CAS: 879-18-5; 1-Naphthoyl Chloride

该化合物是一种多用途有机化合物,主要用作合成化学中的乙酰剂;其氯化萘脊椎和活性乙酰氯组对将1-纳phhoymity引入目标分子,促进染料,药品和特殊化学品的合成十分有用;该化合物表现出与核素高度反应性,能够有效地进行恐吓和受精反应;由于湿度敏感,通常在缺水条件下处理;关键优势包括其在生产具有强化芳香特性的中间体方面的作用及其在建设复杂分子结构方面的效用;适当的储存和处理对于维持稳定和防止水解至关重要.

结构式图片

相似化合物

2243-83-6 2351-36-2 66-77-3

物理性质

MSDS等安全信息

欧盟法规

ECHA物质C&L通报REACH预注册

上下游产品

CAS号86-55-5 1-萘甲酸 | CAS号201230-82-2 carbon monoxide | CAS号90-14-2 α-碘萘 | CAS号79-37-8 草酰氯 | CAS号68-12-2 N,N-二甲基甲酰胺 | CAS号3416-93-1 2-(4,5-dihydro-... | CAS号91-20-3 萘 | CAS号56-23-5 四氯化碳 | CAS号7705-08-0 三氯化铁 | CAS号110-86-1 吡啶 | CAS号43038-45-5 1-萘甲酰肼 | CAS号14271-86-4 1-萘甲酰氰 | CAS号30388-20-6 六甲基氯胍 | CAS号4780-79-4 1-萘甲醇 | CAS号941-98-0 1-萘乙酮 | CAS号90-14-2 α-碘萘 | CAS号10408-64-7 1,2-diphenyl-3H... | CAS号479-33-4 四苯基环戊二烯酮 | CAS号66-77-3 1-萘甲醛

合成工艺路线路线简述

  • 合成目标产物 1-Naphthoyl Chloride 主要起始原料 1-Naphthoic Acid
  • 86-55-5 = 879-18-5
    反应条件:1.1 Reagents: Oxalyl Chloride Catalysts: Dimethylformamide Solvents: Dichloromethane; Rt -> 0 °C; 0 °C; 5 H,Rt
    标题:Direct Construction Of Fused/bridged 3D Rings Via Visible-Light Induced Dearomative Cycloaddition Of Arenes
    作者:Zhen,Guangjin; Et Al
    参考文献:Advanced Synthesis & Catalysis 日期:2023 卷标:365(1) 页码:43-52]

    86-55-5 = 879-18-5
    反应条件:1.1 Catalysts: Dimethylformamide Solvents: Dichloromethane; 5 Min,0 °C1.2 Reagents: Oxalyl Chloride; 0 °C; 12 H,Rt
    标题:Chiral Bronsted Acid-Catalyzed Dynamic Kinetic Resolution Of Atropisomeric Ortho-Formyl Naphthamides
    作者:Gao,Zeng; Et Al
    参考文献:Chemical Communications (Cambridge 日期:2020 卷标:56(53) 页码:7265-7268]

    90-14-2 = 879-18-5
    反应条件:1.1 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,1,1′-(9,9-Dimethyl-9H-Xanthene-4,5-Diyl)Bis[1,1-Diphenylphosphine] Solvents: Toluene; 12 H,125 °C
    标题:Metathesis-Active Ligands Enable A Catalytic Functional Group Metathesis Between Aroyl Chlorides And Aryl Iodides
    作者:Lee,Yong Ho; Et Al
    参考文献:Nature Chemistry 日期:2018 卷标:10(10) 页码:1016-1022]

    52710-27-7 + 90-14-2 = 879-18-5 + 126261-84-5
    反应条件:1.1 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,1,1′-(9,9-Dimethyl-9H-Xanthene-4,5-Diyl)Bis[1,1-Diphenylphosphine] Solvents: Toluene; 12 H,100 °C
    标题:Metathesis-Active Ligands Enable A Catalytic Functional Group Metathesis Between Aroyl Chlorides And Aryl Iodides
    作者:Lee,Yong Ho; Et Al
    参考文献:Nature Chemistry 日期:2018 卷标:10(10) 页码:1016-1022]

    126261-84-5 = 879-18-5 + 126261-84-5
    反应条件:1.1 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,1,1′-(9,9-Dimethyl-9H-Xanthene-4,5-Diyl)Bis[1,1-Diphenylphosphine] Solvents: Toluene; 12 H,100 °C2.1 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,1,1′-(9,9-Dimethyl-9H-Xanthene-4,5-Diyl)Bis[1,1-Diphenylphosphine] Solvents: Toluene; 12 H,100 °C
    标题:Metathesis-Active Ligands Enable A Catalytic Functional Group Metathesis Between Aroyl Chlorides And Aryl Iodides
    作者:Lee,Yong Ho; Et Al
    参考文献:Nature Chemistry 日期:2018 卷标:10(10) 页码:1016-1022]

    126261-84-5 = 879-18-5 + 126261-84-5
    反应条件:1.1 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,1,1′-(9,9-Dimethyl-9H-Xanthene-4,5-Diyl)Bis[1,1-Diphenylphosphine] Solvents: Toluene; 12 H,125 °C2.1 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,1,1′-(9,9-Dimethyl-9H-Xanthene-4,5-Diyl)Bis[1,1-Diphenylphosphine] Solvents: Toluene; 12 H,100 °C
    标题:Metathesis-Active Ligands Enable A Catalytic Functional Group Metathesis Between Aroyl Chlorides And Aryl Iodides
    作者:Lee,Yong Ho; Et Al
    参考文献:Nature Chemistry 日期:2018 卷标:10(10) 页码:1016-1022]

    1711-09-7 + 126261-84-5 = 879-18-5 + 126261-84-5
    反应条件:1.1 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,1,1′-(9,9-Dimethyl-9H-Xanthene-4,5-Diyl)Bis[1,1-Diphenylphosphine] Solvents: Toluene; 12 H,100 °C2.1 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,1,1′-(9,9-Dimethyl-9H-Xanthene-4,5-Diyl)Bis[1,1-Diphenylphosphine] Solvents: Toluene; 12 H,100 °C
    标题:Metathesis-Active Ligands Enable A Catalytic Functional Group Metathesis Between Aroyl Chlorides And Aryl Iodides
    作者:Lee,Yong Ho; Et Al
    参考文献:Nature Chemistry 日期:2018 卷标:10(10) 页码:1016-1022]

    126261-84-5 + 21615-34-9 = 879-18-5 + 126261-84-5
    反应条件:1.1 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,1,1′-(9,9-Dimethyl-9H-Xanthene-4,5-Diyl)Bis[1,1-Diphenylphosphine] Solvents: Toluene; 12 H,100 °C2.1 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,1,1′-(9,9-Dimethyl-9H-Xanthene-4,5-Diyl)Bis[1,1-Diphenylphosphine] Solvents: Toluene; 12 H,100 °C
    标题:Metathesis-Active Ligands Enable A Catalytic Functional Group Metathesis Between Aroyl Chlorides And Aryl Iodides
    作者:Lee,Yong Ho; Et Al
    参考文献:Nature Chemistry 日期:2018 卷标:10(10) 页码:1016-1022]

    126261-84-5 = 879-18-5 + 126261-84-5
    反应条件:1.1 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,1,1′-(9,9-Dimethyl-9H-Xanthene-4,5-Diyl)Bis[1,1-Diphenylphosphine] Solvents: Toluene; 12 H,100 °C2.1 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,1,1′-(9,9-Dimethyl-9H-Xanthene-4,5-Diyl)Bis[1,1-Diphenylphosphine] Solvents: Toluene; 12 H,100 °C
    标题:Metathesis-Active Ligands Enable A Catalytic Functional Group Metathesis Between Aroyl Chlorides And Aryl Iodides
    作者:Lee,Yong Ho; Et Al
    参考文献:Nature Chemistry 日期:2018 卷标:10(10) 页码:1016-1022]

    126261-84-5 + 7377-26-6 = 879-18-5 + 126261-84-5
    反应条件:1.1 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,1,1′-(9,9-Dimethyl-9H-Xanthene-4,5-Diyl)Bis[1,1-Diphenylphosphine] Solvents: Toluene; 12 H,100 °C2.1 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,1,1′-(9,9-Dimethyl-9H-Xanthene-4,5-Diyl)Bis[1,1-Diphenylphosphine] Solvents: Toluene; 12 H,100 °C
    标题:Metathesis-Active Ligands Enable A Catalytic Functional Group Metathesis Between Aroyl Chlorides And Aryl Iodides
    作者:Lee,Yong Ho; Et Al
    参考文献:Nature Chemistry 日期:2018 卷标:10(10) 页码:1016-1022]

    86-55-5 = 879-18-5
    反应条件:1.1 Catalysts: Dimethylformamide Solvents: Dichloromethane; 5 Min,0 °C1.2 Reagents: Oxalyl Chloride; 0 °C; 4 H,25 °C
    标题:Simple And Practical Conversion Of Benzoic Acids To Phenols At Room Temperature
    作者:Xiong,Wenzhang; Et Al
    参考文献:Journal Of The American Chemical Society 日期:2022 卷标:144(34) 页码:15894-15902]

    90-14-2 = 879-18-5
    反应条件:1.1 Reagents: Benzyltriphenylphosphonium Chloride Catalysts: Bis(Tri-Tert-Butylphosphine)Palladium Solvents: Toluene; 24 H,22 °C -> 110 °C
    标题:A Palladium-Catalyzed Carbonylation Approach To Acid Chloride Synthesis
    作者:Quesnel,Jeffrey S.; Et Al
    参考文献:Journal Of The American Chemical Society 日期:2013 卷标:135(45) 页码:16841-16844]

    90-11-9 = 879-18-5
    反应条件:1.1 Reagents: Benzyltriphenylphosphonium Chloride Catalysts: Bis(Tri-Tert-Butylphosphine)Palladium Solvents: Toluene; 24 H,20 Atm,Rt -> 110 °C
    标题:Acid Chloride Synthesis By The Palladium-Catalyzed Chlorocarbonylation Of Aryl Bromides
    作者:Quesnel,Jeffrey S.; Et Al
    参考文献:Chemistry - A European Journal 日期:2015 卷标:21(26) 页码:9550-9555]

    100-20-9 + 90-14-2 = 879-18-5 + 624-38-4
    反应条件:1.1 Catalysts: 2241736-67-2 Solvents: Benzene-D6; 20 H,110 °C
    标题:Functional Group Transposition: A Palladium-Catalyzed Metathesis Of Ar-X σ-Bonds And Acid Chloride Synthesis
    作者:De La Higuera Macias,Maximiliano; Et Al
    参考文献:Journal Of The American Chemical Society 日期:2018 卷标:140(32) 页码:10140-10144]

    90-14-2 = 879-18-5
    反应条件:1.1 Catalysts: 2241736-67-2 Solvents: Benzene; 20 H,90 °C
    标题:Functional Group Transposition: A Palladium-Catalyzed Metathesis Of Ar-X σ-Bonds And Acid Chloride Synthesis
    作者:De La Higuera Macias,Maximiliano; Et Al
    参考文献:Journal Of The American Chemical Society 日期:2018 卷标:140(32) 页码:10140-10144]

    126261-84-5 = 879-18-5 + 126261-84-5
    反应条件:1.1 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,1,1′-(9,9-Dimethyl-9H-Xanthene-4,5-Diyl)Bis[1,1-Diphenylphosphine] Solvents: Toluene; 12 H,100 °C2.1 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,1,1′-(9,9-Dimethyl-9H-Xanthene-4,5-Diyl)Bis[1,1-Diphenylphosphine] Solvents: Toluene; 12 H,100 °C
    标题:Metathesis-Active Ligands Enable A Catalytic Functional Group Metathesis Between Aroyl Chlorides And Aryl Iodides
    作者:Lee,Yong Ho; Et Al
    参考文献:Nature Chemistry 日期:2018 卷标:10(10) 页码:1016-1022]

    126261-84-5 + 129714-97-2 = 879-18-5 + 126261-84-5
    反应条件:1.1 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,1,1′-(9,9-Dimethyl-9H-Xanthene-4,5-Diyl)Bis[1,1-Diphenylphosphine] Solvents: Toluene; 12 H,100 °C2.1 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,1,1′-(9,9-Dimethyl-9H-Xanthene-4,5-Diyl)Bis[1,1-Diphenylphosphine] Solvents: Toluene; 12 H,100 °C
    标题:Metathesis-Active Ligands Enable A Catalytic Functional Group Metathesis Between Aroyl Chlorides And Aryl Iodides
    作者:Lee,Yong Ho; Et Al
    参考文献:Nature Chemistry 日期:2018 卷标:10(10) 页码:1016-1022]

    126261-84-5 + 4521-61-3 = 879-18-5 + 126261-84-5
    反应条件:1.1 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,1,1′-(9,9-Dimethyl-9H-Xanthene-4,5-Diyl)Bis[1,1-Diphenylphosphine] Solvents: Toluene; 12 H,100 °C2.1 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,1,1′-(9,9-Dimethyl-9H-Xanthene-4,5-Diyl)Bis[1,1-Diphenylphosphine] Solvents: Toluene; 12 H,100 °C
    标题:Metathesis-Active Ligands Enable A Catalytic Functional Group Metathesis Between Aroyl Chlorides And Aryl Iodides
    作者:Lee,Yong Ho; Et Al
    参考文献:Nature Chemistry 日期:2018 卷标:10(10) 页码:1016-1022
1-萘甲酸置于氯化亚砜体系中,化学反应 1.0H,反应生成 1-萘甲酰氯
参考文献:从羧酸中高效无酸和无金属一锅法合成苯并噻唑
标题:从羧酸中高效无酸和无金属一锅法合成苯并噻唑
摘要:羧酸在与亚硫酰氯的一锅反应中转化为苯并噻唑,然后在无酸和无催化剂条件下用 2-氨基苯硫酚处理.
DOI:10.1055/s-2005-872092

海关参考信息

专利信息


专利号:US-11926589-B2
优先权日:2019-07-09
标 题 :Process for the synthesis of non-racemic cyclohexenes
发明人：REISMAN SARAH; ROMBOLA MICHAEL; LADD CAROLYN L; MCLAUGHLIN MARTIN JOHN; ZUEND STEPHAN; GOETZ ROLAND
权利人:BASF CORP; CALIFORNIA INST OF TECHN
摘要:This invention relates to a process for the synthesis of a non-racemic cyclohexene compound of formula (I) by a Diels-Alder reaction of a compound of formula (II) with a compound of formula (III) wherein R 1 , R 2 , R 3 , R 4 , R 5 , R 6 , R 7 , R 8 , R 9 and Y have the meanings as defined in the description in the presence of a catalyst comprising at least one m-valent metal cation M m+ wherein the metal M is selected from Scandium (Sc), Yttrium (Y), Lanthanum (La), Cerium (Ce), Praseodymium (Pr), Neodymium (Nd), Promethium (Pm), Samarium (Sm), Europium (Eu), Gadolinium 15 (Gd), Terbium (Tb), Dysprosium (Dy), Holmium (Ho), Erbium (Er), Thulium (Tm), Ytterbium (Yb), Lutetium (Lu), Gallium (Ga) and Indium (In), and m is an integer of 1, 2 or 3, and a chiral ligand of the formula (IV) wherein R 10a , R 10b , R 10c , R 10d , R 10a′ , R 10b′ , R 10c′ , R 10d′ , Z and Z′ have the meanings as defined in the description.

专利号:US-5714127-A
优先权日:1992-10-08
标题 :System for multiple simultaneous synthesis
发明人：DEWITT SHEILA H H; KIELY JOHN S; PAVIA MICHAEL R; SCHROEDER MEL C; STANKOVIC CHARLES J
权利人:WARNER LAMBERT CO
摘要:A system for the multiple, simultaneous synthesis of compounds preferably uses a reaction apparatus comprising a reservoir rack having a plurality of reaction wells, a plurality of reaction tubes, usually gas dispersion tubes, having filters on their lower ends, a holder block, having a plurality of apertures, and a manifold, which has ports to allow introduction/maintenance of a controlled environment. The manifold top wall has a plurality of apertures in axial alignment with the reaction tubes and a gasket which allows penetration by a needle in order to dispense and aspirate materials from the reaction tubes. Sealing members, such as gaskets, are placed between the holder block, manifold and reservoir rack and the components are releasably fastened together. A robotic sample processor is used to automate the synthesis process using the reaction apparatus.

专利号:US-5702672-A
优先权日:1992-10-08
标 题 :Apparatus and method for multiple simultaneous synthesis
发明人：DEWITT SHEILA H H; KELL MICHAEL; PAVIA MICHAEL R; KIELY JOHN S; SCHROEDER MEL C; STANKOVIC CHARLES J; WARE STEVEN
权利人:WARNER LAMBERT CO
摘要:An apparatus for multiple, simultaneous synthesis of compounds which consists of: a reservoir block having a plurality of wells; a plurality of reaction tubes, usually gas dispersion tubes, having filters on their lower ends; a holder block, having a plurality of apertures; and a manifold, which may have ports to allow introduction/maintenance of a controlled environment. The manifold top wall has apertures and a detachable plate with identical apertures. The apparatus is constructed from materials which will accommodate heating, cooling, agitation, or corrosive reagents. Gaskets are placed between the components. Rods or clamps are provided for fastening the components together. Apparatus operation involves placing the filters on the lower ends of the reaction tubes in the reservoir block wells, and the upper ends passing through the holder block apertures and into the manifold.

专利号:US-5766556-A
优先权日:1992-10-08
标题:Apparatus and method for multiple simultaneous synthesis
发明人：DEWITT SHEILA HELEN HOBBS; KIELY JOHN STEVEN; PAVIA MICHAEL RAYMOND; SCHROEDER MEL CONRAD; STANKOVIC CHARLES JOHN
权利人:WARNER LAMBERT CO
摘要:An apparatus and method which provides a suitable location for multiple, simultaneous synthesis of compounds. The apparatus consists of: a reservoir block having a plurality of wells; a plurality of reaction tubes, usually gas dispersion tubes, having filters on their lower ends; a holder block, having a plurality of apertures; and a manifold, which may have ports to allow introduction/maintenance of a controlled environment. The manifold top wall has apertures and a detachable plate with identical apertures. The apparatus is constructed from materials which will accommodate heating, cooling, agitation, or corrosive reagents. Gaskets are placed between the components. Rods or clamps are provided for fastening the components together. Apparatus operation involves placing the filters on the lower ends of the reaction tubes in the reservoir block wells, and the upper ends passing through the holder block apertures and into the manifold. The apparatus provides in excess of 1 mg of each product with structural knowledge and control over each compound. The apparatus can be adapted to manual, semiautomatic or fully automatic performance. Using the apparatus a series of building blocks are covalently attached to a solid support. These building blocks are then modified by covalently adding additional different building blocks or chemically modifying some existing functionality until the penultimate structure is achieved. This is then cleaved from the solid support by another chemical reaction into the solution within the well yielding an array of newly synthesized individual compounds, which after postreaction modification, if necessary, are suitable for testing for activity.

专利号:US-5567391-A
优先权日:1992-10-08
标题 :Apparatus for multiple simultaneous synthesis
发明人：DEWITT SHEILA H H; KIELY JOHN S; PAVIA MICHAEL R; SCHROEDER MEL C; STANKOVIC CHARLES J
权利人:WARNER LAMBERT CO
摘要:An apparatus and method which provides a suitable location for multiple, simultaneous synthesis of compounds. The apparatus consists of: a reservoir block having a plurality of wells; a plurality of reaction tubes, usually gas dispersion tubes, having filters on their lower ends; a holder block, having a plurality of apertures; and a manifold, which may have ports to allow introduction/maintenance of a controlled environment. The manifold top wall has apertures and a detachable plate with identical apertures. The apparatus is constructed from materials which will accommodate heating, cooling, agitation, or corrosive reagents. Gaskets are placed between the components. Rods or clamps are provided for fastening the components together. Apparatus operation involves placing the filters on the lower ends of the reaction tubes in the reservoir block wells, and the upper ends passing through the holder block apertures and into the manifold. The apparatus provides in excess of 1 mg of each product with structural knowledge and control over each compound. The apparatus can be adapted to manual, semiautomatic or fully automatic performance. Using the apparatus a series of building blocks are covalently attached to a solid support. These building blocks are then modified by covalently adding additional different building blocks or chemically modifying some existing functionality until the penultimate structure is achieved. This is then cleaved from the solid support by another chemical reaction into the solution within the well yielding an array of newly synthesized individual compounds, which after postreaction modification, if necessary, are suitable for testing for activity.

专利号:US-6608196-B2
优先权日:2001-05-03
标题 :Process for solid supported synthesis of pyruvate-derived compounds
发明人：WANG BING; JANAGANI SATYANARAYANA; CALLAWAY WYETH B; SESSLER JONATHAN L
权利人:GALILEO PHARMACEUTICALS INC
摘要:Provided are processes for synthesizing structurally diverse pyruvate-derived compounds using a parallel approach on a solid phase support. Examples of such a solid phase support include resins which have also been used in solid phase peptide synthesis.

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✅ COA系统入驻 | 共享模式

主要参考文献

[参考文献]: Agnieszka Zgoa-Grzekowiak, Et Al. Solid-Phase Extraction Combined With Dispersive Liquid-Liquid Microextraction, Fast Derivatisation And High Performance Liquid Chromatography-Tandem Mass Spectrometry Analysis For Trace Determination Of Short-Chained Dodecyl Alcohol Ethoxylates And Dodecyl Alcohol In Environmental Water Samples. J Chromatogr A. 2012 Aug 17:1251:40-47.
[参考文献]: John W Huffman, Et Al. 3-Indolyl-1-Naphthylmethanes: New Cannabimimetic Indoles Provide Evidence For Aromatic Stacking Interactions With The Cb(1) Cannabinoid Receptor. Bioorg Med Chem. 2003 Feb 20;11(4):539-49.

合成参考文献


摘要:Davies, G. H. M.; Wisniewski, S. R., Science of Synthesis Knowledge Updates, (2021) 2, 121.
摘要:Bubnov, Yu. N.; Kolomnikova, G. D., Science of Synthesis Knowledge Updates, (2012) 3, 272.
摘要:Davies, G. H. M.; Wisniewski, S. R., Science of Synthesis Knowledge Updates, (2021) 2, 214.
摘要:Lubell, W. D.; St-Cyr, D. J.; Dufour-Gallant, J.; Hopewell, R.; Boutard, N.; Kassem, T.; Dörr, A.; Zelli, R., Science of Synthesis Knowledge Updates, (2013) 1, 288.
摘要:Mérour, J.-Y.; Joseph, B., Science of Synthesis Knowledge Updates, (2016) 3, 316.
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