CAS: 591-19-5; 3-Bromoaniline

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CAS号915923-02-3 2-(3-溴苯氧基)丙酰胺 | CAS号591-18-4 1-溴-3-碘苯 | CAS号585-79-5 间溴硝基苯 | CAS号621-38-5 3-溴-N-乙酰苯胺 | CAS号111762-31-3 magnesium,bromo... | CAS号40887-80-7 3-溴苯肼 | CAS号22726-00-7 3-溴苯甲酰胺 | CAS号60670-67-9 3-bromo-N-(3-((... | CAS号25216-74-4 N-(叔丁氧羰基)-3-溴苯胺 | CAS号1075719-78-6 2-(3,4-二溴苯基)-4,... | CAS号104997-09-3 N-(3-氨基苯基)苯磺酰胺 | CAS号110598-30-6 (3-氨基苯炔基)三甲基硅烷 | CAS号823-54-1 3-溴4-氯苯胺 | CAS号615-55-4 3,4-二溴苯胺 | CAS号608-22-0 2,3-二溴苯胺 | CAS号3638-73-1 2,5-二溴苯胺 | CAS号40787-96-0 3-溴-4-硝基苯胺 | CAS号5228-61-5 5-溴-2-硝基苯胺 | CAS号4965-36-0 7-溴喹啉

间溴苯甲酸置于氯化亚砜,Hydroxylamine-O-Sulfonic Acid体系中,化学反应生成 间溴苯胺
参考文献:Migration To Electron-Deficient Nitrogen. A One Pot Synthesis Of Aromatic And Heteroaromatic Amines From Carboxylic Acids
标题:Migration To Electron-Deficient Nitrogen. A One Pot Synthesis Of Aromatic And Heteroaromatic Amines From Carboxylic Acids
摘要:在干燥的甲苯中,采用羟胺-O-磺酸对一系列酰氯和异氮烯氯化物进行回流处理,可以得到相应的芳香胺,产率非常好.
DOI:10.1055/s-1990-27117

专利信息

专利号:US-7713446-B2
优先权日:2004-06-28
标 题:Synthesis of nanofibers of polyaniline and substituted derivatives
发明人：EPSTEIN ARTHUR J; CHIOU NAN-RONG
权利人:OHIO STATE UNIVERISTY
摘要:Novel, simple methods are presented directed to the synthesis of nanofibers of polyaniline and substituted derivatives. The production of these fibers is achieved via various methods by controlling the concentration of aniline monomer or substituted aniline derivatives or an oxidant in the reaction medium and maintaining said concentration at a level much lower than conventional polyaniline synthesis methods. Methods are disclosed relating to the use of a permeable membrane to control the release of a monomer and/or oxidant as well as a bulk polymerization method.

专利号:WO-9410327-A1
优先权日:1992-10-28
标 题 :Enzymatic synthesis of polyaniline
发明人：ZEMEL HAYA; QUINN JOHN F
权利人:ALLIED SIGNAL INC
摘要:This invention relates to a process for the enzymatic synthesis of electrically conductive substituted and unsubstituted polyanilines. Aniline monomer(s), an oxidizing agent, which comprises an enzyme and an electron acceptor, and an acidifying agent are reacted together to form polyanilines.

专利号:US-5420237-A
优先权日:1991-08-29
标 题:Enzymatic synthesis of polyaniline
发明人：ZEMEL HAYA; QUINN JOHN F
权利人:ALLIED SIGNAL INC
摘要:This invention relates to a process for the enzymatic synthesis of electrically conductive substituted and unsubstituted polyanilines. Aniline monomer(s), an oxidizing agent, which comprises an enzyme and an electron acceptor, and an acidifying agent are reacted together to form polyanilines.

专利号:US-11459427-B1
优先权日:2021-10-07
标题 :Synthesis of polyaniline or derivatives thereof
发明人：ALAMRY KHALID A; KHAN AJAHAR; ASIRI ABDULLAH MOHAMED
权利人:UNIV KING ABDULAZIZ
摘要:Provided are synthesis methods of polymerizing aniline or derivatives thereof. The production of polyaniline or polyaniline derivatives is controlled by the type of oxidant added in the reaction medium. The methods include the step of using a safe and environmentally friendly carbomethyl cellulose (CMC) or modified CMC as an oxidant in the polymerization reaction to produce polyaniline or aniline derivatives. Synthesis methods of producing O-CMC and O-CMC-S oxidants are also provided herein.

专利号:US-2022315594-A1
优先权日:2019-08-09
标 题 :Method of synthesis of compound for dual inhibition of jak2 and bet
发明人：UPADHAYAYA RAM SHANKAR; UKKALAM MURALI KRISHNA; SARMA K NARASIMHA
权利人:OHM ONCOLOGY
摘要:Embodiments of the invention include quinoline compounds and methods of synthesis. Ohm-581 has demonstrated dual inhibition of JAK2 and BET and acts as a therapeutic agent for micosis fungoides (MF) and other hematologic malignancies. Embodiments also include an efficient process for the preparation of Ohm-581 and pharmaceutically acceptable salts. The process is suited for large-scale production of quinoline compounds including Ohm-581.

专利号:US-9073900-B2
优先权日:2013-10-02
标题:Dihydroquinone derivatives of piperidine and piperazine
发明人：ULLAH NISAR
权利人:UNIV KING FAHD PET & MINERALS; KING ABDULAZIZ CITY SCI & TECH
摘要:The dihydroquinone derivatives of piperidine and piperazine are 7-piperazinyl and 7-piperadinyl-3,4-dihydroquinazolin-2(1H)-ones that exhibit D 2 and 5-HT 1A receptor binding affinities, making them suitable for use as the active ingredient of pharmaceuticals for the treatment of schizophrenia. The derivatives have the general formula: n nwhere X is carbon or nitrogen and R is a group selected from a through f having the formula:n n nor a pharmaceutically acceptable salt thereof. The piperazine compounds are prepared by condensing 4-bromo-2-nitro-benzonitrile with 1-Boc-piperazine (1-tert-butoxycarbonyl-piperazine) to form an intermediate that is converted to a piperazinyl-3,4-dihydroquinazolin-2(1H)-one. Subsequent reductive amination with the biarylaldehydes a through f completes the synthesis of the 7-piperadinyl-3,4-dihydroquinazolin-2(1H)-ones. The piperadinyl compounds are prepared from tert-butyl-4-(2-oxo-1,2,3,4-tetradihydroquinazolin-7-yl)piperidine-1-carboxylate, which is converted to 7-(piperidin-4-yl)-3,4-dihyroquinazolin-2(1H)-one. Subsequent reductive amination with the biarylaldehydes a through f completes the synthesis of the 7-piperidinyl-3,4-dihydroquinazolin-2(1H)-ones.