CAS: 14867-28-8; (3-Iodopropyl)Trimethoxysilane

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CAS号2530-87-2 3-氯丙基三甲氧基硅烷 | CAS号70851-51-3 N-(三甲氧基甲硅烷基丙基)咪唑 | CAS号76788-88-0 3-azidopropyl(t...

3-氯丙基三甲氧基硅烷置于potassium Iodide体系中,用 丙酮 用作溶剂,化学反应 12.0H,反应生成3-碘苯基三甲氧基硅烷
参考文献:Feiii可持续的百万分之一级催化:水中的2,3-二氢喹唑啉-4(1H)-One的一锅级联反应
标题:Feiii可持续的百万分之一级催化:水中的2,3-二氢喹唑啉-4(1H)-One的一锅级联反应
摘要:二氧化硅负载的铁络合物已被确认为合成具有医学重要性的2,3-二氢喹唑啉-4(1 H)-酮的高活性和可重复使用的催化剂.通过各种光谱分析对催化剂进行了全面表征,例如傅立叶变换红外光谱(ft-Ir),紫外可见光谱(uv-Vis),扫描电子显微镜(sem),具有能量色散x射线光谱的扫描电子显微镜( Sem-Edx),能量色散光谱(eds)映射,X射线衍射(xrd),X射线光电子能谱(xps),电子顺磁共振(epr),电感耦合等离子体原子发射光谱(icp-Aes),元素分析,Brunauer-emmett-teller(bet)等温线和热重分析(tga)分析.2,3-二氢喹唑啉-4(1H)-包括一些新的类似物已成功地以水用作溶剂以高至优异的收率(百万分之几(ppm))的fe合成了.在最佳条件下,活性催化剂具有高的周转数(ton)和周转频率(tof),分别为3,087 H和3,087 H-1.Ppm
Doi:10.1002/aoc.6116

专利信息

专利号:US-2023313255-A1
优先权日:2020-07-15
标题:Massively Parallel Enzymatic Synthesis of Polynucleotides
发明人：HORGAN ADRIAN; LACHAIZE HENRI; VERARDO DOMIANO; GODRON XAVIER
权利人:DNA SCRIPT
摘要:The invention is directed to methods and compositions for inkjet assisted synthesis of a plurality of polynucleotides at reaction sites on a substrate using template-free polymerases, such as, terminal deoxynucleotidyl transferases (TdTs). Compositions of the invention include formulations of synthesis reagents for inkjet delivery including, but not limited to, TdT coupling reaction buffers and 3′-O-protected dNTP monomers.

专利号:US-2023323449-A1
优先权日:2021-12-17
标 题:Compositions and methods for detection of variants
发明人：GANTT RICHARD; ARNESON ADRIANA
权利人:TWIST BIOSCIENCE CORP
摘要:Testing the many hypotheses from genomics and systems biology experiments demands accurate and cost-effective gene and genome synthesis. Here we describe a microchip-based technology for multiplex gene synthesis. Pools of thousands of ‘construction’ oligonucleotides and tagged complementary ‘selection’ oligonucleotides are synthesized on photo-programmable microfluidic chips, released, amplified and selected by hybridization to reduce synthesis errors ninefold. A one-step polymerase assembly multiplexing reaction assembles these into multiple genes. This technology enabled us to synthesize all 21 genes that encode the proteins of the Escherichia coli 30S ribosomal subunit, and to optimize their translation efficiency in vitro through alteration of codon bias. This is a significant step towards the synthesis of ribosomes in vitro and should have utility for synthetic biology in general.

专利号:US-9981239-B2
优先权日:2015-04-21
标题:Devices and methods for oligonucleic acid library synthesis
发明人：BANYAI WILLIAM; PECK BILL JAMES; FERNANDEZ ANDRES; CHEN SIYUAN; INDERMUHLE PIERRE; MARSH EUGENE P
权利人:TWIST BIOSCIENCE CORP
摘要:Devices and methods for de novo synthesis of large and highly accurate libraries of oligonucleic acids are provided herein. Devices include structures having a main channel and microchannels, where the microchannels have a high surface area to volume ratio. Devices disclosed herein provide for de novo synthesis of oligonucleic acids having a low error rate.

专利号:WO-2024153643-A1
优先权日:2023-01-16
标 题 :Inkjet-assisted enzymatic nucleic acid synthesis
发明人：MOGHADDAM NICOLAS; ADELIZZI BEATRICE; LOMAN TESSA; VERARDO DAMIANO; RODRIGUEZ-PINZON DANIEL; HORGAN ADRIAN
权利人:DNA SCRIPT
摘要:Methods, devices, and compositions are provided for inkjet-assisted synthesis of a plurality of polynucleotides at reaction sites on a substrate using template-free polymerases, such as, terminal deoxynucleotidyl transferases (TdTs). Compositions include printable stabile formulations of synthesis reagents for inkjet delivery including, but not limited to, template-free polymerases, divalent cations, and nucleotides.

专利号:WO-2024163733-A1
优先权日:2023-02-01
标题:Electrochemical synthesis with redox stable nucleotides
发明人：WU TIANDI; LACKEY JEREMY; LIN YANYOU; PITSCH STEFAN
权利人:TWIST BIOSCIENCE CORP
摘要:Provided herein are compositions, devices, systems and methods for constructing and storing polynucleotides encoding information with redox resistant bases. The compositions, devices, systems, and methods described herein provide for storage or synthesis of a library comprising a plurality of polynucleotides with one or more redox resistance bases. Further provided herein are methods to increase DNA synthesis yield and fidelity.

专利号:US-11512347-B2
优先权日:2015-09-22
标 题 :Flexible substrates for nucleic acid synthesis
发明人：PECK BILL JAMES
权利人:TWIST BIOSCIENCE CORP
摘要:Provided herein are compositions, devices, systems and methods for the generation and use of biomolecule-based information for storage. Further described herein are highly efficient methods for long term data storage with 100% accuracy in the retention of information. Additionally, devices described herein for de novo synthesis of oligonucleic acids encoding information related to the original source information may have a flexible material for oligonucleic acids extension.