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CAS号3674-54-2 四丁基硫氰酸铵 | CAS号33657-49-7 丁酸氯甲酯 | CAS号380-60-9 3,3,4,4,4-penta... | CAS号3637-31-8 4,4,5,5,5-五氟戊酸 | CAS号107-92-6 正丁酸 | CAS号34851-41-7 四丁基甲醇铵 溶液 | CAS号43064-96-6 四丁基氰基硼烷化铵 | CAS号429-41-4 四丁基氟化铵 | CAS号429-42-5 四丁基四氟硼酸铵 | CAS号51693-17-5 (S)-(+)-5-羟甲基-2... | CAS号187409-10-5 1-chloro-3-(1,2...合成工艺路线路线简述
- 合成目标产物 Bis(Tetrabutylammonium) Sulphate 主要起始原料 Tetrabutylammonium Hydroxide
- (文献来源)合成步骤主要原料 Tetrabutylammonium Hydroxide
四丁基碘化铵置于thallium(I) Sulfate体系中,用 水 用作溶剂,化学反应 16.0H,反应生成四正丁基硫酸铵
参考文献:具有广泛可调带填充的分子金属.共面连接的聚合酞菁金属电化学中的结构/化学计量/反离子关系
标题:具有广泛可调带填充的分子金属.共面连接的聚合酞菁金属电化学中的结构/化学计量/反离子关系
摘要:研究了共面连接的酞菁聚合物 (Si(Pc)O){sub N} 的氧化电化学,以产生 ((Si(Pc)O)X{sub Y}){sub N} 类型的分子金属/导电聚合物通过 X 射线衍射和光谱技术的结合.电化学方法包括应用于快速搅拌的浆液或固体聚合物的微压实的受控电位库仑法和电化学电位谱 (Ecps).对于 X{sup {minus}} = Bf{sub 4}{sup {minus}} 在乙腈中,聚合的斜方晶系 (Si(Pc)O){sub N} 氧化(掺杂)以产生四方晶系((si( Pc)O)(Bf{sub 4}){sub N}) (Y {approx} 0.50) 伴随着显着的过电位,Y 的最小可调性,并且涉及一阶结构相变.电化学去掺杂在更宽的电位范围 (0.90 V) 内平稳发生,以提供四方晶 (Si(Pc)O){sub N},也可通过热去掺杂 ((Si(Pc)O)I{sub 1.1}) {子
Doi:10.1021/ja00196A037
专利信息
专利号:US-7241399-B2
优先权日:2000-09-08
标题 :Synthesis of nanoparticles
发明人:HAUBOLD STEPHAN; HAASE MARKUS; RIWOTZKI KARSTEN; WELLER HORST; MEYSSAMY HEIKE; IBARRA FERNANDO
权利人:CT ANGEWANDTE NANOTECH CAN
摘要:Methods for the preparation of inorganic nanoparticles capable of fluorescence, wherein the nanoparticles consist of a host material that comprises at least one dopant. The synthesis of the invention in organic solvents allows to gain a considerably higher yield compared to the prior art synthesis in water. All kinds of objects can advantageously be marked and reliably authenticated by using an automated method on the basis of a characteristic emission. Further, the size distribution of the prepared nanoparticles is nartower which renders a subsequent size-selected separation process superfluous.
专利号:WO-2014080341-A1
优先权日:2012-11-21
标题 :New process for the synthesis of trichloropyrimidine-amine derivatives
发明人:Czibula László; Dobay László; SZAVICSKÓ KRISZTINA; KISS-BARTOS DOROTTYA; Nagyné Bagdy Judit
权利人:RICHTER GEDEON NYRT
摘要:The invention relates to a new process for the synthesis of 2-(N-methyl)-amino-4,5,6- trichloro-l,3-pyrimidine, which is more economical than the known process, as well as the new compounds synthesized as intermediates in the process: 2-(N',N'-dimethylamino- methylene)-amino-4,5,6-trichloro-l,3-pyrimidine and 2-(N-formyl)-amino-4,5,6-trichloro-l,3- pyrimidine.
专利号:EP-1232226-B1
优先权日:2000-09-08
标题:Synthesis of nanoparticles
发明人:HAUBOLD STEPHAN; HAASE MARKUS; RIWOTZKY CARSTEN; WELLER HORST; MEYSAMMY HEIKE; IBARRA FERNANDO
权利人:NANOSOLUTIONS GMBH
摘要:Production of inorganic nanoparticles that can be fluoresced consisting of a host material containing a dopant comprises using an organic solvent for liquid phase synthesis of the particles.
专利号:US-9267213-B1
优先权日:2005-03-25
标题:Electrochemical deblocking solution for electrochemical oligomer synthesis on an electrode array
发明人:MAURER KARL; COOPER JOHN J
权利人:CUSTOMARRAY INC
摘要:There is disclosed an electrochemical deblocking solution for use on an electrode microarray. There is further disclosed a method for electrochemical synthesis on an electrode array using the electrochemical deblocking solution. The solution and method are for removing acid-labile protecting groups for synthesis of oligonucleotides, peptides, small molecules, or polymers on a microarray of electrodes while substantially improving isolation of deblocking to active electrodes. The method comprises applying a voltage or a current to at least one electrode of an array of electrodes. The array of electrodes is covered by the electrochemical deblocking solution.
专利号:US-7312340-B2
优先权日:2003-02-05
标 题:Synthesis of 2-butyl-3-(1-trityl-1H-tetrazol-5-YL)biphenyl-4-YL)-1,3-diazaspiro[4,4]- non-ene-4-one
发明人:DOLITZKY BEN-ZION; KAFTANOV JULIA; PERTSIKOV BORIS; RUKHMAN IGOR; NISNEVICH GENNADY
权利人:TEVA PHARMA
摘要:Provided is a novel method of making 2-butyl-3-[[2′(1-trityl-1H-tetrazol-5-yl)biphen-4-yl]methyl]-1,3-diazaspiro[4.4]non-1-ene-4-one, which can be converted to irbesartan. Also provided are methods of making irbesartan.
专利号:US-7838683-B2
优先权日:2003-01-16
标题:Synthesis of irbesartan
发明人:NISNEVICH GENNADY; RUKHMAN IGOR; PERTSIKOV BORIS; KAFTANOV JULIA; DOLITZKY BEN-ZION
权利人:TEVA PHARMA
摘要:Provided are a method of making irbesartan via a Suzuki coupling reaction and a novel intermediate, 2-butyl-3-(4′-bromobenzyl)-1,3-diazaspiro[4.4]non-1-ene-4-one, for such process. The novel process includes the step of reacting such intermediate with a protected imidazolephenylboronic acid.