131-70-4 = 85-68-7 反应条件:1.1 Reagents: Potassium Carbonate Solvents: Acetone; 3 H,Reflux 标题:Revised Structure For Spatozoate,A Metabolite Of Spatoglossum Variabile 作者:Cheng,Kur-Ta; Et Al 参考文献:Indian Journal Of Chemistry 日期:2003 卷标:(5) 页码:1190-1192]
58902-58-2 = 85-68-7 反应条件:1.1 Reagents: Sodium Bicarbonate Catalysts: Triethylamine 标题:Process And Triethylamine Catalyst For The Production Of Benzyl Butyl Phthalate By The Esterification Of Benzyl Chloride With Butyl Monosodium Phthalate In The Presence Of Sodium Bicarbonate 参考文献:Russian Federation]
71-36-3 = 85-68-7 反应条件:1.1 Reagents: Sulfuric Acid; 15 Min,Reflux2.1 Reagents: Potassium Carbonate Solvents: Acetone; 3 H,Reflux 标题:Revised Structure For Spatozoate,A Metabolite Of Spatoglossum Variabile 作者:Cheng,Kur-Ta; Et Al 参考文献:Indian Journal Of Chemistry 日期:2003 卷标:(5) 页码:1190-1192
苯酐置于乙醇体系中,化学反应生成 邻苯二甲酸丁苄酯 参考文献:Butyl Esters Of Phthalic Acid 标题:Butyl Esters Of Phthalic Acid
专利号:US-11780952-B2 优先权日:2016-08-08 标题:Process for the synthesis of silylated polyurethanes and silylated polyurethane composition 发明人:LAFERTE OLIVIER 权利人:BOSTIK SA 摘要:The present invention provides a process for the synthesis of silylated polyurethanes, comprising three sequential steps, a step (i) of preparing NCO-terminated polyurethane, a step (ii) of partial grafting of the NCO functions with silane functions and a step (iii) of total grafting of the residual NCO functions with functions that react with the NCO functions by means of polyfunctional compounds. The present invention also provides a silylated polyurethane composition that can be obtained by means of the process according to the invention, an adhesive composition comprising said silylated polyurethane composition and a self-adhesive item obtained from the adhesive composition according to the invention.
专利号:US-2025192223-A1 优先权日:2022-03-07 标 题:Synthesis of al-doped llzo thin-tape electrolytes for solid-state batteries using flame-assisted spray pyrolysis 发明人:DENG SILI; MULDOON VALERIE L; ZHANG JIANAN 权利人:MASSACHUSETTS INST TECHNOLOGY 摘要:A method of synthesis of aluminum-doped Li 6.25 Al 0.25 La 3 Zr 2 O 12 (Al-LLZO) can include preparing a precursor solution by dissolving lithium nitrate, aluminum nitrate, zirconium (IV) oxynitrate, and lanthanum nitrate in stoichiometric amounts according to the composition Li 6.25 Al 0.25 La 3 Zr 2 O 12 in water, and decomposing droplets by passing through a co-flow burner. Also disclosed is a method of produce producing a thin-tape comprising Al-LLZO.
专利号:US-11745159-B2 优先权日:2017-10-20 标题:Heated nanowells for polynucleotide synthesis 发明人:MARSH EUGENE P; INDERMUHLE PIERRE F; PECK BILL JAMES 权利人:TWIST BIOSCIENCE CORP 摘要:Defined sequence RNA synthesis by 3′→5′ direction is now well established and currently in use for synthesis and development of vast variety of therapeutic grade RNA and Si RNA etc. A number of such synthetic RNA requires a modification or labeling of 3′-end of an oligonucleotide. The synthesis of 3′-end modified RNA requiring lipophilic, long chain ligands or chromophores, using 3′→5′ synthesis methodology is challenging, requires corresponding solid support and generally results in low coupling efficiency and lower purity of the final oligonucleotide in general because of large amount of truncated sequences containing desired hydrophobic modification. We have approached this problem by developing reverse RNA monomer phosphoramidites for RNA synthesis in 5′→3′-direction. They lead to very clean oligonucleotide synthesis allowing for introduction of various modifications at the 3′-end.
专利号:US-11512347-B2 优先权日:2015-09-22 标 题 :Flexible substrates for nucleic acid synthesis 发明人:PECK BILL JAMES 权利人:TWIST BIOSCIENCE CORP 摘要:Provided herein are compositions, devices, systems and methods for the generation and use of biomolecule-based information for storage. Further described herein are highly efficient methods for long term data storage with 100% accuracy in the retention of information. Additionally, devices described herein for de novo synthesis of oligonucleic acids encoding information related to the original source information may have a flexible material for oligonucleic acids extension.
专利号:US-10987659-B1 优先权日:2020-11-05 标题 :Synthesis of TiO2/Co3O4 core-shell photocatalysts 发明人:KADI MOHAMMAD W; OUF REDA M MOHAMED 权利人:UNIV KING ABDULAZIZ 摘要:A method of synthesizing TiO 2 /Co 3 O 4 core-shell photocatalysts is provided. The method includes preparing SiO 2 hollow nanospheres via sol-gel synthesis in the presence of a triblock copolymer surfactant and a cationic surfactant; adding titanium sec-butoxide to a solution containing the SiO 2 hollow nanospheres to provide a first combined sample; calcinating the first combined sample to provide hollow mesoporous TiO 2 nanospheres; adding cobalt nitrate to a solution comprising the hollow mesoporous TiO 2 nanospheres to provide a second combined sample; and calcinating the second combined sample to provide TiO 2 /Co 3 O 4 core-shell photocatalysts. Methods of producing hydrogen by water-splitting using TiO 2 /Co 3 O 4 core-shell photocatalysts are also provided. Such methods include photodepositing platinum onto the photocatalysts during the reaction.
专利号:WO-9723519-A1 优先权日:1995-12-21 标题:Synthesis of aqueous, anionic, amino acrylate polymers 发明人:DAS SURYYA K; KILIC SONER 权利人:PPG INDUSTRIES INC 摘要:Disclosed is a method of making aqueous, anionic amino polymers in water from olefinically unsaturated monomers including amine-containing monomers, but substantially without the inclusion of acid-group containing monomers. The polymerization of the amino polymer is carried out in the presence of a carboxy functional azo initiator dissolved in water by neutralization of acid groups present on the initiator. The polymer is useful in single-package or two-package coating compositions having pH above 7.0 that may be cured with polyisocyanates or polyepoxides.
参考文献:10.1159/000088841 摘要:Chatterjee S, Mallick S, Dutta TK. Pathways in the degradation of hydrolyzed alcohols of butyl benzyl phthalate in metabolically diverse Gordonia sp. strain MTCC 4818. J Mol Microbiol Biotechnol. 2005;9(2):110–20. doi: 10.1159/000088841. 参考文献:10.1016/j.toxlet.2011.07.007 摘要:Qin XY, Zaha H, Nagano R, Yoshinaga J, Yonemoto J, Sone H. Xenoestrogens down-regulate aryl-hydrocarbon receptor nuclear translocator 2 mRNA expression in human breast cancer cells via an estrogen receptor alpha-dependent mechanism. Toxicol Lett. 2011 Oct 10;206(2):152–7. doi: 10.1016/j.toxlet.2011.07.007.