专利号:US-7355036-B2 优先权日:2001-07-03 标 题 :Two-stage protective groups for the synthesis of biopolymers 发明人:GUEIMIL RAMON; SCHEFFLER MATTHIAS; STAEHLER PEER F; BEIJER BARBRO 权利人:FEBIT AG 摘要:The invention relates to a method for the synthesis of a nucleic acid by gradual breakdown from protected synthesis building blocks carrying two-stage protective groups. The two-stage protective groups are split by means of a first exposure step and a subsequent chemical treatment step
专利号:US-9969823-B1 优先权日:2011-09-01 标题 :Synthesis and polymerization of vinyl triazolium ionic liquids 发明人:LUEBKE DAVID; NULWALA HUNAID; MATYJASZEWSKI KRZYSZTOF; ADZIMA BRIAN 权利人:US ENERGY; THE US DEPARTMENT OF ENERGY 摘要:Herein, we describe polymerized ionic liquids, demonstrate the synthesis of polymerized ionic liquids, and demonstrate the polymerization of triazolium monomers. One embodiment shows the polymeriazation of the triazolium monomers with bis(trifluoromethanesulfonyl)imide anions. In another embodiment we show the feasibility of copolymerizing with commodity monomers such as styrene using free radical polymerization techniques.
专利号:WO-2024260915-A1 优先权日:2023-06-19 标题:Dynamic covalent chemistry of spiropyrans for synthesis of photoswitchable photoinitiators and uses thereof 发明人:GARMSHAUSEN YVES 权利人:XOLO GMBH 摘要:The present invention relates to spiropyrans and process for the manufacture of them. In particular, a method is provided to exchange the indole and salicylaldehyde part of a spiropyran in a reversible reaction. The method is used for the synthesis of dual color photoinitiators with specific substituents and substitution patterns, which result in improved dual color volumetric printing (xolography). Furthermore, a process for locally polymerizing a starting material by dual color photopolymerization is disclosed.
专利号:US-6794547-B2 优先权日:2001-02-23 标题:Process for the synthesis of aryl alkyl monoethers 发明人:BORREDON ELISABETH; GASET ANTOINE; OUK SAMEDY; THIEBAUD-ROUX SOPHIE; LE GARS PIERRE 权利人:POUDRES & EXPLOSIFS STE NALE 摘要:The invention relates to a process for the synthesis of aryl alkyl monoethers by reaction of a phenol compound, comprising one or more hydroxyl groups attached to the aromatic system, and of a dialkyl carbonate. It is a solvent-free process carried out at a pressure of between 0.93x10<5 >Pa and 1.07x10<5 >Pa, at a temperature of between 100° C. and 200° C., and in the presence of a catalyst chosen from the group consisting of alkaline carbonates and alkaline hydroxides. The dialkyl carbonate is added gradually to the reaction mixture.
专利号:WO-2023112055-A1 优先权日:2021-12-15 标 题 :New synthetic process design for the synthesis of carboxy tormifene and purity analysis to strengthen antidoping testing 发明人:KUMAR GANGASANI JAGADEESH; PAWAR SACHIN DATTRAM; RADHAKRISHNANAND PULLAPANTHULA; MURTY UPADHYAYULA SURYANARAYANA; SAHU PURAN LAL; DUBEY SACHIN; SAHU KAPENDRA; UPADHYAY AWANISH; KUMAR PRAMOD 权利人:DIRECTOR NATIONAL INSTITUTE OF PHARMACEUTICAL EDUCATION AND RES GUWAHATI NIPER G; DIRECTOR NAT DOPE TESTING LABORATORY NDTL 摘要:The present invention relates to a process for preparing a compound of formula I: I. The compound of formula I is useful in anti-doping tests.
专利号:EP-4428168-A1 优先权日:2023-03-08 标 题 :Polyurethane/oligomeric urethane synthesis method by radiation 发明人:AKBULUT HÜSEYIN; ÇEL KBA SENA; ENADA SEHER; U AKLI MÜGE; DEM RBAY DUYGU 权利人:CHT TURKEY KIMYA SANAYI VE TICARET A S 摘要:In particular, the invention relates to the synthesis of radiation-curable polyurethane/oligomeric urethane dispersions of anionic and cationic characters, containing neutralization techniques characterized by the selection of counter ions as monomers and/or agents which can be polymers acting as promoters under radiation, to a radiation polyurethane/oligomeric urethane synthesis method that enables the creation of radiation curable binder systems without using cosolvents, surfactants, emulsifiers, defoamers, stabilizers and additives, wherein all components of the radiation-curable binder systems can be polymerized.
[参考文献]: Begoa Redruello, Et Al. A Novel Uhplc Method For The Rapid And Simultaneous Determination Of Daidzein, Genistein And Equol In Human Urine. J Chromatogr B Analyt Technol Biomed Life Sci. 2015 Nov 15:1005:1-8. [参考文献]: Dipratn G Khandare, Et Al. Fluorescence Turn-On Chemosensor For The Detection Of Dissolved Co2 Based On Ion-Induced Aggregation Of Tetraphenylethylene Derivative. Anal Chem. 2015 Nov 3;87(21):10871-7. [参考文献]: Jing Li, Et Al. Construction Of A Portable Sample Preparation Device With A Magnetic Poly(Methacrylic Acid-Co-Ethylene Dimethacrylate) Monolith As The Extraction Medium And Its Application In The Enrichment Of Uv Filters In Water Samples. J Sep Sci. 2014 Oct;37(19):2732-7. [参考文献]: Josef Dib, Et Al. Studies On The Collision-Induced Dissociation Of Adipor Agonists After Electrospray Ionization And Their Implementation In Sports Drug Testing. J Mass Spectrom. 2015 Feb;50(2):407-17. [参考文献]: Marianne Placzek, Et Al. Photosensitizing Properties Of Compounds Related To Benzophenone. Acta Derm Venereol. 2013 Jan;93(1):30-2.
合成参考文献
摘要:Takeda, T.; Tsubouchi, A., Science of Synthesis, (2010) 47, 275. 摘要:Wicha, J., Science of Synthesis, (2009) 48, 110. 摘要:Kwiecień, H., Science of Synthesis Knowledge Updates, (2014) 4, 85. 摘要:Sellars, J. D., Science of Synthesis Knowledge Updates, (2014) 1, 415. 摘要:Harsanyi, A.; Sandford, G., Science of Synthesis Knowledge Updates, (2015) 1, 172.