1721601-A1
优先权日:2005-05-11
标 题 :Use of taurine for enhancing lipid synthesis in the epidermis
发明人：DOERING THOMAS; WALDMANN-LAUE MARIANNE; WADLE ARMIN; ANDERHEGGEN BERND
权利人:HENKEL KGAA
摘要:The present invention is the use of taurine for stimulating the epidermal synthesis of barrier lipids.