CAS: 96-10-6; Diethylaluminum Chloride

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CAS号97-93-8 三乙基铝 | CAS号10038-98-9 氯化锗 | CAS号75-00-3 氯乙烷 | CAS号7646-85-7 氯化锌 | CAS号67-66-3 氯仿 | CAS号7550-45-0 四氯化钛 | CAS号54509-73-8 ethene | CAS号563-43-9 二氯乙基铝 | CAS号7429-90-5 铝片 | CAS号37556-02-8 (1-苯基丙基)丙二酸二乙酯 | CAS号3665-80-3 N-乙基-对-硝基苯胺 | CAS号74-84-0 乙烷 | CAS号557-17-5 甲基丙基醚 | CAS号93-55-0 苯丙酮 | CAS号6740-79-0 3-Phenyl-3-hydr... | CAS号30239-74-8 1-Butanone,2-et... | CAS号3457-55-4 1-phenylbutane-... | CAS号51449-77-5 2-(1H-替硝唑-5-基)苯酚 | CAS号928-97-2 反式-3-己烯-1-醇

三乙基铝置于三氯化铝体系中,用92.4%的收率获得产物氯化二乙基铝
参考文献:Method For Recovering Alkylaluminum Chlorides
标题:Method For Recovering Alkylaluminum Chlorides
摘要:揭示的是一种从含有不超过200Ppm锌浓度的二烷基氯化铝,烷基二氯化铝或二者混合物的混合物中回收产品的方法,其中所述烷基具有1至6个碳原子,所述方法包括在惰性气氛下将所述混合物与氯化铝反应,反应温度高达约150°C,然后蒸馏所述产品.

专利信息

专利号:US-11873305-B2
优先权日:2020-06-30
标题 :Processes for synthesis of substituted indole intermediates for the synthesis of serd compounds
发明人：ZHANG HAIMING; XU JIE; WUITSCHIK GEORG; ANGELAUD REMY; HEROLD SEBASTIAN; STUTZ ALFRED; BRUETSCH TOBIAS; BURKHARD JOHANNES
权利人:GENENTECH INC; HOFFMANN LA ROCHE
摘要:Provided herein are processes for the preparation of indolyl intermediates using Wenker Synthesis for the total synthesis of SERD compounds useful in the treatment of cancer.

专利号:US-7615169-B2
优先权日:2004-09-20
标题 :Method for synthesis of colloidal nanoparticles
发明人：STROUSE GEOFFREY FIELDING; GERBEC JEFFREY A; MAGANA DONNY
权利人:UNIV CALIFORNIA
摘要:A method for synthesis of high quality colloidal nanoparticles using comprises a high heating rate process. Irradiation of single mode, high power, microwave is a particularly well suited technique to realize high quality semiconductor nanoparticles. The use of microwave radiation effectively automates the synthesis, and more importantly, permits the use of a continuous flow microwave reactor for commercial preparation of the high quality colloidal nanoparticles.

专利号:US-7927516-B2
优先权日:2004-09-20
标题 :Method for synthesis of colloidal nanoparticles
发明人：STROUSE GEOFFREY F; GERBEC JEFFREY A; MAGANA DONNY
权利人:UNIV CALIFORNIA
摘要:A method for synthesis of high quality colloidal nanoparticles using comprises a high heating rate process. Irradiation of single mode, high power, microwave is a particularly well suited technique to realize high quality semiconductor nanoparticles. The use of microwave radiation effectively automates the synthesis, and more importantly, permits the use of a continuous flow microwave reactor for commercial preparation of the high quality colloidal nanoparticles.

专利号:US-6258960-B1
优先权日:2000-03-17
标题:Catalytic asymmetric synthesis of chiral aziridines
发明人：ANTILLA JON; WULFF WILLIAM D
权利人:ARCH DEV CORP
摘要:The present invention relates to the synthesis of chiral cis-aziridines (IIIa and IIIb) by reacting an imine (I) with a diazo compound (II) in the presence of a chiral vaulted biary-Lewis Acid complex as shown below:

专利号:US-9809661-B2
优先权日:2012-07-02
标 题 :Process for continuous synthesis of a diene elastomer
发明人：DUSSILLOLS JEROME; KIENER PIERRE; PAROLA HELENE
权利人:MICHELIN & CIE; MICHELIN RECH TECH; MICHELIN RECH TECH
摘要:A process for the continuous synthesis of diene elastomers with a high degree of conversion is provided. The process includes simultaneously:n a) introducing continuously into a polymerization reactor containing a gas phase and equipped with at least one stirring rotor and a discharge device, at least i. one or more monomers, including at least one conjugated diene monomer, and ii. from 0% to 70% by mass of an organic solvent, calculated relative to the total mass of monomers and of solvent b) continuously polymerizing the monomer(s), c) stirring the polymerization medium via the continuous movement of at least one stirring rotor about a rotary axle, d) continuously discharging the elastomer paste, e) continuously conveying the discharged elastomer paste to a chopping device and chopping it into particles, f) removing solvent from the particles of the elastomer paste, and g) recovering diene elastomer.

专利号:US-6020174-A
优先权日:1992-07-27
标题:Chemoenzymatic synthesis of the taxol C-13 side chain N-benzolyl- (2R,3S)-Phenylisoserine
发明人：CHEN CHING-SHIH; GOU DA-MING; LIU YEUK-CHUEN
权利人:RHODE ISLAND EDUCATION
摘要:(2R,3S)- and (2S,3R)-enantiomers of trans- beta -phenylglycidic esters, prepared by lipase-mediated enantioselective transesterification, are used for the synthesis of the taxol C-13 side chain with good yield.