合成目标产物 4-(1-Adamantyl)Phenol 主要起始原料 1-Bromoadamantane And Phenol
(文献来源)合成步骤主要原料 1-Bromoadamantane 和 Phenol
1-溴金刚烷置于palladium 10% On Activated Carbon,三溴化硼,Potassium Carbonate体系中,用 二氯甲烷 用作溶剂,化学反应 22.0H,反应生成4-(1-金刚烷基)苯酚 参考文献:페녹시아크릴 유도체 및 이의 용도 标题:페녹시아크릴 유도체 및 이의 용도 摘要:这项发明涉及苯氧基乙酰诱导体化合物及其作为有效成分包含在非酒精性脂肪肝预防或治疗药物组合物中的药学组合物.根据本发明,由化合物具有出色的srebp-1C活性抑制和fas表达抑制能力,可以预期将其作为预防,改善或治疗非酒精性脂肪肝的药学组合物或功能性食品组合物的活性成分得到有益利用.
专利号:US-10843990-B2 优先权日:2018-02-09 标题 :Processes for preparing calix[4]arenes from calix[8]arenes 发明人:HAASE CORNELIUS; HISCOCK JEFF; ATWOOD PHILIP DAVID 权利人:SI GROUP INC 摘要:This invention relates to a one-pot synthesis of a high-purity calix[4]arene compound by reacting a phenolic compound and an aldehyde in the presence of at least one nitrogen-containing base as a catalyst to form the calix[8]arene compound, and cleaving the calix[8]arene compound into a high-purity calix[4]arene compound, directly, without carrying out a purification step before the cleaving step. The invention also relates to an improved conversion of a calix[8]arene compound to a calix[4]arene compound, by cleaving a calix[8]arene compound in a glycol ether solvent having a boiling point of at least about 200° C., to result in a high-purity calix[4]arene compound, without using an antisolvent.
专利号:CN-114181091-B 优先权日:2021-12-27 标 题:A kind of synthesis process of adamantane triphenylamine
专利号:CN-114181091-A 优先权日:2021-12-27 标题 :A kind of synthesis technique of adamantane triphenylamine