90076-65-6 + 16722-51-3 = 90076-65-6 反应条件:1.1 Solvents: Methanol; 48 H,40 °C 标题:Poly(Pyridinium Salt)S Containing 2,7-Diamino-9,9'-Dioctylfluorene Moieties With Various Organic Counterions Exhibiting Both Lyotropic Liquid-Crystalline And Light-Emitting Properties 作者:Bhowmik,Pradip K.; Jo,Tae S.; Koh,Jung J.; Park,Jongwon; Biswas,Bidyut; Et Al 参考文献:Molecules 日期:2021 卷标:26(6) 页码:1560]
90076-65-6 = 90076-65-6 反应条件:1.1 Reagents: 1-Bromodecane (Reaction Products With Mof Mil-101); 2 H,Rt 标题:Coordinate Covalent Grafted Ils-Modified Mil-101/peba Membrane For Pervaporation: Adsorption Simulation And Separation Characteristics 作者:Zhang,Ao-Shuai; Li,Shen-Hui; Ahmad,Ali; Mao,Heng; Xu,Li-Hao; Et Al 参考文献:Journal Of Membrane Science 日期:2021 卷标:619 页码:118807
专利信息
专利号:US-10260154-B2 优先权日:2015-08-01 标 题:Method for the synthesis of layered luminescent transition metal dichalcogenide quantum dots 发明人:MANIKOTH SHAIJUMON MANCHERI; DAMIEN DIJO; Gopalakrishnan Deepesh 权利人:INDIAN INSTITUTE OF SCIENCE EDUCATION AND RES THIRUVANANTHAPURAM IISER TVM 摘要:The invention discloses a method for the synthesis of monodispersed luminescent quantum dots of transition metal dichalcogenides (TMDC), single- or few-layered, using a single-step electrochemical exfoliation that involves dilute ionic liquid and water. The method disclosed helps to obtain nanoclusters of TMDC of desired size including small sizes ranging up to 6 nm, by varying the concentration of the electrolyte and the applied DC voltage. The invention further discloses a method by which mono- or few-layered luminescent transition metal dichalcogenides can be directly deposited onto conducting substrates in a uniform manner. The monodispersed single- or few-layered luminescent TMDC and electro-deposited substrates exhibit improved electronic conductivity and new active sites, making them suitable as high-performance electrocatalysts in hydrogen evolution reactions in solar water-splitting applications and also as electrodes for solar cell applications.
专利号:US-5072040-A 优先权日:1989-04-06 标 题:Process for synthesis of sulfonylimides 发明人:ARMAND MICHEL 权利人:CENTRE NAT RECH SCIENT; HYDRO QUEBEC 摘要:The invention relates to a process for the synthesis of sulfonylimides. n The process for the synthesis of sulfonylimides of the general formula M[RSO 2 ) 2 N] y , in which M represents a metal chosen from alkali metals, alkaline earth metals, rare earths, Al, Sc, Y and Th, R represents a monovalent radical chosen from linear or branched aliphatic radicals having 1 to 8 carbon atoms, alicyclic radicals having 3 to 8 carbon atoms, aryl radicals having 3 to 8 carbon atoms, and y is a number equal to the valence of M, is characterized in that an ionic nitride of the formula M 3 N y , in which M and y have the meaning given above, is reacted with a sulfonyl halide of the formula RSO 2 X, in which R has the meaning given above, and X is chosen from F or Cl, in an aprotic polar solvent.
专利号:US-9969823-B1 优先权日:2011-09-01 标题 :Synthesis and polymerization of vinyl triazolium ionic liquids 发明人:LUEBKE DAVID; NULWALA HUNAID; MATYJASZEWSKI KRZYSZTOF; ADZIMA BRIAN 权利人:US ENERGY; THE US DEPARTMENT OF ENERGY 摘要:Herein, we describe polymerized ionic liquids, demonstrate the synthesis of polymerized ionic liquids, and demonstrate the polymerization of triazolium monomers. One embodiment shows the polymeriazation of the triazolium monomers with bis(trifluoromethanesulfonyl)imide anions. In another embodiment we show the feasibility of copolymerizing with commodity monomers such as styrene using free radical polymerization techniques.
专利号:EP-4008687-A1 优先权日:2020-12-02 标 题:A method for the large scale synthesis of metal oxide nanosheets, and their uses 发明人:VINCENT MEWIN; ETACHERI VINODKUMAR 权利人:FUNDACION IMDEA MAT 摘要:The present invention relates to a rapid, scalable and inexpensive method for the synthesis of metal oxide nanosheets; the uses of the metal oxide nanosheets as electrode active materials and as catalyst; an electrode comprising the metal oxide nanosheets, a process for producing the electrode, a cell comprising the electrode and an energy storage and/or delivery system.
专利号:US-10280189-B2 优先权日:2012-07-17 标题:Method for the synthesis of aminoalkylenephosphonic acid 发明人:BURCK SEBASTIAN; LECLERCQ CEDRIC NICOLAS; NOTTE PATRICK 权利人:MONSANTO TECHNOLOGY LLC 摘要:A method for the synthesis of an aminoalkylenephosphonic acid or its phosphonate esters including the following steps: a) forming, in the presence of an aldehyde or ketone and an acid catalyst, a reaction mixture by mixing a compound having at least one HNR 1 R 2 moiety or a salt thereof, with a compound having one or more P—O—P anhydride moieties, the moieties having one P atom at the oxidation state (+III) and one P atom at the oxidation state (+III) or (+V), wherein the ratio of moles of aldehyde or ketone to N—H moieties is 1 or more and wherein the ratio of N—H moieties to P—O—P anhydride moieties is 0.3 or more, and b) recovering the resulting aminoalkylenephosphonic acid having compound or its phosphonate esters.
专利号:US-2022227624-A1 优先权日:2019-04-17 标 题:Method for Wet Chemical Synthesis of Lithium Argyrodites 发明人:WANG HUI; DRUFFEL THAD; BUCHBERGER DOMINIKA AGNIESZKA 权利人:BUCHBERGER DOMINIKA AGNIESZKA; UNIV LOUISVILLE RES FOUND INC; UNIV WARSZAWSKI; Uniwersy tet Warszawski 摘要:Methods for wet chemical synthesis of lithium argyrodites are provided, which in some embodiments include includes dissolving a stoichiometric mixture of precursors in a small quantity of solvent in an argon atmosphere, drying the mixture under vacuum or an inert gas atmosphere to evaporate the solvent, and then annealing to obtain a final lithium argyrodite product. Further embodiments comprise synthesizing the precursors, and excess halide doping to achieve higher ionic conductivity.
[参考文献]: Dominica H C Wong, Et Al. Nonflammable Perfluoropolyether-Based Electrolytes For Lithium Batteries. Proc Natl Acad Sci U S A. 2014 Mar 4;111(9):3327-31. [参考文献]: Enrique D Gomez, Et Al. Effect Of Ion Distribution On Conductivity Of Block Copolymer Electrolytes. Nano Lett. 2009 Mar;9(3):1212-6. [参考文献]: Lizhen Qiao, Et Al. Preparation And Evaluation Of Surface-Bonded Tricationic Ionic Liquid Silica As Stationary Phases For High-Performance Liquid Chromatography. J Chromatogr A. 2015 May 29:1396:62-71. [参考文献]: Mario Marinaro, Et Al. Electrochemical And Electron Microscopic Characterization Of Super-P Based Cathodes For Li-O2 Batteries. Beilstein J Nanotechnol. 2013 Oct 18:4:665-70. [参考文献]: Nurul Nadiah Sa'Adun, Et Al. Development And Characterization Of Poly(1-Vinylpyrrolidone-Co-Vinyl Acetate) Copolymer Based Polymer Electrolytes. Scientificworldjournal. 2014:2014:254215.
合成参考文献
摘要:Vashchenko, B. V.; Grygorenko, O. O., Science of Synthesis Knowledge Updates, (2021) 3, 368. 摘要:Galczynski, J.; Huang, H.; Lambert, T. H., Science of Synthesis: Special Topics, (2021) 1, 340. 摘要:Wang, P.-S.; Sayed, M.; Gong, L.-Z., Science of Synthesis: Knowledge Updates, (2023) 1, 204. 摘要:Iwasaki, T.; Kambe, N., Science of Synthesis: Cross-Dehydrogenative Coupling, (2023) nan, 220. 参考文献:10.2116/analsci.22.667 摘要:Tsujioka N, Imakura S, Nishi N, Kakiuchi T. Voltammetry of ion transfer across the electrochemically polarized micro liquid-liquid interface between water and a room-temperature ionic liquid, tetrahexylammonium bis(trifluoromethylsulfonyl)imide, using a glass capillary micropipette. Anal Sci. 2006 May;22(5):667–71. doi: 10.2116/analsci.22.667.