专利号:US-2018076373-A1 优先权日:2016-09-13 标题 :SOLUTION PHASE SYNTHESIS OF HIGHLY PROCESSIBLE NANOCRYSTALLINE LiZnP AND SIMILAR TERNARY SEMICONDUCTORS 发明人:Vela-Becerra Javier; White Miles Arthur Burris; THOMPSON MICHELLE JOANN; MILLER GORDON J 权利人:VELA BECERRA JAVIER; White Miles Arthur Burris; THOMPSON MICHELLE JOANN; MILLER GORDON J; UNIV IOWA STATE RES FOUND INC 摘要:Nowotny-Juza phases offer a wide range of potential applications including solar cell and thermoelectric device fabrication. The disclosure presents a solution phase synthesis of the Nowotny-Juza semiconductors LiZnP, LiCdP, and LiZnSb. These samples are phase pure, crystalline, and exhibit particle sizes of around 20 nm.
专利号:US-2024097109-A1 优先权日:2021-02-11 标 题:Bottom-Up, Scalable Synthesis Of Oxide-Based Sub-Nano And Nanofilaments And Nanofilament-Based Two-Dimensional Flakes And Mesoporous Powders 发明人:BARSOUM MICHEL W; BADR HUSSEIN OSAMA 权利人:UNIV DREXEL 摘要:Provided are methods to convert—through a bottom-up approach—binary and ternary titanium carbides, nitrides, borides, phosphides, aluminides, and silicides into lepidocrocitic nanofilaments that in some cases self-assemble into 2D flakes by immersing them in a quaternary ammonium solution at moderate temperatures. The resulting flakes can comprise nanofilaments in cross-section, some of which nanofilaments can be few microns long in some instances.
专利号:WO-2022174264-A1 优先权日:2021-02-11 标题:Bottom-up, scalable synthesis of oxide-based sub-nano and nanofilaments and nanofilament-based two-dimensional flakes and mesoporous powders 发明人:BADR HUSSEIN O; BARSOUM MICHEL W 权利人:UNIV DREXEL 摘要:Provided are methods to convert - through a bottom-up approach – binary and ternary titanium carbides, nitrides, borides, phosphides, aluminides, and silicides into nanofilaments that in some cases self-assemble into 2D flakes by immersing them in a quaternary ammonium solution at moderate temperatures. The resulting flakes can be C-containing anatase-based layers that are in turn comprised of nanofilaments in cross-section, some of which nanofilaments can be few microns long in some instances. Electrodes made from these materials performed well in energy systems. The materials also reduce the viability of some cancer cells. Also provided are mesoporous materials, devices, and related methods.
专利号:US-5350540-A 优先权日:1992-10-22 标题 :Method of making alkaline earth metal halophosphate phosphor using metal phosphide reducing agent 发明人:CHAU CHUNG-NIN 权利人:OSRAM SYLVANIA INC 摘要:Metal phosphide used as a raw material in the synthesis of alkaline earth metal halophosphate phosphor activated by antimony and manganese acts as a reducing agent to prevent oxidation of the antimony and manganese. The result is maximum availability of trivalent antimony and divalent manganese for incorporation into the phosphor lattice.
专利号:US-9790093-B2 优先权日:2016-01-19 标题:High-yield synthesis of nanostructured boron phosphide by a pyrotechnic method 发明人:LUAN ZHAOHUA; MORRIS LAUREN A; SHAW ANTHONY P; HAINES CHRISTOPHER D; PORET JAY C 权利人:US ARMY 摘要:A simplified method for synthesizing boron phosphide at high yields. The method requires mixing of boron phosphate and magnesium metal without diluents into a homogenous mixture, loosely packing the mixture at less than 20,000 psi and igniting the mixture using an energy input that is not greater than 20% of the reaction energy output to create a self-propagating high-temperature reaction wherein the boron phosphate and magnesium metal is completely burned during the reaction to synthesize boron phosphide at high yields.
专利号:US-8801979-B2 优先权日:2010-06-10 标题:Apparatus and method for continuous production of materials 发明人:CHANG CHIH-HUNG; JIN HYUNGDAE 权利人:CHANG CHIH-HUNG; JIN HYUNGDAE; OREGON STATE 摘要:Embodiments of a continuous-flow injection reactor and a method for continuous material synthesis are disclosed. The reactor includes a mixing zone unit and a residence time unit removably coupled to the mixing zone unit. The mixing zone unit includes at least one top inlet, a side inlet, and a bottom outlet. An injection tube, or plurality of injection tubes, is inserted through the top inlet and extends past the side inlet while terminating above the bottom outlet. A first reactant solution flows in through the side inlet, and a second reactant solution flows in through the injection tube(s). With reference to nanoparticle synthesis, the reactant solutions combine in a mixing zone and form nucleated nanoparticles. The nucleated nanoparticles flow through the residence time unit. The residence time unit may be a single conduit, or it may include an outer housing and a plurality of inner tubes within the outer housing.