CAS: 6212-33-5; 2-Amino-2-(4-Chlorophenyl)Acetic Acid

相似化合物

67336-19-0 43189-37-3 53994-85-7

上下游产品

CAS号7099-88-9 (4-氯苯基)乙醛酸 | CAS号6212-32-4 5-(4-chlorophen... | CAS号24091-92-7 2'-溴-4-氯苯乙酸甲酯 | CAS号39546-47-9 1-氯-4-(异氰基甲基)苯 | CAS号104-88-1 对氯苯甲醛 | CAS号39533-35-2 α-Is°Cyano-p-ch... | CAS号140-53-4 对氯苯乙腈 | CAS号43189-37-3 (R)-4-氯苯甘氨酸 | CAS号110314-98-2 4-(4-chlorophen... | CAS号43189-20-4 对氯苯甘氨酸甲酯 | CAS号544-10-5 氯(代)正己烷 | CAS号43189-43-1 d-4-氯苯甘氨酸甲酯 | CAS号43189-37-3 (R)-4-氯苯甘氨酸 | CAS号42718-19-4 2-氨基-2-(4-氯苯基)乙... | CAS号623-03-0 对氯苯腈 | CAS号53994-85-7 N-B°C-(4'-氯苯基)甘氨酸 | CAS号629-06-1 1-氯庚烷

5-(4-氯苯基)咪唑烷-2,4-二酮置于potassium Carbonate体系中,用 水 作为反应溶剂,178.0 °C,2.5 Mpa 条件下,反应 0.07H,反应生成 Dl-对氯苯甘氨酸
参考文献:一种连续快速制备dl-苯甘氨酸及其类似物的方法
标题:一种连续快速制备dl-苯甘氨酸及其类似物的方法
摘要:本发明提供一种连续快速制备dl‑苯甘氨酸及其类似的方法,包括:将2‑羟基‑苯乙腈及其类似物(简称氰醇)与碳铵水溶液加入微通道反应器进行反应,控制反应温度为80~130°C,压力为0.5~2.0Mpa,反应物在微通道内停留时间为1~8Min,得到5‑苯基‑乙内酰脲及其类似物(简称海因)水溶液;将海因与碱加入微通道反应器进行反应,控制反应温度为120~200°C,压力为1.0~3.5Mpa,反应物在微通道内的停留时间为1~8Min,得到苯甘氨酸及其类似物盐水溶液,经酸化中和,结晶,得到苯甘氨酸及其类似物.本发明采用微通道反应器,大大缩短了反应时间,加快反应速率,减少了氰醇热解聚合,无副产物产生,产品收率高,清洁环保,降低了生产成本.

专利信息

专利号:US-10458995-B2
优先权日:2016-03-25
标 题 :Combinatorial synthesis and biomarker development
发明人：MOOLA MURALIDHAR REDDY
权利人:MOOLA MURALIDHAR REDDY
摘要:Provided herein are methods, kits, and compositions for use in the diagnosis and treatment of diseases. Peptoids recognized by Alzheimers disease specific antibodies are identified.

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