CAS: 934-60-1; 6-Methyl-2-Pyridinecarboxylic Acid
该化合物是一种含有分子式C7H7NO2的杂交有机化合物,其分子式为C7H7NO2,其特点是在皮球酸脚架的6处放置一个甲基组,该化合物是制药和农用化学合成的多用途中间体,特别是在开发金属切合剂和生物活性分子方面,其丙烯酮-碳oxylic酸结构能够与金属离子协调,使其在催化和材料科学应用方面有用.甲基替代可增强其亲脂性,从而影响合成途径的溶性和再活性.可精确应用的高纯度可用作精度,确保研究和工业过程的一贯性能.
相似化合物
1122-71-0 1122-72-1 13602-11-4物理性质
MSDS等安全信息
- GHS象形图
- GHS符号GHS07;
注释: Exclamation mark - 危险类别特定目标器官毒性 - 单次接触 类别3
皮肤腐蚀/刺激 类别2
严重眼刺激 类别2
严重眼刺激 类别2A - 警示词Warning(警告)
- 危险描述H335 |可能引起呼吸道刺激.
H315 |造成皮肤刺激.
H319 |造成严重眼刺激. - 防范说明P261-P264-P270-P271-P280-P302+P352-P304+P340-P305+P351+P338-P330-P362+P364-P403+P233-P405-P501
- 危险等级IRRITANT
- UN编号NONH for all modes of transport
- 危险品标志Xi
- 安全声明26-36/37/39-36
- 危险类别码36/37/38
- WGK Germany3
欧盟法规
ECHA物质C&L通报REACH预注册上下游产品
2,6-dimethylpyridine 6-methyl-2-pyridinecarboxaldehyde 2-(6-methylpyridin-2-yl)-ethanol 3-methylbenzene-1,2-diol ethyl 6-methylpyridine-2-carboxylate (4-Methoxy-phenyl)-(6-methyl-[2]pyridyl)-methanol 6-methyl-1-oxy-pyridine-2-carboxylic acid 2-(6-methylpyridin-2-yl)-benzooxazole合成工艺路线路线简述
- 合成目标产物 6-Methyl-2-Pyridinecarboxylic Acid 主要起始原料 2,6-Lutidine
- 108-48-5 = 934-60-1
反应条件:1.1 Reagents: Permanganic Acid (Hmno4),Potassium Salt (1:1) Solvents: Water; 300 Min,60 °C; 5 H,Rt
标题:A Kind Of Polysubstituted Pyridines Medicine Intermediate And The Synthetic Method Thereof
参考文献:China]
108-48-5 = 934-60-1
反应条件:1.1 Reagents: Chromium Trioxide
标题:Liquid-Phase Oxidation Of 2,6-Lutidine And 2,4,6-Collidine With Sodium Bichromate And Chromium Trioxide
作者:Kreile,D.; Milman,I. A.; Eglite,D.; Krumina,L.; Sile,D.; Et Al
参考文献:Zhurnal Prikladnoi Khimii (Sankt-Peterburg 日期:1978 卷标:51(7) 页码:1644-8]
108-48-5 = 934-60-1
反应条件:1.1 Reagents: Oxygen Catalysts: Cobalt Diacetate,N-Hydroxyphthalimide,Manganese Diacetate Solvents: Acetic Acid
标题:Preparation Of Carboxylic Acids By Oxidation With Molecular Oxygen
参考文献:Japan]
1620-75-3 = 934-60-1 [标题:Reaction Conditions
标题:Picolinic Or 6-Methylpicolinic Acids
参考文献:Ussr]
108-48-5 = 934-60-1 [标题:Reaction Conditions
标题:Synthesis And Resolution Of Substituted Pipecolic Acids
作者:Overberger,C. G.; Shalati,M. D.
参考文献:European Polymer Journal 日期:1983 卷标:19(10-11) 页码:1055-65]
= 934-60-1 [标题:Reaction Conditions
标题:Syntheses Of Some Amide And Ester Derivatives Of 6-Methyl-2-Pyridinecarboxylic Acid Of Expected Activity On Circulatory System
作者:Gutkowska,Bozenna; Kabzinska,Zofia; Slowinski,Tomasz
参考文献:Acta Poloniae Pharmaceutica 日期:1996 卷标:53(2) 页码:133-135]
= 934-60-1 [标题:Reaction Conditions
标题:Active Oxygen-Inhibiting Compositions Containing Picolinic Acid Compounds,Electrolytes And Other Substances For Organ Preservation
参考文献:Japan]
= 934-60-1 + 116-53-0 + 4518-10-9 + 51-67-2 + 868-57-5 + 23950-04-1 + 13231-81-7 + 79491-14-8 + 83647-42-1 + 20282-39-7
反应条件:1.1 300 - 900 °C
标题:Synthesis And Pyrolysis Of Two Novel Pyrrole Ester Flavor Precursors
作者:Fan,Wenpeng; Et Al
参考文献:Journal Of Heterocyclic Chemistry 日期:2022 卷标:59(8) 页码:1397-1406]
34034-36-1 = 934-60-1 + 116-53-0 + 4518-10-9 + 51-67-2 + 868-57-5 + 23950-04-1 + 13231-81-7 + 79491-14-8 + 83647-42-1 + 20282-39-7
反应条件:1.1 Reagents: Potassium Carbonate Catalysts: Tetrabutylammonium Bromide Solvents: Acetonitrile; 17 H,65 °C2.1 Reagents: Sodium Borohydride Solvents: Methanol; 20 Min,0 °C2.2 Reagents: Sodium Chloride Solvents: Water; 2 Min3.1 Reagents: 1-Ethyl-3-(3′-Dimethylaminopropyl)Carbodiimide Solvents: Dichloromethane; 1 H,Rt3.2 Catalysts: 4-(Dimethylamino)Pyridine; 24 H,Rt4.1 300 - 900 °C
标题:Synthesis And Pyrolysis Of Two Novel Pyrrole Ester Flavor Precursors
作者:Fan,Wenpeng; Et Al
参考文献:Journal Of Heterocyclic Chemistry 日期:2022 卷标:59(8) 页码:1397-1406]
174293-65-3 = 934-60-1
反应条件:1.1 Reagents: Ammonium Chloride Solvents: Water; 10 Min,50 °C
标题:Production Of Pyridine Synthons By Biotransformations Of Benzene Precursors And Their Cyclization With Nitrogen Nucleophiles
作者:Matthews,Colette; Rossiter,John T.; Ribbons,Douglas W.; Geary,Philip J.; Ryback,George; Et Al
参考文献:Biocatalysis And Biotransformation 日期:1995 卷标:12(4) 页码:241-54]
= 934-60-1
反应条件:1.1 Reagents: Sodium Hydroxide Solvents: Ethanol,Water; Rt -> Reflux; 25 Min,Reflux; Reflux -> Rt1.2 Reagents: Hydrochloric Acid Solvents: Water; Ph 1,Rt
标题:A Long-Range Chiral Relay Via Tertiary Amide Group In Asymmetric Catalysis: New Amino Acid-Derived N,P-Ligands For Copper-Catalysed Conjugate Addition
作者:Malkov,Andrei V.; Hand,John B.; Kocovsky,Pavel
参考文献:Chemical Communications (Cambridge 日期:2003 卷标:(15) 页码:1948-1949]
1620-75-3 = 934-60-1
反应条件:1.1 Reagents: Hydrochloric Acid Solvents: Water; 24 H,Reflux
标题:Smart Contrast Agents Using Cyclodextrin Derivatives For Mri Imaging
参考文献:World Intellectual Property Organization]
108-48-5 = 934-60-1
反应条件:1.1 Reagents: Oxygen Solvents: Water; 54 H,Ph 7,30 °C1.2 Reagents: Methanol
标题:Bioconversion Of 2,6-Dimethylpyridine To 6-Methylpicolinic Acid By Exophiala Dermatitidis (Kano) De Hoog Da5501 Cells Grown On N-Dodecane
作者:Yoshida,Toyokazu; Sada,Yuki; Nagasawa,Toru
参考文献:Applied Microbiology And Biotechnology 日期:2010 卷标:86(4) 页码:1165-1170]
68470-59-7 = 934-60-1
反应条件:1.1 Reagents: Iodobenzene Diacetate Catalysts: (Sp-5-12)-Chloro[5,10,15,20-Tetrakis(4-Nitrophenyl)-21H,23H-Porphinato(2-)-Kn21,... Solvents: Methanol,Water; 12 H,50 °C
标题:Preparation Of 4,7-Diphenyl-1,10-Phenanthroline-2,9-Dicarboxylic Acid Catalyzed By Iron(Iii)Porphyrins With (Diacetoxyiodo)Benzene
作者:Zhong,Qi-Di; Xue,Yun-Zhou; Yan,Hong; Song,Xiu-Qing; Zhong,Ru-Gang
参考文献:Bioorganic & Medicinal Chemistry Letters 日期:2010 卷标:20(18) 页码:5532-5535]
108-48-5 = 934-60-1
反应条件:1.1 Reagents: Permanganic Acid (Hmno4),Potassium Salt (1:1) Solvents: Water; Rt
标题:Connecting Terminal Carboxylate Groups In Nine-Coordinate Lanthanide Podates: Consequences On The Thermodynamic,Structural,Electronic,And Photophysical Properties
作者:Senegas,Jean-Michel; Bernardinelli,Gerald; Imbert,Daniel; Bunzli,Jean-Claude G.; Morgantini,Pierre-Yves; Et Al
参考文献:Inorganic Chemistry 日期:2003 卷标:42(15) 页码:4680-4695]
= 934-60-1
反应条件:1.1 Reagents: Sodium Hydroxide Solvents: Ethanol,Water; 1 H,80 °C
标题:Preparation Of Compounds For Transforming Growth Factor Receptor Antagonists
参考文献:China]
108-48-5 = 934-60-1
反应条件:1.1 Reagents: Permanganic Acid (Hmno4),Potassium Salt (1:1) Solvents: Water; Rt -> 70 °C; 70 °C; 5 H,70 °C1.2 Reagents: Hydrochloric Acid Solvents: Water; Ph 3.3
标题:Preparation Of Aryl Sulfonamides As Antagonists Of Ccr9 Receptor
参考文献:United States]
488-17-5 = 934-60-1
反应条件:1.1 -1.2 Reagents: Ammonia Solvents: Water
标题:Catechol 2,3-Dioxygenase-Catalyzed Synthesis Of Picolinic Acids From Catechols
作者:Asano,Yasuhisa; Yamamoto,Yasushi; Yamada,Hideaki
参考文献:Bioscience 日期:1994 卷标:58(11) 页码:2954-6]
4593-07-1 = 934-60-1 [标题:Reaction Conditions
标题:Pyridine Derivatives
参考文献:Japan]
= 934-60-1 [标题:Reaction Conditions
标题:Use Of Indazole Compound For Treating Psoriasis
参考文献:World Intellectual Property Organization]
= 934-60-1 [标题:Reaction Conditions
标题:Smart Contrast Agents For Mri Imaging
参考文献:United States]
= 934-60-1 [标题:Reaction Conditions
标题:Preparation Of Heterocyclic Carboxylic Acids Or Ketones By Oxidation Of Heterocyclic Compounds
参考文献:Japan]
65-85-0 = 934-60-1 + 116-53-0 + 4518-10-9 + 51-67-2 + 868-57-5 + 23950-04-1 + 13231-81-7 + 79491-14-8 + 83647-42-1 + 20282-39-7
反应条件:1.1 Reagents: 1-Ethyl-3-(3′-Dimethylaminopropyl)Carbodiimide Solvents: Dichloromethane; 1 H,Rt1.2 Catalysts: 4-(Dimethylamino)Pyridine; 24 H,Rt2.1 300 - 900 °C
标题:Synthesis And Pyrolysis Of Two Novel Pyrrole Ester Flavor Precursors
作者:Fan,Wenpeng; Et Al
参考文献:Journal Of Heterocyclic Chemistry 日期:2022 卷标:59(8) 页码:1397-1406]
= 934-60-1 + 116-53-0 + 4518-10-9 + 51-67-2 + 868-57-5 + 23950-04-1 + 13231-81-7 + 79491-14-8 + 83647-42-1 + 20282-39-7
反应条件:1.1 Reagents: Sodium Borohydride Solvents: Methanol; 20 Min,0 °C1.2 Reagents: Sodium Chloride Solvents: Water; 2 Min2.1 Reagents: 1-Ethyl-3-(3′-Dimethylaminopropyl)Carbodiimide Solvents: Dichloromethane; 1 H,Rt2.2 Catalysts: 4-(Dimethylamino)Pyridine; 24 H,Rt3.1 300 - 900 °C
标题:Synthesis And Pyrolysis Of Two Novel Pyrrole Ester Flavor Precursors
作者:Fan,Wenpeng; Et Al
参考文献:Journal Of Heterocyclic Chemistry 日期:2022 卷标:59(8) 页码:1397-1406]
= 934-60-1 + 116-53-0 + 4518-10-9 + 51-67-2 + 868-57-5 + 23950-04-1 + 13231-81-7 + 79491-14-8 + 83647-42-1 + 20282-39-7
反应条件:1.1 300 - 900 °C2.1 Reagents: 1-Ethyl-3-(3′-Dimethylaminopropyl)Carbodiimide Solvents: Dichloromethane; 1 H,Rt2.2 Catalysts: 4-(Dimethylamino)Pyridine; 24 H,Rt3.1 300 - 900 °C
标题:Synthesis And Pyrolysis Of Two Novel Pyrrole Ester Flavor Precursors
作者:Fan,Wenpeng; Et Al
参考文献:Journal Of Heterocyclic Chemistry 日期:2022 卷标:59(8) 页码:1397-1406]
116-53-0 = 934-60-1 + 116-53-0 + 4518-10-9 + 51-67-2 + 868-57-5 + 23950-04-1 + 13231-81-7 + 79491-14-8 + 83647-42-1 + 20282-39-7
反应条件:1.1 Reagents: 1-Ethyl-3-(3′-Dimethylaminopropyl)Carbodiimide Solvents: Dichloromethane; 1 H,Rt1.2 Catalysts: 4-(Dimethylamino)Pyridine; 24 H,Rt2.1 300 - 900 °C3.1 Reagents: 1-Ethyl-3-(3′-Dimethylaminopropyl)Carbodiimide Solvents: Dichloromethane; 1 H,Rt3.2 Catalysts: 4-(Dimethylamino)Pyridine; 24 H,Rt4.1 300 - 900 °C
标题:Synthesis And Pyrolysis Of Two Novel Pyrrole Ester Flavor Precursors
作者:Fan,Wenpeng; Et Al
参考文献:Journal Of Heterocyclic Chemistry 日期:2022 卷标:59(8) 页码:1397-1406]
33302-94-2 = 934-60-1 + 116-53-0 + 4518-10-9 + 51-67-2 + 868-57-5 + 23950-04-1 + 13231-81-7 + 79491-14-8 + 83647-42-1 + 20282-39-7
反应条件:1.1 Reagents: Sodium Periodate Solvents: Water; 10 Min,Rt2.1 Reagents: Potassium Carbonate Catalysts: Tetrabutylammonium Bromide Solvents: Acetonitrile; 17 H,65 °C3.1 Reagents: Sodium Borohydride Solvents: Methanol; 20 Min,0 °C3.2 Reagents: Sodium Chloride Solvents: Water; 2 Min4.1 Reagents: 1-Ethyl-3-(3′-Dimethylaminopropyl)Carbodiimide Solvents: Dichloromethane; 1 H,Rt4.2 Catalysts: 4-(Dimethylamino)Pyridine; 24 H,Rt5.1 300 - 900 °C
标题:Synthesis And Pyrolysis Of Two Novel Pyrrole Ester Flavor Precursors
作者:Fan,Wenpeng; Et Al
参考文献:Journal Of Heterocyclic Chemistry 日期:2022 卷标:59(8) 页码:1397-1406]
66-84-2 = 934-60-1 + 116-53-0 + 4518-10-9 + 51-67-2 + 868-57-5 + 23950-04-1 + 13231-81-7 + 79491-14-8 + 83647-42-1 + 20282-39-7
反应条件:1.1 Reagents: Sodium Bicarbonate Solvents: Water; 24 H,Rt2.1 Reagents: Sodium Periodate Solvents: Water; 10 Min,Rt3.1 Reagents: Potassium Carbonate Catalysts: Tetrabutylammonium Bromide Solvents: Acetonitrile; 17 H,65 °C4.1 Reagents: Sodium Borohydride Solvents: Methanol; 20 Min,0 °C4.2 Reagents: Sodium Chloride Solvents: Water; 2 Min5.1 Reagents: 1-Ethyl-3-(3′-Dimethylaminopropyl)Carbodiimide Solvents: Dichloromethane; 1 H,Rt5.2 Catalysts: 4-(Dimethylamino)Pyridine; 24 H,Rt6.1 300 - 900 °C
标题:Synthesis And Pyrolysis Of Two Novel Pyrrole Ester Flavor Precursors
作者:Fan,Wenpeng; Et Al
参考文献:Journal Of Heterocyclic Chemistry 日期:2022 卷标:59(8) 页码:1397-1406
2,6-二甲基吡啶置于potassium Permanganate体系中,用 重水 作为反应溶剂,化学反应 5.0H,以75%的收率获得产物6-甲基-2-吡啶甲酸
参考文献:一种多取代吡啶类医药中间体及其合成方法
标题:一种多取代吡啶类医药中间体及其合成方法
摘要:本发明属于医药中间体技术领域,具体为一种多取代吡啶类医药中间体及其合成方法.多取代吡啶类医药中间体是许多药物合成的关键中间体,市场潜力巨大.本发明合成路线简单,起始原料简单易得,价格便宜,对于吡啶类中间体的合成,吡啶类药物的开发以及新型药物的研发具有重大意义.
海关参考信息
- 2905110000-甲醇
2912110000-甲醛
2915110000-甲酸
2933310010-吡啶 - 💡 提示：海关信息按照顺序优先匹配，如需确认的海关信息，请参考相关资料。
- 详情请参考：📖 海关编码查询和海关进出口税则
专利信息
专利号:US-2003083352-A1
优先权日:2000-07-31
标 题 :Synthesis of imidazole intermediates
发明人：HELAL CHRISTOPHER J
权利人:PFIZER
摘要:The invention provides a method for synthesis of compounds of formula n n n wherein R 1 and R 19 are as defined. Compounds of formula 12 are useful as intermediates for synthesizing compounds having pharmacological activity inhibiting cdk5, cdk2, and GSK-3.
专利号:US-9475814-B2
优先权日:2011-10-03
标题:Chiral N-acyl-5,6,7(8-substituted)-tetrahydro-[1,2,4]triazolo[4,3-a]pyrazines as selective NK-3 receptor antagonists, pharmaceutical composition, methods for use in NK-3 receptor mediated disorders and chiral synthesis thereof
发明人：HOVEYDA HAMID R; DUTHEUIL GUILLAUME; FRASER GRAEME L; ROY MARIE-ODILE; EL BOUSMAQUI MOHAMED; BATT FREDERIC
权利人:EUROSCREEN SA
摘要:The present invention relates to novel compounds of Formula I and their use in therapeutic treatments. The invention further relates to a novel chiral synthesis of 5,6,7,(8-substituted)-tetrahydro-[1,2,4]triazolo[4,3-a]pyrazines using N-sp3 protective groups. The invention also provides intermediates for use in the synthesis of compounds of Formula I.
专利号:US-10633365-B2
优先权日:2016-04-29
标题 :Synthesis of indazoles
发明人：THALER TOBIAS; PLATZEK JOHANNES; GUIMOND NICOLAS
权利人:Bayer Pharma AG
摘要:The present invention relates to a novel method of preparing a 2-substituted indazole of formula (I) to novel intermediate compounds, and to the use of intermediate compounds for the preparation of said 2-substituted indazole.
专利号:US-9676783-B2
优先权日:2008-10-22
标 题:Method of treatment using substituted pyrazolo[1,5-A] pyrimidine compounds
发明人：HAAS JULIA; ANDREWS STEVEN W; JIANG YUTONG; ZHANG GAN
权利人:ARRAY BIOPHARMA INC
摘要:Compounds useful in the synthesis of compounds for treating pain, cancer, inflammation, neurodegenerative disease or Typanosoma cruzi infection in a mammal.
专利号:US-5169935-A
优先权日:1990-06-20
标 题:Method of making peptides
发明人：HOEGER CARL A; THEOBALD PAULA G; PORTER JOHN S; RIVIER JEAN E F
权利人:SALK INST FOR BIOLOGICAL STUDI
摘要:Methods for making peptides of a suitable length for solid phase synthesis, which peptides include in their sequence a pair of residues of a different character which have acylated side chains and a residue which has an N-alkylated side chain. A peptide intermediate is constructed on the resin using commercially available starting materials. The N-terminus can be acylated by removing the alpha -amino protecting group and acylating under standard conditions. First primary amino protecting groups included in those residues to be acylated are removed, and acylation is effected, preferably by using a carboxypyridine or a similar heterocyclic acylating agent. Following such side chain acylation, a second protecting group included in the residue to be N-alkylated is removed, and the N-alkylation reaction is carried out while the peptide remains on the resin using a borohydride and an appropriate aldehyde or ketone. Following cleavage from the resin and removal of any protecting groups still remaining, the peptide is appropriately purified, thus requiring only a single purification to be carried out while forming a synthetic peptide including residues for which the modified amino acids are not readily commercially available.
专利号:US-4224330-A
优先权日:1979-09-13
标题 :Esters and thiolesters of benzothienyl acids
发明人：HENRICK CLIVE A; LABOVITZ JEFFREY N; LEIPPE MICHAEL M; WOO SAM L
权利人:ZOECON CORP
摘要:Esters and thiolesters of benzothienyl acids, intermediates thereof, synthesis thereof, and the use thereof for the control of pests.
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供应商参考报价(招募中)
品牌试剂参考报价(招募中)
📌 第三方产品分析报告
主要参考文献
[参考文献]: Rong Gao, Et Al. Synthesis Of Benzoxazolylpyridine Nickel Complexes And Their Efficient Dimerization Of Ethylene To Alpha-Butene. Dalton Trans. 2008 Nov 7:(41):5645-51.合成参考文献
摘要:Vicens, L.; Borrell, M.; Costas, M., Science of Synthesis: Catalytic Oxidation in Organic Synthesis, (2017) 1, 135.
摘要:F. Holmes and W. R. C. Crimmin, J. Chem. Soc. 1955, 1175.
摘要:G. Anderegg. Helv. Chim. Acta 43, 414 (1960).
📝 需求与反馈
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