CAS: 16282-16-9; 1,2-Diphenylbutan-1-One

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2-苯基丁酸置于正丁基锂,硫酸体系中,用 四氢呋喃,正己烷 用作溶剂,化学反应 56.67H,反应生成2-苯基丁酰苯
参考文献:Continuous Flow-Processing Of Organometallic Reagents Using An Advanced Peristaltic Pumping System And The Telescoped Flow Synthesis Of (E/z)-Tamoxifen
标题:Continuous Flow-Processing Of Organometallic Reagents Using An Advanced Peristaltic Pumping System And The Telescoped Flow Synthesis Of (E/z)-Tamoxifen
摘要:A New Enabling Technology For The Pumping Of Organometallic Reagents Such As N-Butyllithium,Grignard Reagents,And Dibal-H Is Reported,Which Utilises A Newly Developed,Chemically Resistant,Peristaltic Pumping System. Several Representative Examples Of Its Use In Common Transformations Using These Reagents,Including Metal-Halogen Exchange,Addition,Addition-Elimination,Conjugate Addition,And Partial Reduction,Are Reported Along With Examples Of Telescoping Of The Anionic Reaction Products. This Platform Allows For Truly Continuous Pumping Of These Highly Reactive Substances (And Examples Are Demonstrated Over Periods Of Several Hours) To Generate Multigram Quantities Of Products. This Work Culminates In An Approach To The Telescoped Synthesis Of (E/z)-Tamoxifen Using Continuous-Flow Organometallic Reagent-Mediated Transformations.
Doi:10.1021/op4001548

专利信息

专利号:US-2009227701-A1
优先权日:2004-08-19
标题:Water-soluble, radiation-curable products and use thereof
发明人：KRUEGER CHRISTIAN; BRUCHMANN BERND; HEES ULRIKE; KLUGE MICHAEL; DIELEMAN CEDRIC; WEISER JUERGEN
权利人:BASF AG
摘要:Water soluble radiation curable products (A) obtainable by mixingn mixing with or without reaction of at least one hyperbranched polyurethane (a) with at least one photoinitiator (b) or by synthesis of at least one hyperbranched polyurethane (a) in the presence of at least one photoinitiator (b),n nare used to produce aqueous inks for the ink jet process.

专利号:EP-1565563-B1
优先权日:2002-11-22
标题:Enzymatic synthesis of polyol acrylates
发明人：PAULUS WOLFGANG; HAUER BERNHARD; HAERING DIETMAR; DIETSCHE FRANK
权利人:BASF SE

专利号:US-2006030013-A1
优先权日:2002-11-22
标题 :Enzymatic synthesis of polyol acrylates

专利号:JP-2006506993-A
优先权日:2002-11-22
标 题:Enzymatic synthesis of acrylic polyols.

专利号:US-2011123721-A1
优先权日:2002-11-22
标 题 :Enzymatic synthesis of polyol acrylates

专利号:EP-1781743-B1
优先权日:2004-08-19
标 题:Water-soluble products hardening with radiation and use thereof
发明人：KRUEGER CHRISTIAN; BRUCHMANN BERND; DIELEMAN CEDRIC; KLUGE MICHAEL
权利人:BASF AG
摘要:Water soluble radiation curable products (A) obtainable by mixing with or without reaction of at least one hyperbranched polyurethane (a) with at least one compound having at least one ethylenic double bond per molecule (b) or by synthesis of at least one hyperbranched polyurethane (a) in the presence of at least one compound having at least one ethylenic double bond per molecule (b) are used to produce aqueous inks for the ink jet process.