氯丁烷 在 铜,Sodium Sulfite体系中,用 乙醇,水作为反应溶剂,反应 40.0H,以65.2%的收率获得1-Butanesulfonic Acid Sodium Salt 参考文献:Preparation Of Sodium Sulfonates Using By Copper As Catalyst 标题:Preparation Of Sodium Sulfonates Using By Copper As Catalyst 摘要:通过斯特雷克反应制备了钠烷基磺酸盐.研究了从二氯乙烷和亚硫酸钠合成氯乙基磺酸钠的不同催化剂,发现铜是一种高效的催化剂,产率为81%.反应条件也经过优化,使该路线在大规模工业生产中更具竞争力和适用性.此外,还通过斯特雷克反应在铜催化下获得了一些其他的磺酸盐. Doi:10.14233/Ajchem.2014.16579
专利号:US-2012190064-A1 优先权日:2004-10-01 标题 :Feeding buffers, systems, and methods for in vitro synthesis of biomolecules 发明人:KUDLICKI WIESLAW ANTONI; KEPPETIPOLA SHIRANTHI; FLETCHER JULIA; GETBEHEAD ASHLEY ELAINE; KATZEN FEDERICO; VOZZA-BROWN LAURA 权利人:KUDLICKI WIESLAW ANTONI; KEPPETIPOLA SHIRANTHI; FLETCHER JULIA; GETBEHEAD ASHLEY ELAINE; KATZEN FEDERICO; VOZZA-BROWN LAURA; LIFE TECHNOLOGIES CORP 摘要:Compositions, methods and kits for in vitro systems for synthesis of biomolecules such as polypeptides, are provided herein. Cell extracts that provide enhanced yields of soluble proteins using in vitro protein synthesis methods are provided. The invention also includes methods for producing high yields of proteins by the addition of a feeding solution that includes amino acids and an energy source to an ongoing in vitro synthesis system. The invention also includes methods of using a high-yield in vitro synthesis system to produce large quantities of proteins with incorporated labeled amino acids for analysis by methods such as by NMR. The invention further includes vectors for enhanced production of proteins from nucleic acid templates using in vitro synthesis systems.
专利号:RU-2205178-C2 优先权日:1997-05-17 标 题 :Method of synthesis of 1-substituted 3-hydroxymethyl-4-(4- fluorophenyl)piperidine, method of synthesis of (-)-trans-4-(4-fluorophenyl)-3-[3,4-methylenedioxy)phenoxy]methylpiperidine
专利号:US-2009209032-A1 优先权日:2004-10-01 标 题 :Feeding buffers, systems, and methods for in vitro synthesis of biomolecules
专利号:EP-1848812-A2 优先权日:2004-10-01 标题:Feeding buffers, systems, and methods for in vitro synthesis of biomolecules
专利号:US-2006110788-A1 优先权日:2004-10-01 标题 :Feeding buffers, systems, and methods for in vitro synthesis of biomolecules
专利号:WO-2006039622-A2 优先权日:2004-10-01 标 题 :Feeding buffers, systems, and methods for in vitro synthesis of biomolecules
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合成参考文献
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