CAS: 18643-08-8; Dimethyloctadecylchlorosilane

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66604-31-7 38051-57-9 18162-84-0

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Ethoxy(octadecyldimethyl)Silane置于氯化亚砜,四丁基氟化铵,N,N-二甲基甲酰胺体系中,用 四氢呋喃,正庚烷,二氯甲烷 用作溶剂,化学反应 26.0H,反应生成二甲基十八烷基氯硅烷
参考文献:烃类可溶性可循环硅烷化试剂和纯化助剂
标题:烃类可溶性可循环硅烷化试剂和纯化助剂
摘要:描述了使用庚烷相选择性溶解的十八烷基二甲基甲硅烷基基团以促进分离和甲硅烷基试剂再生的方法.这些结果表明,由这些基团保护的醇和炔烃在烃溶剂中是相选择地可溶的.在热定型环己烷/ Dmf系统中,> 96%的甲硅烷基化醇都在环己烷相中,从而可以通过简单的液/液萃取来纯化这些化合物.描述了这些甲硅烷基化剂在格利雅(grignard)合成和sonogashira反应中的应用.
Doi:10.1021/acs.Orglett.6B00263

专利信息

专利号:US-2023323449-A1
优先权日:2021-12-17
标 题:Compositions and methods for detection of variants
发明人：GANTT RICHARD; ARNESON ADRIANA
权利人:TWIST BIOSCIENCE CORP
摘要:Testing the many hypotheses from genomics and systems biology experiments demands accurate and cost-effective gene and genome synthesis. Here we describe a microchip-based technology for multiplex gene synthesis. Pools of thousands of ‘construction’ oligonucleotides and tagged complementary ‘selection’ oligonucleotides are synthesized on photo-programmable microfluidic chips, released, amplified and selected by hybridization to reduce synthesis errors ninefold. A one-step polymerase assembly multiplexing reaction assembles these into multiple genes. This technology enabled us to synthesize all 21 genes that encode the proteins of the Escherichia coli 30S ribosomal subunit, and to optimize their translation efficiency in vitro through alteration of codon bias. This is a significant step towards the synthesis of ribosomes in vitro and should have utility for synthetic biology in general.

专利号:US-9981239-B2
优先权日:2015-04-21
标题:Devices and methods for oligonucleic acid library synthesis
发明人：BANYAI WILLIAM; PECK BILL JAMES; FERNANDEZ ANDRES; CHEN SIYUAN; INDERMUHLE PIERRE; MARSH EUGENE P
权利人:TWIST BIOSCIENCE CORP
摘要:Devices and methods for de novo synthesis of large and highly accurate libraries of oligonucleic acids are provided herein. Devices include structures having a main channel and microchannels, where the microchannels have a high surface area to volume ratio. Devices disclosed herein provide for de novo synthesis of oligonucleic acids having a low error rate.

专利号:US-11512347-B2
优先权日:2015-09-22
标 题 :Flexible substrates for nucleic acid synthesis
发明人：PECK BILL JAMES
权利人:TWIST BIOSCIENCE CORP
摘要:Provided herein are compositions, devices, systems and methods for the generation and use of biomolecule-based information for storage. Further described herein are highly efficient methods for long term data storage with 100% accuracy in the retention of information. Additionally, devices described herein for de novo synthesis of oligonucleic acids encoding information related to the original source information may have a flexible material for oligonucleic acids extension.

专利号:US-2006000773-A1
优先权日:2003-03-07
标题:Process for the synthesis of a chromatographic phase
发明人：GLENNON JEREMY; HEALY LIAM
权利人:GLENNON JEREMY; HEALY LIAM
摘要:A process for the synthesis, delivery or deposition or localisation of a chromatographic phase, especially for chromatographic separation or solid phase extraction, comprises introducing a chemical moiety to a support using a supercritical fluid such as supercritical carbon dioxide.

专利号:US-11033507-B2
优先权日:2013-12-19
标 题 :Method of synthesis of silica vesicles and use thereof
发明人：YU CHENGZHONG; MITTER NEENA; ZHANG JUN
权利人:UNIV QUEENSLAND
摘要:The invention relates, in part, to a method of producing silica vesicles including under controlled conditions to thereby heavily influence the morphology and characteristics of the vesicles. The vesicles are shown to be effective as delivery agents for chemical and biological agents. They are also shown to be useful in methods of treatment and as components of an immunogenic composition.

专利号:US-4919804-A
优先权日:1988-03-01
标 题:Ultrasound driven synthesis of reversed and normal phase stationary phases for liquid chromatography
发明人：DORSEY JOHN G; SENTELL KAREN B; BARNES KAREN W
权利人:UNIV FLORIDA
摘要:In a method for producing a reversed phase bonded metal oxide by reacting the metal oxide with a reactive silane, the improvement comprising conducting the reaction in the presence of ultrasonic waves.