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CAS号50651-39-3 N-(4-甲氧基-3-硝苯基)乙酰胺 | CAS号51868-45-2 3-(N,N-二烯丙基)氨基-... | CAS号19433-93-3 3-(N,N-二乙基)氨基-4...2,4-二硝基酚置于palladium On Activated Charcoal,Methyl Tributylmethylammonium Carbonate,Sodium Carbonate,Sodium Hydroxide体系中,用 甲醇,二氯甲烷 作为反应溶剂,1.0~65.0 °C,850.02 Kpa 条件下,反应 15.58H,反应生成 3-氨基-4-甲氧基乙酰苯胺
参考文献:分散染料中间体的合成方法
标题:分散染料中间体的合成方法
摘要:本发明公开了一种分散染料中间体的合成方法,包括将2,4‑二硝基苯酚和氢气发生还原反应制备2,4‑二氨基苯酚的步骤;将2,4‑二氨基苯酚与碘甲烷在催化剂甲基三丁基甲基碳酸铵作用下发生醚化反应制备2,4‑二氨基苯甲醚的步骤;将2,4‑二氨基苯甲醚与醋酐发生酰化反应制备目标产物3‑氨基‑4‑甲氧基乙酰苯胺的步骤.相比2,4‑二硝基苯甲醚加氢还原法,采用本发明的2,4‑二硝基苯酚加氢还原法,其转化率高,副反应少.
海关参考信息
- 2905110000-甲醇
2912110000-甲醛
2912120000-乙醛
2924292000-扑热息痛 - 💡 提示:海关信息按照顺序优先匹配,如需确认的海关信息,请参考相关资料。
- 详情请参考:📖 海关编码查询和海关进出口税则
专利信息
专利号:US-5107022-A
优先权日:1989-08-28
标 题 :Process for the preparation of aromatic amines
发明人:DE BESSET AMAURY P
权利人:CIBA GEIGY CORP
摘要:The invention relates to a process for the preparation of compounds of formula (1) wherein R is unsubstituted or substituted C1-C4alkyl or unsubstituted or substituted phenyl, X is hydrogen or unsubstituted or substituted C1-C4alkyl, and Y is unsubstituted or substituted C1-C4alkyl, which process comprises subjecting compounds of formula (2) wherein R, X and Y are as defined for formula I, to catalytic hydrogenation in the alkaline pH range. The compounds obtained by the process of this invention are suitable intermediates for the synthesis of dyes.
专利号:US-4719053-A
优先权日:1980-08-01
标题 :Beta-chloroethylsulfonylmethyl-benzoic halides as intermediates
发明人:SCHLAEFER LUDWIG; HAEHNLE REINHARD
权利人:HOECHST AG
摘要:New beta -chloroethylsuflonylmethyl-benzoic acid halides which can serve as fibre-reactive anchors for thesynthesis of novel organic, water-soluble compounds, preferably dyestuffs, having fibre-reactive and fibre-finishing properties, such as preferably dyestuff properties, and containing, as a fibre-reactive group, one or two beta -chloroethylsufonylmethylbenzoic acid amide groups. For the synthesis of these novel fibre-finishing compounds, said new beta -chloroethylsulfonylmethyl-benzoic acid halide compounds are reacted with an organic, water-soluble compound having fibre-finishing properties and continuing one or two amino groups. Also precursors of the fibre-finishing, fibre-reactive compounds, containing said beta -chloroethylsulfonylmethyl-benzxoic acid amid grouping, can be employed for their synthesis. The novel fibre-finishing compounds can be applied onto suitable fibre materials, such as especially cellulose fibre material and natural or synthetic polyamide fibre materials, and fixed on these fibre materials in a manner similar to application and fixation methods usual in the technique for fibre-reactive compounds. The fibre-finished material, such as dyed material, shows very good wet fastnesses.
专利号:WO-2024074814-A9
优先权日:2022-10-04
标题 :Composition comprising a functionalised dye and a diallylamine comonomer and use thereof
发明人:CANNON PAUL; DONLEY ADAM; LAWRENCE ANTHONY; WRIGHT GAVIN; TURNER CARL; ROBERTS PHILIP
权利人:SUBLINO LTD; COLOUR SYNTHESIS SOLUTIONS LTD
摘要:The present teachings relate to a composition comprising a functionalised dye and a diallylamine comonomer, and the use of such compositions in methods of colouring a substrate. The present teachings provide improved bonding of a dye to a substrate, and preferably allow colouring to be conducted entirely in the presence of an aqueous solvent.
专利号:CN-115160177-A
优先权日:2021-04-01
标题:A new method for the synthesis of 2-amino-4-acetamidoanisole
专利号:CN-112094405-B
优先权日:2020-09-23
标题 :A kind of synthesis and application method of modified PEG sphere
专利号:CN-114436876-B
优先权日:2020-10-30
标 题:A kind of continuous synthesis method of 2-amino-4-acetamidoanisole