专利号:US-2016214860-A1 优先权日:2013-09-19 标题:Method of synthesis of unsolvated mixed cation borohydrides 发明人:JARON TOMASZ; WEGNER WOJCIECH; GROCHALA WOJCIECH 权利人:JAROÑ Tomasz; WEGNER WOJCIECH; GROCHALA WOJCIECH 摘要:The present invention relates to a novel method of synthesis of unsolvated mixed cation borohydrides of a general formula M x M′ y (BH 4 ) z , where M and M′ stand for metal cations, x, y, and z are stoichiometric coefficients. The method of synthesis according to the present invention is characterised in that the precursors having a general formula M[A n ] u and [Cat] v M′(BH 4 ) w are used for the synthesis, where [An] stands for a weakly coordinating anion; [Cat] stands for weakly coordinating cation; u, v, and w are the stoichiometric coefficients; and the synthesis is carried out under an inert to the reagents atmosphere—according to the general reaction equation: x M[An] u +y [Cat] v M′(BH 4 ) w →M x M′ y (BH 4 ) z +xu [Cat][An] where z=yw, xu=yv; M x M′ y (BH 4 ) z is the product of the reaction.
专利号:US-2004249114-A1 优先权日:2001-02-06 标题 :Methods of synthesis of polysuccinimide or polyaspartate by end capping polymerization 发明人:SWIFT GRAHAM; REDLICH GEORGE H; WEHBY JOHN NOLAN 摘要:Disclosed are methods of synthesis of homopolymers or copolymers containing succinimide or aspartate moieties formed in the presence of an end capping initiator. Also disclosed are methods of isolating, compounding, stabilizing and processing the homopolymers and copolymers.
专利号:US-4522886-A 优先权日:1984-10-09 标 题 :Method of ion beam synthesis of thin silicon nitride films and resulting articles 发明人:CHIN ROLAND L; FERGUSON SUSAN A 权利人:ALLIED CORP 摘要:A method is disclosed for the synthesis of ultra-thin silicon nitride (Si x N y ) films by the direct interaction of a low energy noble ion beam (e.g. Ar + or He + ), with NH 3 physically absorbed on a silicon surface. The method is directed toward applications which require the use of ultra-thin insulating layers, such as in MIS technology. n The disclosed method provides for the synthesis of ultra-thin films of silicon nitride via the interaction of NH 3 absorbed on a silicon substrate and a low energy nobel ion beam. Preferential absorption of NH 3 is effected by cooling of the substrate below the boiling point of NH 3 . The ion beam is used to generate reactive N and Si species which combine to form compounds of silicon nitride. The physical appearance of the films formed by this method is comparable to those produced by low pressure chemical vapor deposition.
专利号:US-2023257270-A1 优先权日:2020-07-10 标 题 :Synthesis of carbon nano-onions by nanodiamond annealing and functionalization of carbon materials 发明人:GOLSHARIFI NIMA; AMAKUBO SUGURU FREDERICK 权利人:NDB INC 摘要:Disclosed herein are methods of synthesizing carbon nano-onions, their functionalization methods, and their use as electrode material. More specifically, disclosed are methods of converting nanodiamonds into carbon nano-onions, chemical synthesis of carbon nano-onions from reagents, and functionalization using reagents, reactive gases, and photoexcitation. The use of the synthesized and functionalized carbon nano-onions as an electrode by using them as a composite structure is also disclosed.
专利号:US-2006211843-A1 优先权日:2001-02-06 标题:Methods of synthesis of poly(succinimide-aspartate) polysuccinimide or polyaspartate by end capping polymerization 发明人:SWIFT GRAHAM; REDLICH GEORGE H 权利人:SWIFT GRAHAM; REDLICH GEORGE H 摘要:Disclosed are methods of synthesis of homopolymers or copolymers containing succinimide or aspartate moieties formed in the presence of an end capping initiator. Also disclosed are methods of isolating, compounding, stabilizing and processing the homopolymers and copolymers.
专利号:US-6919421-B2 优先权日:2001-02-06 标 题:Methods of synthesis of polysuccinimide, copolymers of polysuccinimide and derivatives thereof 发明人:SWIFT GRAHAM 权利人:FOLIA INC 摘要:Disclosed are methods of synthesis of polysuccinimide, copolymers, derivatives and blends with additives thereof, using a supercritical fluid. Also disclosed are methods of isolating, compounding, stabilizing and processing the polysucciminide, its copolymers and derivatives.
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