25322-68-3 + 80-05-7 = 25322-68-3 + 80-05-7 反应条件:1.1 Solvents: 1-Methoxy-2-Propanol; Rt -> 70 °C1.2 Catalysts: Boron Trifluoride Etherate; 3 H,70 °C; 70 °C; 70 °C -> 95 °C; 9 H,95 °C; 95 °C -> 60 °C 标题:Preliminary Results On Preparation And Performance Of A Self-Emulsifying Waterborne Epoxy Curing Agent At Room Temperature 作者:Pi,Zhenzhen; Deng,Changyu; Pan,Hongmei; Pei,Kemei 参考文献:Polymers (Basel 日期:2023 卷标:15(7)]
25322-68-3 + 80-05-7 = 25322-68-3 + 80-05-7 反应条件:1.1 4 H,120 °C 标题:Preparation Of High-Strength,Water-Resistant Starch Adhesive And Its Bonding Mechanism To Cotton Stalk 作者:Li,Kui; Zuo,Yingfeng; Zheng,Long; Wang,Huifen; Wu,Yiqiang 参考文献:Industrial Crops And Products 日期:2023 卷标:194]
25322-68-3 + 80-05-7 = 25322-68-3 + 80-05-7 [标题:Reaction Conditions 标题:Preparation Of Epoxy Resin Emulsifiers With Different Structures And A Comparative Study Of Their Properties 作者:Zhang,Yancheng; Huang,He 参考文献:Chemistryselect 日期:2022 卷标:7(34)
专利信息
专利号:US-2025051339-A1 优先权日:2021-12-15 标题:Methods for the synthesis of complement factor d inhibitors 发明人:HASHIMOTO AKIHIRO 权利人:ALEXION PHARMA INC 摘要:The present disclosure provides methods for the synthesis of complement factor D inhibitors and intermediates thereof. The methods involve subjecting an intermediate in the synthesis of a complement factor D inhibitor to a t-butyl ester deprotection reaction using a weak base.
专利号:US-7527712-B2 优先权日:2002-07-23 标 题 :Method for the continuous purification by distillation of the solvent methanol, used in the synthesis of propylene oxide 发明人:BASSLER PETER; GOEBBEL HANS-GEORG; TELES JOAQUIM HENRIQUE; RUDOLF PETER 权利人:BASF AG 摘要:Process for the continuously operated purification by distillation of the methanol used as solvent in the synthesis of propylene oxide by reaction of a hydroperoxide with propylene, with the methoxypropanols being separated off simultaneously, wherein the solvent mixture obtained in the synthesis is separated in a dividing wall column into a low-boiling fraction including methanol, an intermediate-boiling fraction containing the methoxypropanols as azeotrope with water and a high-boiling fraction including water and propylene glycol.
专利号:US-7332634-B2 优先权日:2002-07-23 标题:Method for the continuous purification by distillation of 1,2-propylene glycol that accumulates during the synthesis of propylene oxide without coupling products 发明人:BASSLER PETER; GOEBBEL HANS-GEORG; TELES JOAQUIM HENRIQUE; RUDOLF PETER 权利人:BASF AG 摘要:The invention relates to a continuously operated process for the purification by distillation of the 1,2-propylene glycol formed as by-product in the synthesis of propylene oxide, wherein the mixture formed in the synthesis which contains the 1,2-propylene glycol is separated in a dividing wall column into low-, intermediate- and high-boiling fractions and the 1,2-propylene glycol is taken off as intermediate boiler at the side offtake of the column.
专利号:US-9040739-B2 优先权日:2012-06-18 标题 :Catalyst and method for synthesis of lactic acid and its derivatives 发明人:ZHOU XIAOPING; BI RUI 权利人:ZHOU XIAOPING; BI RUI; MICROVAST POWER SYSTEMS CO LTD 摘要:A catalyst for synthesis of lactic acid and it derivatives is provided. The catalyst includes SnY2.mH 2 O and at least one of NH 4 X or quaternary ammonium salts, wherein X and Y are selected from F—, Cl—, Br—, I—, CH 3 SO 3 —, C 6 H 5 SO 3 —, CH 3 C 6 H 4 SO 3 — or CN—, m represents an integer of 1 to 15. A method for synthesis of lactic acid and it derivatives with the above catalyst is also provided. By using the above catalyst and method, it is capable of converting carbohydrate-containing raw material to lactic acid and its derivatives directly in a more efficient and economical way.
专利号:WO-9517903-A1 优先权日:1993-12-28 标 题:Modular design and synthesis of oxazolone-derived molecules 发明人:HOGAN JOSEPH C JR; CASEBIER DAVID; FURTH PAUL; TU CHENG 权利人:ARQULE PARTNERS L P; HOGAN JOSEPH C JR; CASEBIER DAVID; FURTH PAUL; TU CHENG 摘要:The design and synthesis of novel oxazolone-derived molecular modules and the use of the modules in the construction of new molecules and fabricated materials is disclosed. The new molecules and fabricated materials are molecular recognition agents useful in the design and synthesis of drugs, and have applications in separations and materials science.
专利号:WO-2024105700-A1 优先权日:2022-11-18 标 题:A method for the synthesis of anthranilic amide compounds and intermediates thereof 发明人:MALVIYA NITIN; MAL SANJIB; KLAUSENER ALEXANDER G M 权利人:PI INDUSTRIES LTD 摘要:The present invention discloses a method for the synthesis of a compound of formula (V) or a salt thereof, wherein, R, R1, R2, R3, R4a and R4b are as defined in the detailed description. The method further comprises the synthesis of an anthranilic diamide compound of formula (Z).
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合成参考文献
参考文献:10.1007/s00216-010-3487-0 摘要:Tomicic C, Berode M. Sensitive headspace gas chromatography analysis of free and conjugated 1-methoxy-2-propanol in urine. Analytical and Bioanalytical Chemistry. 2010 Feb 13;396(7):2709–14. doi: 10.1007/s00216-010-3487-0. 参考文献:10.1007/s11239-010-0450-z 摘要:Hua X, Liu P, Gao YH, Tan KB, Zhou LN, Liu Z, Li X, Zhou SW, Gao YJ. Construction of thrombus-targeted microbubbles carrying tissue plasminogen activator and their in vitro thrombolysis efficacy: a primary research. J Thromb Thrombolysis. 2010 Jul;30(1):29–35. doi: 10.1007/s11239-010-0450-z. 参考文献:10.1007/s10384-011-0062-y 摘要:Kobayashi T, Gibbon L, Mito T, Shiraishi A, Uno T, Ohashi Y. Efficacy of commercial soft contact lens disinfectant solutions against Acanthamoeba. Japanese Journal of Ophthalmology. 2011 Sep 01;55(5):547–57. doi: 10.1007/s10384-011-0062-y. 参考文献:10.1208/s12249-011-9661-7 摘要:Badıllı U, Sen T, Tarımcı N. Microparticulate based topical delivery system of clobetasol propionate. AAPS PharmSciTech. 2011 Sep;12(3):949–57. 摘要:Mbah CJ. Physicochemical properties of valsartan and the effect of ethyl alcohol, propylene glycol and pH on its solubility. Pharmazie. 2005 Nov;60(11):849–50.