2-甲基-1,3-二恶烷置于偶氮二异丁腈,氯体系中,化学反应生成 3-氯丙基乙酸酯 参考文献:Rakhmankulov,D.L. Et Al.,Journal Of Applied Chemistry Of The Ussr,1975,Vol. 48,P. 968-969 标题:Rakhmankulov,D.L. Et Al.,Journal Of Applied Chemistry Of The Ussr,1975,Vol. 48,P. 968-969
专利号:US-2023312617-A1 优先权日:2020-07-25 标题 :Process for synthesis of organosilicon compounds from halosilanes 发明人:DOLAI SUKANTA; BHAT SHREEDHAR; TARAFDAR GOURAV 权利人:MOMENTIVE PERFORMANCE MAT INC 摘要:A process for synthesis of an organosilicon compound is provided herein. Also, novel organosilicon compounds prepared by the present process is provided herein. The process comprises the reaction of a halosilane with an organofunctional alkyl halide in the presence of a metal catalyst, a promoter, and an optional co-catalyst. The process provides an efficient synthetic route to produce organosilicon compounds. The process also allows synthesis of organosilicon compounds with a plurality of different functional groups.
专利号:US-8299309-B2 优先权日:2007-11-20 标题:Synthesis of hydrofluoroalkanols and hydrofluoroalkenes 发明人:NAPPA MARIO JOSEPH; SUN XUEHUI; YAGUPOLSKII LEV MOISEEVICH; FILATOV ANDREY ANATOLIEVICH; BOIKO VLADIMIR NIKOLAEVICH; YAGUPOLSKII YURII LVOVICH 权利人:NAPPA MARIO JOSEPH; SUN XUEHUI; YAGUPOLSKII LEV MOISEEVICH; FILATOV ANDREY ANATOLIEVICH; BOIKO VLADIMIR NIKOLAEVICH; YAGUPOLSKII YURII LVOVICH; DU PONT 摘要:Described herein is a process for the manufacture of hydrofluoroalkanols of the structure R f CFClCHROH. Also described herein are methods of manufacturing hydrofluoroalkenes of the structure R f CFâ•?CHR from halofluorocarbons of the structure R f CFX 2 . In particular, 2,3,3,3,-tetrafluoro-1-propene may be manufactured with this process. Also described are compounds of the formula R f CFClCHROC(â•?O)R′.
专利号:US-9371334-B2 优先权日:2010-09-22 标题:Synthesis of substituted salicylaldehyde derivatives 发明人:FARMER JAY J; JOB GABRIEL E 权利人:NOVOMER INC 摘要:Among other things, the present invention encompasses methods of synthesizing salicylaldehyde derivatives comprising the steps of: a) providing salicylaldehyde or a derivative thereof, b) forming an anhydro dimer of the provided salicylaldehyde compound, c) performing one or more chemical transformations on the anhydro dimer and d) hydrolyzing the anhydro dimer to provide a salicylaldehyde derivative different from that provided in step (a).
专利号:US-10040800-B2 优先权日:2010-09-22 标 题:Synthesis of substituted salicylaldehyde derivatives
专利号:US-2012083619-A1 优先权日:2007-11-20 标 题:Synthesis of Hydrofluoroalkanols and Hydrofluoroalkenes
专利号:US-2015011761-A1 优先权日:2010-09-22 标题 :Synthesis of substituted salicylaldehyde derivatives
摘要:Zeitschrift fuer die Gesamte Hygiene und Ihre Grenzgebiete., 26(17), 1980 [] 摘要:Zhang, M.; Hanson, P. R., Science of Synthesis, (2007) 20, 928. 摘要:Virieux, D.; Volle, J.-N.; Pirat, J.-L., Science of Synthesis, (2009) 42, 526.