丙烯酸,3-氯丙基三甲氧基硅烷置于四丁基溴化铵 吩噻嗪,2,6-二叔丁基-4-甲基苯酚,Sodium Methylate体系中,用 甲醇,Xylene 作为反应溶剂,化学反应 5.0H,反应生成 3-三甲氧基硅烷丙烯酸丙脂 参考文献: Process For Preparing An Acryloyloxysilane[fr] Procédé De Synthèse D'Un Acryloyloxysilane 标题: Process For Preparing An Acryloyloxysilane[fr] Procédé De Synthèse D'Un Acryloyloxysilane
专利号:WO-2023102600-A1 优先权日:2021-12-06 标题:Synthesis of amphiphilic block copolymers and polymeric nanofibers produced therefrom 发明人:ZETTERLUND PER B; ISHIZUKA FUMI; KIM HYUN JIN; CHATANI SHUNSUKE; NIINO HIROSHI 权利人:NEWSOUTH INNOVATIONS PTY LTD 摘要:The present disclosure relates to the field of synthesis of block copolymers, and polymeric nanofibers having a core-shell morphology produced therefrom. The present disclosure relates to the field of synthesis of block copolymers where one block is more hydrophobic than the other block and is a different composition. The disclosure also relates to uses of these polymeric nanofibers in various applications, such as reinforcing a polymeric matrix and for coatings applications.
专利号:US-6512081-B1 优先权日:1997-07-21 标题:Synthesis of dithioester chain transfer agents and use of bis(thioacyl) disulfides or dithioesters as chain transfer agents 发明人:RIZZARDO ENZIO; THANG SAN HOA; MOAD GRAEME 权利人:E I DUPONT NEMOURS AND COMPANY; COMMW SCIENT IND RES ORG 摘要:This invention relates to the synthesis of dithiocarboxylic acid esters by reaction of bis(thioacyl) disulphides, thioacetals or vinylidane bis(thioether) with free-radicals (optionally in the presence of monomers). The invention also relates to processes for the synthesis of polymers utilising these dithioesters as polymerisation regulators (chain transfer agents) or to the use of bis(thioacyl) disulphides to generate dithioester chain transfer agents in situ.
专利号:US-6100350-A 优先权日:1996-02-23 标题 :Branched polymer synthesis 发明人:WILCZEK LECH; MCCORD ELIZABETH FORRESTER 权利人:DU PONT; COMMW SCIENT IND RES ORG 摘要:PCT No. PCT/US97/02913 Sec. 371 Date Aug. 19, 1998 Sec. 102(e) Date Aug. 19, 1998 PCT Filed Feb. 18, 1997 PCT Pub. No. WO97/31031 PCT Pub. Date Aug. 28, 1997This invention relates to a process for the synthesis of addition polymers containing branches upon branches and having a polymerizable olefin end group by a convenient one-pot copolymerization of selected vinyl monomers with chain polymerization initiators and a method to provide olefin end groups by chain transfer or termination agents; and polymers produced thereby.
专利号:US-6291620-B1 优先权日:1994-11-09 标 题:Polymer synthesis 发明人:MOAD GRAEME; MOAD CATHERINE LOUISE; KRSTINA JULIA; RIZZARDO EZIO; DARLING THOMAS ROBERT; BERGE CHARLES THOMAS 权利人:DU PONT; COMMW SCIENT IND RES ORG 摘要:Process for the synthesis of block polymers, homopolymers and copolymers of narrow polydispersity having formula (1) by contacting selected vinyl monomer(s), vinyl-terminated compound(s) and free radicals in which effective control of production of polymer is achieved by controlling the mole ratio of vinyl monomer(s), vinyl-terminated compound(s) and free radicals relative to one another; and polymers produced thereby
专利号:US-2024010511-A1 优先权日:2019-05-02 标 题 :Methods and compositions for synthesis of phosphor and its incorporation in a polymer matrix for light conversion 发明人:SAHI SUNIL 权利人:SOLGO INC; SOLGRO INC 摘要:The invention relates to methods and compositions for synthesizing a phosphor and preparing a surface-modified phosphor comprising a phosphor, a silica, and a silane, and articles comprising same. The invention also relates to a method of dispersion of the disclosed surface-modified phosphor with a blue emitting agent in a polymer matrix and uses thereof.
专利号:US-2023212107-A1 优先权日:2021-12-30 标 题:Synthesis of para-alkylated syringyl (meth)acrylate derivatives and photopolymerizable compositions for additive manufacturing in dental applications 发明人:CHOUDHARY UMESH UPENDRA; SU JESSICA KALAY 权利人:ALIGN TECHNOLOGY INC 摘要:The present disclosure provides polymerizable monomers which may be used as reactive diluents in additive manufacturing. The polymerizable monomers may have low vapor pressures and may be compatible with a range of low glass transition temperature oligomers.
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合成参考文献
参考文献:10.1007/s10544-012-9730-z 摘要:Corbin EA, Millet LJ, Pikul JH, Johnson CL, Georgiadis JG, King WP, Bashir R. Micromechanical properties of hydrogels measured with MEMS resonant sensors. Biomed Microdevices. 2013 Apr;15(2):311–9. doi: 10.1007/s10544-012-9730-z. 参考文献:10.1016/j.jdent.2005.09.007 摘要:Matinlinna JP, Lassila LV, Vallittu PK. The effect of a novel silane blend system on resin bond strength to silica-coated Ti substrate. J Dent. 2006 Aug;34(7):436–43. doi: 10.1016/j.jdent.2005.09.007.