CAS: 629-93-6; 1-Iodooctadecane

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硬脂醇置于咪唑,碘,三苯基膦体系中,用 甲苯 作为反应溶剂,化学反应 2.0H,以82%的收率获得产物1-碘十八烷
参考文献:Irras研究了6-硫代伪糖脂的合成及其在金载玻片上的取向.
标题:Irras研究了6-硫代伪糖脂的合成及其在金载玻片上的取向.
摘要:我们合成了四个6-硫代伪糖脂类似物,并评估了其中两个如何在金表面上自组装.这些结构被设计为候选束缚分子,以将双层脂质膜锚定在金上.选择6-脱氧-6-硫代半乳糖以将大分子锚定在金上并在金表面限定水区.选择与糖残基的异头位置连接的长链烷烃链(c-12或c-18)以固定双层脂质膜.碳水化合物和疏水链之间的连接是糖苷键或由炔丙基十二烷和叠氮-十八烷的铜(i)催化的炔丙基糖苷的炔-叠氮化物环加成(cuaac)形成的1,4-二取代的三唑.我们期望烃链将自身垂直于金表面定向并结合到双层膜的第一张小叶中.我们已经使用红外反射吸收光谱法(irras)研究了c-12糖苷配基类似物在金上的自组装单分子层.我们将irras实验给出的结果与通过衰减全反射(atr)光谱记录在随机取向类似物薄膜上的ir光谱进行了比较.我们的结果表明,C-12类似物确实与金结合,并使其自身垂直于金载玻片.我们将irras实验给出的结果与
DOI:10.1016/j.Carres.2010.09.035

专利信息

专利号:EP-0021497-A1
优先权日:1979-06-21
标 题 :Synthesis of polyoxyalkylene glycol monoalkyl ethers
发明人：GIBSON THOMAS WILIAM
权利人:PROCTER & GAMBLE
摘要:A solvent free method for preparing monoalkyl ethers of polyoxyalkylene glycols, comprising mixing a polyoxyalkylene glycol, especially polyoxyethylene glycol, with a concentrated aqueous solution of a metal hydroxide, contacting said mixture with a primary alkyl halide, and recovering the monoalkyl ether.

专利号:CN-113880737-A
优先权日:2021-09-23
标 题 :Application of a new type of persulfide reagent in the synthesis of asymmetric persulfide

专利号:US-7101993-B1
优先权日:1990-01-11
标 题 :Oligonucleotides containing 2′-O-modified purines
发明人：COOK PHILLIP DAN; MCGEE DANIEL PETER CLAUDE; GUINOSSO CHARLES JOHN
权利人:ISIS PHARMACEUTICALS INC
摘要:Compounds are provided containing purine nucleotides that bear moieties X at the 2' position thereof wherein X is R₁-(R₂)_n; R₁ is C₃-C₂₀ alkyl, C₄-C₂₀ alkenyl or C₂-C₂₀ alkynyl; R₂ is halogen, hydroxyl, thiol, keto, carboxyl, nitro, nitroso, nitrile, trifluoromethyl, trifluoromethoxy, O-alkyl, S-alkyl, NH-alkyl, N-dialkyl, O-aryl, S-aryl, NH-aryl, O-aralkyl, S-aralkyl, NH-aralkyl, amino, N-phthalimido, imidazole, azido, hydrazino, hydroxylamino, isocyanato, sulfoxide, sulfone, sulfide, disulfide, silyl, aryl, heterocycle, carbocycle, intercalator, reporter molecule, conjugate, polyamine, polyamide, polyalkylene glycol, polyether, a group that enhances the pharmacodynamic properties of oligonucleotides, or a group that enhances the pharmacokinetic properties of oligonucleotides; and n is an integer from 0 to about 6. Such compounds are useful for modulating the synthesis of proteins.

专利号:CN-113880737-B
优先权日:2021-09-23
标 题:Application of novel persulfate reagent in synthesis of asymmetric polysulfide

专利号:JP-2011525927-A
优先权日:2008-06-25
标 题 :Synthesis and use of heterocyclic antibacterial agents

专利号:CN-118026908-A
优先权日:2023-12-27
标题 :Synthesis method of DIL or DID