CAS: 605-70-9; Naphthalene-1,4-Dicarboxylic Acid

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38153-01-4 57322-45-9 7487-15-2

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CAS号3029-30-9 萘-1,4-二腈 | CAS号18274-34-5 1,4-dihydronaph... | CAS号83-53-4 1,4-二溴萘 | CAS号571-58-4 1,4-二甲基萘 | CAS号91-20-3 萘 | CAS号30716-26-8 4-methyl-1-(nit... | CAS号4488-40-8 4-甲基-1-萘甲酸 | CAS号24157-79-7 1,4-二异丙基萘 | CAS号5261-50-7 1-氯甲基-4-甲基萘 | CAS号29903-04-6 naphthalene-1-c... | CAS号5690-24-4 1,4,5,8-萘四甲酰基二酰亚胺 | CAS号5089-22-5 荧光增白剂KCB | CAS号57322-45-9 萘-1,4-二基二甲醇 | CAS号3451-02-3 tetramethyl ben... | CAS号7487-15-2 1,4-萘二甲酸二甲酯 | CAS号43115-21-5 2,2'-(naphthale... | CAS号476-73-3 benzene-1,2,3,4... | CAS号40350-11-6 5-methylsulfony...

1,4-二甲基萘置于sodium Dichromate体系中,用 水 作为反应溶剂,化学反应生成 1,4-萘二甲酸
参考文献:分散介质中 1,8-萘二甲酸二钾的锌 (II) 催化汉克尔反应
标题:分散介质中 1,8-萘二甲酸二钾的锌 (II) 催化汉克尔反应
摘要:与没有分散介质的反应相比,1,8-萘二甲酸二钾在作为分散介质的萘中的汉克尔反应以更高的产率和更好的重现性得到了 2,6-萘二甲酸二钾 (1).详细研究了催化剂,特别是锌催化剂.锌催化剂的阴离子部分影响反应,卤化物阴离子对1的选择性形成有效.在锌催化剂中加入卤化钾也提高了1的产率.卤化物阴离子的催化活性依次增加; 氯-
DOI:10.1246/bcsj.62.786

专利信息

专利号:US-12263464-B2
优先权日:2018-03-14
标题 :Method for in-situ synthesis of metal organic frameworks (MOFs), covalent organic frameworks (COFs) and zeolite imidazolate frameworks (ZIFs), and applications thereof
发明人：PAHWA DEEPAK; PAHWA VARUN; CHOUDHARY ANIL KUMAR; SONIA; JHA VIVEK KUMAR; CHAUHAN ANJALI; YADAV ANNU
权利人:DESICCANT ROTORS INTERNATIONAL PRIVATE LTD
摘要:The present invention relates to a method for the in situ synthesis of of MOFs (metal organic frameworks), COFs (covalent organic frameworks), and ZIFs (Zeolitic imidazolate framework), onto and within different types of porous substrates, and their applications. The present invention provides a unique and easy to utilize method by which a number of MOFs, COFs and ZIFs can be synthesized directly onto and within a porous substrate with high performance efficiency ensuring higher grammage in formation of adsorbent product onto and within the substrate.

专利号:US-7880026-B2
优先权日:2006-04-14
标 题 :MOF synthesis method
发明人：NI ZHENG; MASEL RICHARD I
权利人:UNIV ILLINOIS
摘要:A rapid, simple and versatile metal organic framework molecule (MOF) synthesis method particularly adapted to make non-linear MOFs includes heating MOF precursors, such as a metal or metal oxide and an organic ligand, in a microwave oven for a period sufficient to achieve crystallization. Microwave-assisted MOF synthesis yields high quality MOF crystals in a reaction time ranging from about 5 seconds to about 2.5 minutes, compared to hours and days required in conventional solvothermal and hydrothermal methods. In addition, microwave assisted methods provide MOF materials with uniform crystal size and well-defined shape. Further, microwave synthesis of MOFs allows the size and shape of MOF crystals to be tailored for use in a wide range applications by manipulating reaction conditions. Secondary growth processes may also be employed to grow larger crystals using seeds obtained from microwave-assisted synthesis methods.

专利号:US-10737239-B2
优先权日:2015-11-27
标题 :Ultrafast high space-time-yield synthesis of metal-organic frameworks
发明人：BURCKHART JULIA; MARX STEFAN; ARNOLD LENA; HOFMANN CLAUS; Müller Ulrich
权利人:BASF SE
摘要:The invention relates to a process for the preparation of metal-organic frameworks (MOFs) in form of a homogenous powder, and a process wherein the metal-organic framework is molded into shaped bodies.

专利号:US-9951095-B2
优先权日:2014-05-16
标 题:Chromium metal organic frameworks and synthesis of metal organic frameworks
发明人：ZHOU HONG-CAI; Liu tian-fu; LIAN XIZHEN; ZOU LANFANG; FENG DAWEI
权利人:TEXAS A & M UNIV SYS
摘要:The present invention relates to monocrystalline metal organic frameworks comprising chromium ions and carboxylate ligands and the use of the same, for example their use for storing a gas. The invention also relates to methods for preparing metal organic frameworks comprising chromium, titanium or iron ions and carboxylate ligands. The methods of the invention allow such metal organic frameworks to be prepared in monocrystalline or polycrystalline forms.

专利号:US-12371444-B2
优先权日:2018-07-19
标 题:Methods of making MOFs, systems for synthesizing MOFs, and methods of coating textiles with MOFs
发明人：GIRI GAURAV; HUELSENBECK LUKE
权利人:UNIV VIRGINIA PATENT FOUNDATION
摘要:A method of synthesis of metal organic frameworks (“MOFsâ€?) includes preparing a metal solution by dissolving at least one metal salt in an aqueous solution and buffering the metal solution with a base to achieve a first pH, the metal solution optionally comprising an organic co-solvent, preparing a linker solution by adding at least one organic acid linker and at least one base to an aqueous solution, and mixing the metal solution and the linker solution to produce the MOFs. The at least one organic acid linker has an ability to be protonated or deprotonated in response to a second pH, and the mixture of the metal solution and the linker solution has a third pH value, where the third pH value is greater than a highest pKa of the organic acid linker. The MOFs may be applied to a textile.

专利号:US-2024316508-A1
优先权日:2021-07-13
标题:Electrical synthesis of continuous metal-organic framework memranes
发明人：EDDAOUDI MOHAMED; ZHOU SHENG; SHEKHAH OSAMA; JIA JIANGTAO
权利人:UNIV KING ABDULLAH SCI & TECH
摘要:Embodiments include a method of making a continuous metal-organic framework membrane, the method including contacting a rare earth- or zirconium-containing compound, an acid, a solvent, and optionally water sufficient to form a hexanuclear cluster solution, contacting the hexanuclear cluster solution with one or more ditopic ligands sufficient to form a metal-organic framework (MOF) solution, contacting the MOF solution with a support, and applying a current to the MOF solution with support, sufficient to provide a continuous metal-organic framework membrane.