CAS: 574-93-6; Phthalocyanine

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CAS号14320-04-8 酞菁锌 | CAS号10026-04-7 四氯化硅 | CAS号91-15-6 邻苯二甲腈 | CAS号85-44-9 苯酐 | CAS号504-29-0 2-氨基吡啶 | CAS号31643-49-9 4-硝基邻苯二甲腈 | CAS号183059-86-1 4-(p-tolylthio)... | CAS号160956-25-2 1,3-diimino-iso... | CAS号3317-67-7 酞菁钴 | CAS号14320-04-8 酞菁锌 | CAS号147-14-8 酞菁蓝 | CAS号14055-02-8 酞菁镍(II)

1,3-二亚胺基异吲哚啉置于金体系中,化学反应 0.17H,反应生成 酞青
参考文献:黄金(II)酞菁的再研究:黄金(iii)酞菁和前所未有的环收缩酞菁类似物的合成和光谱性质
标题:黄金(II)酞菁的再研究:黄金(iii)酞菁和前所未有的环收缩酞菁类似物的合成和光谱性质
摘要:1965年,有人描述了酞菁金(II)(aupc,1)是由未取代的1,3-二亚氨基异吲哚啉和金粉或aubr合成的.化合物1被认为是顺磁性金(II)配合物的罕见实例.但是,由于其未取代的结构所固有的1的固有不溶性,因此以前尚未对其化学性质,尤其是中心金离子的氧化态进行过探索.在我们尝试通过使用5,6-二取代的1,3-二亚氨基异吲哚啉,金(iii)酞菁氯化物(3)和前所未有的环收缩的酞菁类似物的金(iii)配合物来合成可溶性aupcs的过程中[18].三苯并五杂氮杂三卟啉(4,1,1),4)被隔离.鉴于原始文献的这一不同结果,使用未取代的1,3-二亚氨基异吲哚啉和各种金盐(包括金粉和aubr)对原始aupc合成进行了重新研究,发现只有3和4的未取代类似物或获得了游离碱酞菁.不能分离出含金(II)的物质.
DOI:10.1002/chem.201201701

专利信息

专利号:US-2011172437-A1
优先权日:2008-04-01
标题:Perfluorophthalocyanine Molecules and Methods of Synthesis
发明人：GORUN SERGIU M; GERDES ROBERT; GERDES OLGA; LAPOK LUKASZ
权利人:NEW JERSEY TECH INST
摘要:Advantageous methods for synthesis of fluorinated phthalocyanines are provided. Typical implementation involves a reaction mixture that includes perfluoro compound that is reacted for a reaction period sufficient to yield a fluorinated phthalocyanine of formula F 64 PcM, wherein “Pcâ€? is any phthalocyanine macrocycle and “Mâ€? is hydrogen. Novel fluorinated phthalocyanine molecules/compounds are also provided herein, including specifically compounds that include fluorinated phthalocyanines wherein “Mâ€? is Cu or Vâ•?O. The fluorinated phthalocyanines have wide ranging applications, e.g., corrosion-related applications, coating-related applications, catalysis, and the production of optical and electronic materials.

专利号:US-6491796-B1
优先权日:2001-06-26
标 题:Synthesis of phthalocyanines by microwave irradiation
发明人：HU ANDREW TEH; TSENG TSAI-WIE; HWU HERNG-DAR; LIU LUNG-CHANG; LEE CHUNG-CHUN; LEE MING-CHIA; CHEN JUN-RONG
权利人:AGI CORP; UNIV TSINGHUA
摘要:This invention provides a novel process for preparing soluble phthalocyanines by microwave irradiation in the absence of any organic solvent. Three different starting materials, i.e. t-butylphthalic anhydride, t-butyl phthalonitrile and metal-free H 2 Pc (tetra-t-butylphthalocyanine) have been adopted, respectively. The starting material with proper metal compound, such as chloride or acetate were irradiated in a commercial microwave oven for a period of 1 to 30 minutes at a power of 200Ëœ900 W. This process is noted to reduce drastically reaction time of MPc formation from 8Ëœ24 hours to 10Ëœ30 minutes due to its unique heating by microwave irradiation. Sandwiched type MPc 2 (such as Lu Pc 2 ) can be produced only through metal replacement from metal-free phthalocyanine by microwave irradiation.

专利号:US-2018171086-A1
优先权日:2016-12-16
标题 :Large area monolayer of perfluoro polymers
发明人：SUN HAORAN
权利人:SOUTH DAKOTA BOARD OF REGENTS
摘要:Synthesis and growth of large area free-standing ultra-thin two-dimensional (2D) polymeric films including 2D covalent organic frameworks (COF) are achieved by utilizing fluorocarbon-soluble fluorinated aldehyde derivatives and hydrocarbon-soluble amine derivatives at a liquid-liquid interface of respective fluorocarbon and hydrocarbon solvents.

专利号:US-2025010279-A1
优先权日:2021-11-17
标 题:Synthesis of carbonylation catalysts
发明人：WILDERS ALISON M; TEDDER JONATHAN D; BOYCE RONALD; JOSEPH ASHLEY
权利人:NOVOMER INC
摘要:A method including contacting a ligand complex, a metalation compound, and a metal carbonyl in a mixture to form a catalyst. The ligand complex includes one or more of phosphine, imine, and/or hydroxyl groups bound to one or more cyclic structures. The method includes separating the catalyst from the mixture. Contacting the ligand complex with a metalation compound and the metal carbonyl in the mixture to form a catalyst is conducted without isolating any intermediates, performed within a single vessel, and/or performed in a moisture, oxygen, and/or air free environment.

专利号:EP-1248788-B1
优先权日:1999-12-29
标 题 :Synthesis of isosorbide mononitrate
发明人：MARSTON RICHARD WALDRON; QUIGLEY PAUL FINBAR; BROWN CHRISTOPHER MARTIN; ROBERTS STANLEY MICHAEL; CROSS SIMON JOHN
权利人:CLARIANT LSM ITALIA SPA
摘要:A method of synthesising a compound of formula (1), in which each of R<1> and R<2> is independently selected from H or optionally substituted straight or branched chain C1-C30 alkyl, C1-C30 carboxyalkyl, C1-C30 sulphoxyalkyl, C1-C30 alkoxy, C3-C30 cycloalkyl, C3-C30 carboxycycloalkyl, C3-C30 sulphoxycycloalkyl, C3-C30 cycloalkoxy, heterocyclic, carboxyheterocyclic, sulphoxyheterocyclic, oxyheterocylic, C3-C30 cycloalkenyl, carboxycycloalkenyl, sulphoxycycloalkenyl or cycloalkenoxy, C8-C30 cycloalkynyl, carboxycycloalkynyl, sulphoxycycloalkynyl or cycloalkynoxy, C2-C30 alkynyl, carboxyalkynyl, sulphoxyalkynyl or alkynoxy group, C4-C30 aromatic, carboxyaromatic, sulphoxyaromatic or aryloxy, C4-C30 heteroaromatic, carboxyheteroaromatic, sulphoxyheteroaromatic or heteroaryloxy group, wherein in any of the hereto atom-containing groups the hetero atom is selected from O, S, and N; comprises treating a compound of formula (2) with a reducing system effective to reduce preferentially the compound of formula (2) at the 2-position to produce the compound of formula (1), wherein the reducing system comprises (i) hydrogen in the presence of a platinum-containing catalyst, or (ii) a hybride source in the presence of a transition metal phthalocyanine or polyphthalocyanine in which the transition metal is iron and/or cobalt.

专利号:US-2009004396-A1
优先权日:2007-06-26
标题:Highly-Branched, Allyl Ether-Functionalized, Unsaturated Polyester Resins and Coating Compositions of the Same
发明人：WU SHAOBING; BRANDENBURGER LARRY; MELNYK THOMAS
权利人:VALSPAR CORP
摘要:The synthesis of highly-branched, allyl ether-functionalized, unsaturated polyester resins is disclosed herein, along with the utility of these resins in formulating formaldehyde-free, isocyanate-free, and styrene-free, low temperature and fast curing solvent-borne coatings, including wood coatings, and their use as alternatives for conventional acid catalyzed urea- or melamine-crosslinked coating systems.