9005-53-2 = 697-82-5 + 488-17-5 + 496-16-2 + 876-02-8 + 90-00-6 + 93-51-6 + 496-78-6 + 527-55-9 + 134-96-3 反应条件:1.1 Catalysts: Choline Chloride,Imidazole; 150 °C 标题:Insights Into Alkaline Choline Chloride-Based Deep Eutectic Solvents Pretreatment For Populus Deltoides: Lignin Structural Features And Modification Mechanism 作者:Li,Haichao; Et Al 参考文献:International Journal Of Biological Macromolecules 日期:2021 卷标:193 页码:319-327]
9005-53-2 = 697-82-5 + 103-81-1 + 831-00-5 + 60826-26-8 + 2219-78-5 + 74421-05-9 + 22607-11-0 + 94391-24-9 + 219726-60-0 + 7443-70-1 + 51504-54-2 + 72386-20-0 反应条件:1.1 Reagents: Sodium Hydroxide Catalysts: Molybdenum,Copper Solvents: Methanol,Water; 7 H,220 °C1.2 Reagents: Water 标题:Cu-Mo Doped Zeolite Zsm-5 Catalyzed Conversion Of Lignin To Alkyl Phenols With High Selectivity 作者:Singh,Sunit Kumar; Et Al 参考文献:Catalysis Science & Technology 日期:2015 卷标:5(4) 页码:2117-2124
异佛尔酮置于lithium Chloride体系中,用 N,N-二甲基甲酰胺 作为反应溶剂,化学反应生成 2,3,5-三甲基苯酚 参考文献:Halogenation With Copper(II). Ii. Unsaturated Ketones 标题:Halogenation With Copper(II). Ii. Unsaturated Ketones 摘要: DOI:10.1021/jo01038A008
专利号:WO-2025132814-A1 优先权日:2023-12-21 标 题:Novel synthesis of methyl-2-fluoroacrylate 发明人:BRUNKE JESSICA; FISCHER MICHAEL; WÖSSNER JAN STEPHAN 权利人:VIFOR INT AG 摘要:The present invention relates to novel synthesis methods of methyl 2-fluoroacrylate (MFA) which is a key precursor for the production of Veltassa® (Patiromer). The methods according to the invention are conducted by reacting an α-substituted β-hydroxy propionic acid derivative (I) via one or more intermediate steps involving one or more α-, β-substituted propionic acid derivatives (II) to obtain MFA (III).
专利号:US-5670465-A 优先权日:1993-01-08 标题 :Preparation of p-fuchsones and synthesis of p-dihydroxylated aromatic compounds therefrom 发明人:COSTANTINI MICHEL; MANAUT DANIEL; MICHELET DANIEL 权利人:RHONE POULENC CHIMIE 摘要:p-Dihydroxylated aromatic compounds are prepared via the oxidation of p-fuchsones, the latter advantageously being synthesized by reacting a phenolic compound having at least one hydrogen atom in the para-position to the hydroxyl function with a non-enolizable ketonic compound, in the presence of a catalytically effective amount of an acid catalyst and, optionally, a cocatalytically effective amount of an ionizable sulfur-containing compound.
专利号:US-10287412-B2 优先权日:2012-10-18 标题:Process for the preparation of hierarchically meso and macroporous structured materials 发明人:KARTHIK MANI; FAIK ABDESSAMAD; DOPPIU STEFANIA 权利人:CIC ENERGIGUNE 摘要:The present invention describes a hierarchical graphitized carbon foam comprising an interconnected macroporous structure with an ordered mesoporous wall structure, a process for its preparation, as well as to a process for the synthesis of a variety of bimodal porous organic polymer and/or inorganic metal oxide materials.
专利号:WO-0112791-A1 优先权日:1999-08-12 标 题 :Dna shuffling of dioxygenase genes for production of industrial chemicals 发明人:SELIFONOV SERGEY A; NEWMAN LISA M 权利人:MAXYGEN INC; SELIFONOV SERGEY A; NEWMAN LISA M 摘要:This invention provides improved polypeptides, including dioxygenases, dehydrogenases, ligases and transferases that are useful for the biocatalytic synthesis of compounds such as α-hydroxycarboxylic acids, and aryl- and alkyl-hydroxy and carboxylic acid compounds. The polypeptides provided herein are improved in properties such as regioselectivity, enzymatic activity, stereospecificity, and the like. Methods for obtaining recombinant polynucleotides that encode these improved polypeptides are also provided, as are organisms that express the polypeptides and are thus useful for carrying out said biocatalytic syntheses. Also provided by the invention are methods for increasing said solvent resistance of organisms that are used in the synthetic methods.
专利号:US-2004110228-A1 优先权日:2002-04-01 标 题:Combinatorial organic synthesis of unique biologically active compounds 发明人:MCALPINE SHELLI R; TAYLOR RACHEL E; BOLLA MEGAN L; SEGALL ANCA M 摘要:The invention provides a method for making a combinatorial library of cyclic compounds, such as Holliday junction-trapping compounds, comprising the steps of (a) obtaining a plurality of trimers according to the generic structure X 1- X 2- X 3 , wherein X 1 , X 2 and X 3 can be independently any naturally or nonnaturally occurring amino acids or peptidomimetics thereof; (b) optionally coupling a spacer S to the trimer at either end; (c) cyclizing two trimers or trimer-spacer conjugates in a head-to-tail orientation; thereby obtaining a combinatorial library of compounds, wherein the library does not include an unmodifed or naturally occurring Holliday Junction-trapping compounds. The invention additionally provides methods macrocyclic compounds that are synergimycin derivatives.
专利号:WO-2019053605-A1 优先权日:2017-09-12 标题 :SYNTHESIS OF TOCOTRIENOLS FROM O-CRESOL DERIVATIVES 发明人:SAMBASIVAM GANESH; VASANTRAO GADAKH AMOL; A M SATHIYANARAYANAN; KASTURCHAND GODHA ATUL 权利人:ANTHEM BIOSCIENCES PRIVATE LTD 摘要:The present invention provides an environmentally benign, facile process for preparation of Tocotrienols from commercially available derivatives of o-Cresol.
[参考文献]: H. Dakshinamurty, Et Al. Syntheses Of Polymethylphenols And Their Derivatives. I.J. Org. Chem. 1962, 27, 5, 1839–1842. [参考文献]: Shu-Ling Lin, Et Al. Preparation And Evaluation Of Poly(Alkyl Methacrylate-Co-Methacrylic Acid-Co-Ethylene Dimethacrylate) Monolithic Columns For Separating Polar Small Molecules By Capillary Liquid Chromatography. Anal Chim Acta. 2015 Apr 29:871:57-65.
合成参考文献
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