CAS: 1002-69-3; 1-Chlorodecane

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癸烷置于丙醇,四氯化碳,氧气体系中,用 异辛烷 用作溶剂,化学反应生成1-氯癸烷
参考文献:在环境重要过程中铜与接枝离子液体的配合物
标题:在环境重要过程中铜与接枝离子液体的配合物
摘要:氯化铜(II)与季铵盐接枝在各种矿物载体上的复合物(sio 2-Ksk,Silochrome,Perlkat的改性)在两个对环境重要的过程中具有很高的活性:四氯化碳与烷烃的反应和氧化偶联硫醇.催化剂的有效性取决于过渡金属,离子液体和载体性质.在ccl 4转化中,与接枝在具有宽孔的二氧化硅上的烷基胺衍生物形成的配合物显示出最高的活性.在硫醇氧化的情况下,与具有窄孔的嫁接在perlkat上的杂环衍生物的复合物最活跃.Ccl 4的有效性 在将醇加入反应混合物中后,转化催化剂增加.
Doi:10.1016/j.Apcata.2013.10.041

专利信息

专利号:US-5779904-A
优先权日:1992-03-31
标题:Synthesis of inorganic membranes on supports
发明人：RUDERMAN WARREN; FEHLNER JAMES R; ZHANG ZHENYU
权利人:INRAD
摘要:Inorganic membranes such as zeolite membranes or other molecular sieve membranes can be provided by using silicone polymer material as starting material. A thin film zeolite membrane or a thin film membrane formed of interlocking zeolite crystals can be provided. Water soluble or water insoluble silicones can be treated in a basic solution under conditions and with an appropriate structure directing template, suitable aluminum content and at a temperature that is appropriate for growing a desired inorganic crystal framework. The membranes can be formed across the perforation of a support, such as a steel screen.

专利号:US-5474681-A
优先权日:1992-03-31
标 题:Synthesis of inorganic membranes
发明人：FEHLNER JAMES R; RUDERMAN WARREN; ZHANG ZHENYU
权利人:INRAD
摘要:Inorganic membranes such as zeolite membranes or other molecular sieve membranes can be provided by using silicone polymer material as starting material. A thin film zeolite membrane or a thin film membrane formed of interlocking zeolite crystals can be provided. Water soluble or water insoluble silicones can be treated in a basic solution under conditions and with an appropriate structure directing template, suitable aluminum content and at a temperature that is appropriate for growing a desired inorganic crystal framework. The continuous thin film membranes or interlocking crystal membranes can be formed on the sides of a reaction vessel, on the surface of the solution or on the surfaces of substrates introduced into the vessel.

专利号:EP-0021497-A1
优先权日:1979-06-21
标 题 :Synthesis of polyoxyalkylene glycol monoalkyl ethers
发明人：GIBSON THOMAS WILIAM
权利人:PROCTER & GAMBLE
摘要:A solvent free method for preparing monoalkyl ethers of polyoxyalkylene glycols, comprising mixing a polyoxyalkylene glycol, especially polyoxyethylene glycol, with a concentrated aqueous solution of a metal hydroxide, contacting said mixture with a primary alkyl halide, and recovering the monoalkyl ether.

专利号:US-3720697-A
优先权日:1971-03-01
标题 :Preparation of ortho-substituted aryl phosphines and metal complexes
发明人：FENTON D
权利人:UNION OIL CO
摘要:A METHOD IS DESCRIBED FOR THE PREPARATION OF MONOCYCLIC ARYL COMPOUNDS OF TRIVALENT GROUP V-A ELEMENTS WHEREIN THE ARYL SUBSTITUENT IS SUBSTITUTED IN ITS ORTHO POSITION WITH A HALOGEN, ALKYL, ARYLOXY OR ALJYLOXY SUBSTITUENT. THE RESULTANT COMPOUND IS USEFUL AS A LIGAND IN THE PREPARATION OF METAL COMPLEXES, SUCH AS COMPLEXES OF PALLADIUM AND PLATINUM, WHICH ARE CATALYSTS FOR HYDROCARBON CONVERSIONS SUCH AS OXIDATIONS OR HYROFORMYLATIONS. THE METHOD FOR THE ORTHO SUBSTITUTION OF THE AROMATIC COMPOUNDS COMPRISES THE REACTION OF A PALLADIUM OR PLATINUM CHELATE OF THE AROMATIC COMPOUND WITH SUBSTITUTING AGENYS SUCH AS HALOGEN OR HALIDE FOR THE HALOGENSUBSTITUTED, AN ALKYL HALID FOR THE ALKYL-SUBSTITUTED, OR AN ALKYL OR ARYK ORTHOFORMATE ESTER FOR THE ALKOLY OR ARYLOCYSUBSTITUTED COMPOUND. SUITABLE CHELATES FOR REACTION IN THIS METHOD OF SYNTHESIS ARE DISCLOSED IN MY APPLICATION, SER. NO. 873,641. FILED NOV. 3, 1969, NOW PAT. NO. 3,622,607.

专利号:TW-200806637-A
优先权日:2006-05-25
标题:Synthesis of triazole compounds that modulate HSP90 activity

专利号:US-6512146-B2
优先权日:1998-04-28
标 题 :Process for preparing a dialkyl acetal of a C8 to C30 aldehyde
发明人：PAULEY EDWARD P; NEIGHBOR KATHERINE SUE
权利人:PENFORD CORP
摘要:Improved water resistant acetal sizing agents including 1,1-octadecoxyoctadecane are provided along with methods for their synthesis including methods in which C 8 to C 30 alkyl bromides are reacted with a polyol under basic conditions and those in which a C 8 to C 30 primary alcohol is reacted with an organic base in the presence of a suitable oxidizing agent under basic conditions.