CAS: 433-19-2; 1,4-Bis(Trifluoromethyl)Benzene

上下游产品

CAS号68-36-0 α,α,α,α',α',α'-... | CAS号128796-39-4 4-(三氟甲基)苯硼酸 | CAS号2926-29-6 三氟代甲烷亚磺酸钠 | CAS号160911-78-4 ethyl 4-(triflu... | CAS号637-87-6 对氯碘苯 | CAS号100-21-0 对苯二甲酸(PTA) | CAS号624-38-4 1,4-二碘苯 | CAS号120-61-6 对苯二甲酸二甲酯 | CAS号328-91-6 2-氯-1,4-双(三氟甲基)苯 | CAS号361-01-3 1,2,4,5-tetrach... | CAS号320-55-8 1,4-二氯-2,5-双三氟甲基苯 | CAS号328-93-8 2,5-二(三氟甲基)苯胺 | CAS号320-88-7 1-硝基-2,5-双(三氟甲基)苯 | CAS号42580-42-7 2,5-双(三氟甲基)苯甲酸 | CAS号75-46-7 三氟甲烷 | CAS号124-38-9 二氧化碳 | CAS号3345-29-7 1,1,2,2,9,9,10,...

在 1-氟-2,4,6-三甲基吡啶三氟甲烷磺酸盐体系中,用 硝基苯-D5 作为反应溶剂,化学反应 3.0H,以61%的收率获得产物对二三氟甲苯
参考文献:Ball,Nicholas D.; Kampf,Jeff W.; Sanford,Melanie S.,Journal Of The American Chemical Society,2010,Vol. 132,P. 2878-2879
标题:Ball,Nicholas D.; Kampf,Jeff W.; Sanford,Melanie S.,Journal Of The American Chemical Society,2010,Vol. 132,P. 2878-2879

专利信息

专利号:US-8841473-B2
优先权日:2009-09-01
标题 :Synthesis of fluorosilicones and their derivatives
发明人：MARCINIEC BOGDAN; MACIEJEWSKI HIERONIM; DABEK IZABELA; KARASIEWICZ JOANNA
权利人:MARCINIEC BOGDAN; MACIEJEWSKI HIERONIM; DABEK IZABELA; KARASIEWICZ JOANNA; UNIV ADAM MICKIEWICZ
摘要:The subject of invention is the method of synthesis of fluorosilicone co-polymers of arbitrary topology and general formula 1 in which among others if A stands for CH—O(CH 2 ) m (CF 2 ) n CF 2 H group, then the method is based on hydrosilylation reaction of appropriate fluoroalkyl-allyl ether with polyhydrosiloxanes containing at least one Si—H group, catalyzed by siloxide rhodium complex. If A stands for in which Z stands for divalent group either then the method is based on the reaction of nucleophilic opening of oxirane ring in appropriate epoxyfunctional co-polysiloxanes, in acidic environment.

专利号:US-2013184465-A1
优先权日:2010-09-30
标 题:Process for the synthesis of thio-triazolo-group containing compounds
发明人：DOCHNAHL MAXIMILIAN; KEIL MICHAEL; GEBHARDT JOACHIM; VOGELBACHER UWE JOSEF; RACK MICHAEL
权利人:DOCHNAHL MAXIMILIAN; KEIL MICHAEL; GEBHARDT JOACHIM; VOGELBACHER UWE JOSEF; RACK MICHAEL; BASF SE
摘要:The present invention relates to a process using specific magnesium reagents for providing thio-triazolo group-containing compounds and for the synthesis of precursors therefor. The invention furthermore relates to intermediates and to their preparation.

专利号:US-12378221-B2
优先权日:2022-07-05
标 题:Salts of obicetrapib and processes for their manufacture and intermediates thereof
发明人：CUI SHENG; RÖTHELI ANDREAS RENÉ; BORTHS CHRISTOPHER J; KISHIDA MUNEKI; SMOLENSKAYA VALERIYA NIKOLAYEVNA
权利人:NEWAMSTERDAM PHARMA B V
摘要:Provided herein is a method for the manufacture of a compound of obicetrapib and salts thereof, such as calcium salts thereof. Also provided herein is amorphous obicetrapib hemicalcium. New intermediates for use in the synthesis of obicetrapib, and salts thereof are also provided, including obicetrapib HCl and a mesylate salt for the use in the synthesis of obicetrapib and amorphous obicetrapib hemicalcium.

专利号:US-6150499-A
优先权日:1998-01-06
标 题:Process for preparation of TFPX-dichloride
发明人：DOLBIER JR WILLIAM R; DUAN JIANXIN
权利人:SPECIALTY COATING SYSTEMS INC
摘要:A method for the synthesis of TFPX-dichloride is disclosed. The method involves reacting hexachloro-p-xylene with anhydrous HF in an inert organic solvent. The reaction is advantageous in that it produces relatively high yields of TFPX-dichloride, provides little waste, and is carried out as a simple, one-step process.

专利号:WO-2024019698-A1
优先权日:2022-07-18
标题 :Photocatalytic synthesis of alpha, beta unsaturated carbonyl compounds and their intermediates
发明人：SUGURI TAKUYA; MARUYAMA YOUICHIROU; LIM CHERN-HOOI; QIAN GANG; LIU YUE; COPE ELANA
权利人:JSR CORP; NEW IRIDIUM INC
摘要:Described herein is a process of producing α,β unsaturated acids and amides and their intermediates via a photocatalytic reaction in the presence of a photocatalyst, oxygen, and optionally a solvent. The photocatalyst contains a tungstic acid or a salt of a tungstic acid. The process is simple, clean, and energy efficient, and provides good conversion, good selectivity, good turnover, and easy purification of end products.

专利号:US-5422416-A
优先权日:1993-06-30
标题 :Process for the synthesis of polybenzazole polymers
发明人：SO YING H
权利人:DOW CHEMICAL CO
摘要:Described herein is a process for synthesizing polybenzazole polymers comprising: (a) contacting a bis(trihalomethyl) organic compound with a polyphosphoric acid under reaction conditions sufficient to convert at least about 25 mole percent of the trihalomethyl groups present to carboxylic acid or carboxylate groups, forming a reaction mixture thereby; and (b) contacting the reaction mixture with an aromatic compound having two o-amino-basic moieties under reaction conditions sufficient to form a polybenzazole polymer.