专利号:WO-2015120485-A1 优先权日:2014-02-10 标 题:Water, bubble collapse and syngas species in the synthesis of graphene and its derivatives 发明人:SHANKMAN RICHARD S 权利人:PEERLESS WORLDWIDE LLC 摘要:Hydrodynamic cavitation-inducing inertial, non-inertial, and combination reactors are employed in the hydrothermal synthesis of graphene and its derivatives, both in solution and vapor. Various hydrodynamic cavitation reactor embodiments are revealed. Water is used to both nucleate and 'self-heal' graphene sheet growth in solution and vapor. Various methods of combustion, hydrothermal and dehydration synthesis of graphene and its derivatives are revealed. Additionally, water and ice are used as a substrate, both alone and in combination with other substrates, to grow and recover useful graphene and its derivatives.
专利号:US-4592867-A 优先权日:1984-10-19 标题:Synthesis method for reductant precursor 发明人:YU TERRY T; YEN MEI-RONG 权利人:ENERGY CONVERSION DEVICES INC 摘要:A synthesis method is provided for the synthesis of quinone compounds of the formula ##STR1## where n is 0-3, Y 1 is alkoxy, Y 2 is alkoxy, chloro, bromo or hydrogen and R' and R' each and independently are hydrogen, alkyl or phenyl. These compounds are useful as reductant precursors in tellurium imaging compositions.
专利号:US-9428524-B2 优先权日:2010-05-25 标 题:Synthetic process for the manufacture of ecteinascidin compounds 发明人:MARTIN LÓPEZ MA JESÚS; FRANCESCH SOLLOSO ANDRÉS; CUEVAS MARCHANTE MARIA DEL CARMEN 权利人:MARTIN LÓPEZ MA JESÚS; FRANCESCH SOLLOSO ANDRÉS; CUEVAS MARCHANTE MARIA DEL CARMEN; PHARMA MAR SA 摘要:This invention relates to compounds of formula II: wherein R 1 , R 2 , Prot SH , and Prot NH are as defined, to processes for the synthesis of ecteinascidins of formula I from compounds of formula II, and to processes for the synthesis of compounds of formula II.
专利号:US-5721371-A 优先权日:1995-12-18 标题 :Synthesis of substituted pterocarpans 发明人:LAROCK RICHARD C 权利人:UNIV IOWA STATE RES FOUND INC 摘要:The present invention provides a method of synthesizing compounds of formula (I): ##STR1## wherein R 1 and R 3 are independently H or (C 1 -C 4 )alkyl--O--; n R 2 is R 5 C(O)-- where R 5 is (C 1 -C 4 )alkyl or H; and n R 4 is H, (C 1 -C 4 )alkyl or (C 5 -C 7 )aryl optionally substituted with (C 1 -C 4 )alkyl or halo.
专利号:US-10487052-B2 优先权日:2016-12-28 标 题 :Synthesis method of N-substituted maleimide using solid acid catalysts 发明人:CHEON JOO YOUNG; CHOI JUN SEON; KIM JI YEON; JOE WANG RAE; KIM KYUNG SOO; YEOM EUNG SEOB; LEE WON KYUN 权利人:LG CHEMICAL LTD 摘要:The present invention relates to a synthesis method of N-substituted maleimides using a non-homogeneous solid acid catalyst, and particularly, a synthesis method of N-substituted maleimides with high synthesis yield by using a zirconium(IV) hydrogen phosphate as a catalyst, by which, the loss of the catalyst is minimized, the separation and recovering processes of the catalyst are simplified, in case when the activity of the separated and recovered catalyst is decreased, the complete regeneration of the catalyst is possible via washing or firing, and solvents that could be used during a washing process of the catalyst are not limited.
专利号:US-9023308-B2 优先权日:2011-03-15 标题:Facile synthesis of graphene, graphene derivatives and abrasive nanoparticles and their various uses, including as tribologically-beneficial lubricant additives
参考标题:Organophotocatalytic Aerobic Oxygenation Of Phenols In A Visible‐light Continuous‐flow Photoreactor 作者:Joël Wellauer,Dragan Miladinov,Thomas Buchholz,Jan Schütz,René T. Stemmler,Jonathan A. Medlock,Werner Bonrath,Christof Sparr |发布日期:2021.7.7 摘要:A Mild Photocatalytic Phenol Oxygenation Enabled By A Continuous-Flow Photoreactor Using Visible Light And Pressurized Air Is Described Herein. Products For Wide-Ranging Applications, Including The Synthesis Of Vitamins, Were Obtained In High Yields By Precisely Controlling Principal Process Parameters. The Reactor Design Permits Low Organophotocatalyst Loadings To Generate Singlet Oxygen. It Is Anticipated
合成参考文献
参考文献:10.1002/pmic.201100208 摘要:Qiao L, Su F, Bi H, Girault HH, Liu B. Ga2O3 photocatalyzed on‐line tagging of cysteine to facilitate peptide mass fingerprinting. Proteomics. 2011 Jul 21;11(17):3501–9. doi: 10.1002/pmic.201100208.