CAS: 611-74-5; N,N-Dimethylbenzamide

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2-nitropropane N,N,N',N'-tetramethyl-C-phenylmethanediamine methyl N-methylbenzimidate N,N'-dimethylbenzylaminephenyl(pyridin-2-yl)methanone 3-benzoylindole 9-benzoyl-9H-carbazole phenyl thiobenzoate

过氧化苯甲酸叔丁酯置于叔丁基过氧化氢,Copper(II) Oxide体系中,用 水 作为反应溶剂,化学反应 40.0H,反应生成 N,N-二甲基苯甲酰胺
参考文献:源自单一来源分子前体的金属氧化物纳米催化剂可轻松地从氧化或不饱和有机化合物中获取酰胺
标题:源自单一来源分子前体的金属氧化物纳米催化剂可轻松地从氧化或不饱和有机化合物中获取酰胺
摘要:氧化酰胺化是将氧化的有机化合物转化为有价值的酰胺的有价值的过程.然而,该反应由于使用昂贵的催化剂和有限的底物范围而受到严重限制.为了克服这些限制,期望通过更直接和经济的方法设计具有优异的催化性能和广泛的底物范围的过渡金属基纳米催化剂.为解决上述问题,我们报道了一种通过溶胶-凝胶辅助复合物[ni(hep-H)(H2O)4] So 4(ssmp-1)的溶胶-凝胶热分解合成纳米催化剂nio和cuo的简便方法)和[cu(μ-Hep)(ba)] 2(ssmp-2)[hep-H = 2-(2-羟乙基)吡啶;ba通过使用=苯甲酸]为单源分子前体(ssmps)为苯甲醇,苯甲醛和ba的氧化酰胺化ñ,ñ二甲基甲酰胺(dmf)作作为反应溶剂和作为胺源,在存在叔在t = 80oc时,使用正丁基过氧化氢(tbhp)作为氧化剂.除纳米催化剂nio和cuo外,我们先前报道的co / Coo纳米催化剂(conc)源自复合物[co
DOI:10.1021/acs.Inorgchem.7B01576

专利信息

专利号:WO-2023039068-A1
优先权日:2021-09-08
标题:Compositions and methods for synthesis of peptide nucleic acid intermediates
发明人：COULL JAMES M; GILDEA BRIAN D
权利人:NEUBASE THERAPEUTICS INC
摘要:The present disclosure provides intermediates for the synthesis of peptide nucleic acid (PNA) backbones and monomers, such as cyclic intermediates, and methods of making the same.

专利号:US-8618281-B2
优先权日:2006-01-03
标 题 :Geometric synthesis of porphyrin rods
发明人：LINDSEY JONATHAN S; YU LIANHE; THAMYONGKIT PATCHANITA; BHISE ANIL D
权利人:LINDSEY JONATHAN S; YU LIANHE; THAMYONGKIT PATCHANITA; BHISE ANIL D; UNIV NORTH CAROLINA STATE
摘要:A method of making a compound of Formula I′ n ncomprises reacting a compound of the formula DLCHO, with a compound of the formulan n nto produce the compound of Formula I′. Methods of using the compounds are also described, particularly as intermediates for the synthesis of porphyrin rods, which porphyrin rods are in turn useful for (among other things) the production of molecular memory devices.

专利号:US-10611864-B2
优先权日:2015-09-22
标 题:Synthesis of substituted amidobenzoate compounds, the compounds obtained and the use thereof as phthalate free internal electron donor for polymerization of olefins
发明人：ZUIDEVELD MARTIN ALEXANDER; SAINANI JAIPRAKASH BRIJLAL; AL-HUMAIDAN OSAMAH; PADMANABHAN SUDHAKAR R; SHINGE PRASHANT SUKUMAR; SHETTY SHARANKUMAR G; SHAIKH ABBAS-ALLI GHUDUBHAI
权利人:SABIC GLOBAL TECHNOLOGIES BV
摘要:The present invention relates to a compound according to Formula (I) wherein R 1 is a hydrocarbyl group selected from the group consisting of alkyl, alkenyl, aryl, aralkyl, and alkylaryl groups, and one or more combinations thereof; wherein R 2 is a hydrogen atom, an aryl group or an alkyl group; and wherein R 3 , R 4 , R 5 and R 6 , are the same or different and are each independently a hydrogen atom, a halogen atom, a cyano group, an amino group, a hydrocarbyl group selected from the group consisting of alkyl, alkenyl, aryl, aralkyl, and alkylaryl groups or an alkoxy group, and one or more combinations thereof as internal electron donor and to a process for the synthesis of a compound according to Formula (I), wherein R 1 is a hydrocarbyl group selected from the group consisting of alkyl, alkenyl, aryl, aralkyl, alkoxycarbonyl and alkylaryl groups, and one or more combinations thereof; wherein R 2 is a hydrogen atom or an alkyl group; wherein R 3 , R 4 , R 5 and R 6 , are the same or different and are each independently selected from a group consisting of a hydrogen atom; a hydrocarbyl, preferably, said process comprising the step of reacting a compound according to Formula (II) [R 1 —C(â•?O)Cl] with a compound according to Formula (III) to obtain the compound according to Formula (I) and to the use of these compounds as internal donor in Ziegler-Natta catalysis of lefins.

专利号:WO-8103020-A1
优先权日:1980-04-22
标 题 :Triazine synthesis
发明人：HARRIS R
权利人:COMMW SCIENT IND RES ORG; HARRIS R
摘要:A process for the synthesis of substituted 1,3,5-triazine compounds of the general formula: (FORMULA) wherein Rs and Rs, which may be the same or different, are selected from the group consisting of hydrogen, halogen, alkoxycarbonyl, alkyl, substituted alkyl, aryl, substituted aryl, heteroaryl, substituted heteroaryl, alkylamino, dialkylamino, arylamino, alkyl-arylamino, alkylthio, arylthio, alkoxy and aryloxy (provided that Rs and Rs are not both halogen); and Rs is selected from the group consisting of halogen, alkylamino, dialkylamino, arylamino, alkyl-arylamino and N-heteroaryl; comprises reaction of a substituted halomethyleneiminium salt with a substituted N-cyanoamidine, N-cyanoguanidine, N-cyanocarbamimidate or N-cyanocarbamidothioate. Substituted 1,3,5-triazine compounds having fungal germination inhibition properties are also disclosed. The following compounds 1) 2-chloro-4-phenyl-1,3,5-triazine, 2) 2-chloro-4-phenoxymethyl-6-phenyl-1,3,5-triazine, 3) 2-N-methylphenylamino-4-phenyl-1,3,5-triazin, 4) 2-chloro-4-cyanomethyl-6-phenyl-1,3,5-triazine are also disclosed and claimed.

专利号:US-2004152897-A1
优先权日:2002-09-13
标 题 :Synthesis of indolizines
发明人：SUN LIJUN; KOYA KEIZO; XIA ZHI-QIANG; PRZEWLOKA TERESA; ZHANG SHIJIE; ONO MITSUNORI
权利人:SYNTA PHARMACEUTICALS CORP
摘要:Disclosed are methods of preparing substituted indolizines represented by the following formula: n n n comprising reacting a substrate represented by the following formula: n n n with either the cyclization reagent of the following formula: n n n or, a reagent prepared by reacting the compound represented the formula below with an alkylating agent: n n n The variables in the above formulas are defined herein.

专利号:US-10053420-B2
优先权日:2015-01-30
标 题 :Processes for the preparation of compounds, such as 3-arylbutanals, useful in the synthesis of medetomidine
发明人：EKLUND LARS; EEK MARGUS; EKAMBARAM RAMESH; MAASALU ANTS
权利人:CAMBREX KARLSKOGA AB
摘要:There is provided a process for the preparation of a compound of formula (I) as defined herein, wherein said process comprises reacting a compound of formula (II) as defined s herein with one or more suitable Vilsmeier reagent.