CAS: 3063-94-3; 1,1,1,3,3,3-Hexafluoroisopropylmethacrylate

相似化合物

2160-89-6 352-87-4 105935-24-8

六氟异丙醇,甲基丙烯酰氯置于三乙胺,对苯二酚体系中,用 环己酮 用作溶剂,化学反应 3.0H,反应生成1,1,1,3,3,3-六氟异丙基异丁烯酸酯
参考文献:甲基丙烯酸六氟异丙酯及其制备方法
标题:甲基丙烯酸六氟异丙酯及其制备方法
摘要:本发明提供了一种甲基丙烯酸六氟异丙酯的制备方法,该方法包括:将1份六氟异丙醇与1.5‑4份缚酸剂,2‑4份有机溶剂加入到反应瓶内,混合均匀;向所述反应瓶中增加阻聚剂;将2‑2.5份甲基丙烯酰氯滴加到所述反应瓶内,预设温度下进行酯化反应;反应结束后,将反应液分离纯化得到甲基丙烯酸六氟异丙酯.本发明还提供一种甲基丙烯酸六氟异丙酯.本发明中的甲基丙烯酸六氟异丙酯的制备方法,得到高纯度的甲基丙烯酸六氟异丙酯产物,经效液相色谱仪检测,产物的纯度大于99.5%,金属离子杂质在100Ppb以下,满足半导体行业的质量标准.

专利信息

专利号:US-10465033-B2
优先权日:2016-11-10
标题:One step synthesis of ultrahigh molecular weight block copolymers
发明人：URBAN MAREK W
权利人:UNIV CLEMSON; UNIV CLEMSON RES FOUNDATION
摘要:Single-step synthesis processes for production of ultrahigh molecular weight block copolymers are described. The ultrahigh molecular weight copolymers can have a molecular weight of about 10 6 or greater and can be formed within a few hours in a surfactant-free environment. The formation process is controlled by initiator-starvation conditions in a sequential polymerization of monomers exhibiting different solubility in the solvent.

专利号:US-4889948-A
优先权日:1987-08-18
标题:Acrylate ester ether derivatives
发明人：MATHIAS LON J; KUSEFOGLU SELIM H
权利人:UNIV SOUTHERN MISSISSIPPI
摘要:A process for synthesizing ethers of alkyl alpha(hydroxymethyl)-acrylate by reacting alkyl acrylate and formaldehyde in the presence of a DABCO catalyst. The ethers may be used as cross-linking agents for thermoplastic polymers. Further, these ethers in turn enable synthesis of cyclopolymers that may show promising biological activity.

专利号:US-2016002367-A1
优先权日:2014-07-02
标题 :Synthesis of an acrylate polymer in flow reactor

专利号:WO-2025043025-A2
优先权日:2023-08-21
标题 :Methods for the synthesis of nanosheet membranes

专利号:US-4999410-A
优先权日:1987-08-18
标 题 :Acrylate ester ether derivatives
发明人：MATHIAS LON J; KUSEFOGLU SELIM H
权利人:UNIV SOUTHERN MISSISSIPPI
摘要:A process for synthesizing ethers of alkyl alpha-(hydroxymethyl)-acrylate by reacting alkyl acrylate and formaldehyde in the presence of a DABCO catalyst. The ethers may be used as cross-linking agents for thermoplastic polymers. Further, these ethers in turn enable synthesis of cyclopolymers that may show promising biological activity.

专利号:JP-2017524797-A
优先权日:2014-07-02
标 题 :Synthesis of acrylic polymers in a flow reactor.