CAS: 145022-48-6; 1-Butyl-3-Methylimidazoliumtrifluoromethanesulfonate

N-丁基咪唑,三氟甲烷磺酸乙酯 反应 21.0H,以100%的收率获得1-丁基-3-甲基咪唑三氟甲烷磺酸酯
参考文献:三氟甲磺酸盐阴离子液体的简便合成及其性质
标题:三氟甲磺酸盐阴离子液体的简便合成及其性质
摘要:通过有机碱(胺,膦或杂环化合物)与三氟甲磺酸甲酯和乙酯(三氟甲磺酸甲酯和乙酯)的直接烷基化,开发了一种无溶剂和无卤素的高纯度三氟甲磺酸盐离子液体合成方法.在通过本发明的方法制备三氟甲磺酸甲酯和乙酯中,廉价且无毒的碳酸二甲酯和碳酸二乙酯用作甲基和乙基的来源.确定并讨论了含有三氟甲磺酸根阴离子的离子液体的性质.
Doi:10.3390/molecules17055319

专利信息

专利号:US-9267213-B1
优先权日:2005-03-25
标题:Electrochemical deblocking solution for electrochemical oligomer synthesis on an electrode array
发明人：MAURER KARL; COOPER JOHN J
权利人:CUSTOMARRAY INC
摘要:There is disclosed an electrochemical deblocking solution for use on an electrode microarray. There is further disclosed a method for electrochemical synthesis on an electrode array using the electrochemical deblocking solution. The solution and method are for removing acid-labile protecting groups for synthesis of oligonucleotides, peptides, small molecules, or polymers on a microarray of electrodes while substantially improving isolation of deblocking to active electrodes. The method comprises applying a voltage or a current to at least one electrode of an array of electrodes. The array of electrodes is covered by the electrochemical deblocking solution.

专利号:US-10407676-B2
优先权日:2014-12-09
标题 :High efficiency, small volume nucleic acid synthesis
发明人：POEHMERER THOMAS; KUHN PHILLIP; NOTKA FRANK; ZEIDLER ANDREAS; HEIL KORBINIAN; TREFZER AXEL; FONNUM GEIR; KATZEN FEDERICO; ANDERSSON KRISTIAN
权利人:LIFE TECHNOLOGIES CORP; THERMO FISHER SCIENT GENEART GMBH; LIFE TECH AS
摘要:The disclosure generally relates to compositions and methods for the production of nucleic acid molecules. In some aspects, the invention allows for the microscale generation of nucleic acid molecules, optionally followed by assembly of these nucleic acid molecules into larger molecules. In some aspects, the invention allows for efficient production of nucleic acid molecules (e.g., large nucleic acid molecules such as genomes).

专利号:MX-2007011815-A
优先权日:2005-03-25
标题 :ELECTROCHEMICAL UNLOCK SOLUTION FOR ELECTROCHEMICAL SYNTHESIS OF OLIGOMEROS IN AN ARRANGEMENT OF ELECTRODES.

专利号:RU-2007139631-A
优先权日:2005-03-25
标题 :SOLUTION FOR ELECTROCHEMICAL DEPARTMENT IN ELECTROCHEMICAL SYNTHESIS OF OLIGOMERS ON THE ELECTRODE MATRIX