合成目标产物 Benzoguanamine 主要起始原料 2-Chloro-4,6-Diamino-1,3,5-Triazine And Phenylboronic Acid
461-58-5 = 91-76-9 反应条件:1.1 Reagents: Potassium Hydroxide Solvents: Polyethylene Glycol; 30 Min,170 °C 标题:Polyethylene Glycol As A Green Medium For The Microwave-Assisted Synthesis Of Guanamines 作者:Lim,Han Yin; Dolzhenko,Anton V. 参考文献:Chemistryselect 日期:2023 卷标:8(29)]
461-58-5 = 91-76-9 反应条件:1.1 Reagents: Potassium Hydroxide Solvents: Dimethyl Sulfoxide; 10 Min,463 K 标题:Green Synthesis And Self-Association Of 2,4-Diamino-1,3,5-Triazine Derivatives 作者:Diaz-Ortiz,Angel; Elguero,Jose; Foces-Foces,Concepcion; De La Hoz,Antonio; Moreno,Andres; Et Al 参考文献:New Journal Of Chemistry 日期:2004 卷标:28(8) 页码:952-958]
461-58-5 = 91-76-9 反应条件:1.1 Reagents: Potassium Hydroxide Solvents: Glycol Monoethyl Ether; 24 H,Reflux 标题:Synthesis Of New Derivatives Of 2,4-Diamino-6-Phenyl-1,3,5-Triazines 作者:Ouerfelli,Ines; Gatri,Rafik; Efrit,Mohamed Lotfi; Fillaut,Jean-Luc 参考文献:Journal De La Societe Chimique De Tunisie 日期:2010 卷标:12(2) 页码:117-122]
461-58-5 = 91-76-9 [标题:Reaction Conditions 标题:Hydroxide-Catalyzed Synthesis Of Heterocyclic Aromatic Amine Derivatives From Nitriles 作者:Smyrl,Norman R.; Smithwick,Robert W. Iii 参考文献:Journal Of Heterocyclic Chemistry 日期:1982 卷标:19(3) 页码:493-6]
461-58-5 + 100-52-7 = 91-76-9 反应条件:1.1 Reagents: Iodine,Ammonia Solvents: Tetrahydrofuran,Water; 1 H,Rt1.2 15 - 30 Min,80 °C 标题:Microwave-Assisted One-Pot Tandem Reactions For Direct Conversion Of Primary Alcohols And Aldehydes To Triazines And Tetrazoles In Aqueous Media 作者:Shie,Jiun-Jie; Fang,Jim-Min 参考文献:Journal Of Organic Chemistry 日期:2007 卷标:72(8) 页码:3141-3144]
98-80-6 + 3397-62-4 = 91-76-9 反应条件:1.1 Catalysts: Tetrakis(Triphenylphosphine)Palladium Solvents: 1,2-Dimethoxyethane1.2 Reagents: Sodium Carbonate Solvents: Water 标题:Synthesis Of 6-Aryl-2,4-Diamino-Pyrimidines And Triazines Using Palladium Catalyzed Suzuki Cross-Coupling Reactions 作者:Cooke,G.; Augier De Cremiers,H.; Rotello,V. M.; Tarbit,B.; Vanderstraeten,P. E. 参考文献:Tetrahedron 日期:2001 卷标:57(14) 页码:2787-2789]
= 91-76-9 [标题:Reaction Conditions 标题:Synthesis And Properties Of Sym-Triazine Derivatives. 5. Synthesis And Mass Spectrometric Investigation Of Sym-Triazinylureas 作者:Kelarev,V. I.; Bellul,M.; Karakhanov,R. A.; Ammar,Dibi; Lunin,A. F. 参考文献:Khimiya Geterotsiklicheskikh Soedinenii 日期:1987 卷标:(3) 页码:356-62]
= 91-76-9 [标题:Reaction Conditions 标题:A New Synthesis Of S-Triazines 作者:Alsofrom,D.; Grossberg,H.; Sheffer,H. 参考文献:Journal Of Heterocyclic Chemistry 日期:1976 卷标:13(4) 页码:917-19]
461-58-5 = 91-76-9 反应条件:1.1 Reagents: Potassium Hydroxide Solvents: 2-Methoxyethanol; 5 H,90 °C 标题:Synthesis Of Nanodispersible 6-Aryl-2,4-Diamino-1,3,5-Triazine And Its Derivatives 作者:Padalkar,Vikas S.; Patil,Vikas S.; Phatangare,Kiran R.; Gupta,Vinod D.; Umape,Prashant G.; Et Al 参考文献:Materials Science & Engineering 日期:2010 卷标:170(1-3) 页码:77-87]
461-58-5 + 100-52-7 = 91-76-9 反应条件:1.1 Catalysts: Copper Solvents: Water; 5 Min,Rt; 80 °C 标题:A Novel One-Pot Three Component Approach To 6-Substituted 2,4-Diamino-1,3,5-Triazines Using Nano-Sized Copper/zinc-Modified Mcm-41 (Cu/zn-Mcm-41) As A New Heterogeneous Mesoporous Catalyst 作者:Shekouhy,Mohsen; Moaddeli,Ali; Khalafi-Nezhad,Ali 参考文献:Journal Of Industrial And Engineering Chemistry (Amsterdam 日期:2017 卷标:50 页码:41-49]
461-58-5 = 91-76-9 反应条件:1.1 Reagents: Potassium Hydroxide Solvents: 1-Butyl-3-Methylimidazolium Hexafluorophosphate; 12 Min,130 °C 标题:Microwave-Assisted Clean Synthesis Of 6-Aryl-2,4-Diamino-1,3,5-Triazines In [bmim][pf6] 作者:Peng,Yanqing; Song,Gonghua 参考文献:Tetrahedron Letters 日期:2004 卷标:45(27) 页码:5313-5316]
461-58-5 + 100-52-7 = 91-76-9 反应条件:1.1 Reagents: Iodine,Ammonia Solvents: Tetrahydrofuran,Water; 1 H,Rt1.2 Reagents: Potassium Hydroxide; 24 H,Reflux 标题:Direct Conversion Of Aldehydes To Amides,Tetrazoles,And Triazines In Aqueous Media By One-Pot Tandem Reactions 作者:Shie,Jiun-Jie; Fang,Jim-Min 参考文献:Journal Of Organic Chemistry 日期:2003 卷标:68(3) 页码:1158-1160]
461-58-5 = 91-76-9 反应条件:1.1 Reagents: Potassium Hydroxide Solvents: Glycol Monoethyl Ether; 10 H,130 - 135 °C; Rt 标题:Synthesis,Molecular Docking Studies,And In Vitro Evaluation Of 1,3,5-Triazine Derivatives As Promising Antimicrobial Agents 作者:Patil,Vikrant; Noonikara-Poyil,Anurag; Joshi,Shrinivas D.; Patil,Shivaputra A.; Patil,Siddappa A.; Et Al 参考文献:Journal Of Molecular Structure 日期:2020 卷标:1220]
461-58-5 = 91-76-9 反应条件:1.1 Reagents: Potassium Hydroxide Solvents: 2-Methoxyethanol; 6 H,160 °C 标题:Control Of The Aggregation Of A Phenylenevinylenediimide Chromophore By Use Of Supramolecular Chemistry: Enhanced Electroluminescence In Supramolecular Organic Devices 作者:Delbosc,Nicolas; Reynes,Mathias; Dautel,Olivier J.; Wantz,Guillaume; Lere-Porte,Jean-Pierre; Et Al 参考文献:Chemistry Of Materials 日期:2010 卷标:22(18) 页码:5258-5270]
1853-95-8 = 91-76-9 反应条件:1.1 Reagents: Potassium Amide Solvents: Ammonia 标题:Ring Transformations Of Heterocycles. 35. Potassium Amide Induced Ring Transformation Of 1,2,4-Triazines Into 1,2,4-Triazoles And 1,3,5-Triazines 作者:Rykowski,A.; Van Der Plas,H. C. 参考文献:Journal Of Organic Chemistry 日期:1987 卷标:52(1) 页码:71-3]
113-00-8 + 100-51-6 = 91-76-9 反应条件:1.1 Reagents: Potassium Hydroxide,Hydrogen Catalysts: Platinum Solvents: Toluene; 24 H,Reflux 标题:Direct Synthesis Of Triazines From Alcohols And Amidines Using Supported Pt Nanoparticle Catalysts Via The Acceptorless Dehydrogenative Methodology 作者:Poly,Sharmin Sultana; Hashiguchi,Yuta; Nakamura,Isao; Fujitani,Tadahiro; Siddiki,S. M. A. Hakim 参考文献:Catalysis Science & Technology 日期:2022 卷标:12(15) 页码:4679-4687]
461-58-5 = 91-76-9 反应条件:1.1 Reagents: Sodium Hydroxide Solvents: Methanol; Rt -> 80 °C; 6 H,0.22 Mpa,80 °C 标题:A Green Technology For Production Of Benzoguanamine 作者:Liu,Hui; Li,Ling-Lan; Miao,Jun-Feng; Zhang,Shu; Guo,Liang-Liang 参考文献:Jingxi Huagong Zhongjianti 日期:2015 卷标:45(3) 页码:61-63]
461-58-5 = 91-76-9 反应条件:1.1 Catalysts: Sodium Hydroxide Solvents: 1-Butanol 标题:Synthesis Of Fluorescent Pigments Based On High-Temperature Resistant Organic Resin 作者:Xu,Li-He 参考文献:Ranliao Yu Ranse 日期:2003 卷标:40(1)]
= 91-76-9 [标题:Reaction Conditions 标题:Dimroth Rearrangement Of Acylamino-1,3,5-Triazines. V. Synthesis And Dimroth Rearrangement Of 2-Acylamino-4-Substituted-1,3,5-Triazines 作者:Honda,Itaru; Shimomura,Yoji 参考文献:Fukui Daigaku Kogakubu Kenkyu Hokoku 日期:1987 卷标:35(2) 页码:233-43]
= 91-76-9 [标题:Reaction Conditions 标题:Dimroth Rearrangement Of Acylamino-1,3,5-Triazines. I. Bisbenzoylation Of 2,4-Diamino-1,3,5-Triazine And Dimroth Rearrangement Of That Bis-Benzoylated Compound 作者:Honda,Itaru; Shimomura,Youji 参考文献:Fukui Daigaku Kogakubu Kenkyu Hokoku 日期:1985 卷标:33(2) 页码:185-95]
= 91-76-9 [标题:Reaction Conditions 标题:Syntheses Of Formaldehyde Stabilizers 作者:Kollar,Terezia; Bacaloglu,R.; Safta,M. 参考文献:Buletinul Stiintific Si Tehnic Al Institutului Politehnic Traian Vuia Timisoara 日期:1979 卷标:24(1) 页码:97-101]
= 91-76-9 [标题:Reaction Conditions 标题:Improved Synthesis Of Arylguanamines. Reaction Of Aromatic Nitriles With Dicyandiamide In Presence Of Sodium Ethoxide 作者:Lalezari,Iradj; Golgolab,Homa 参考文献:Journal Of Chemical And Engineering Data 日期:1971 卷标:16(1)]
= 91-76-9 [标题:Reaction Conditions 标题:Triazines And Related Products. Vi. Synthesis And Properties Of 4-Amino-2(2H)-Imino-S-Triazino[1,2-C][1,2,3]Benzotriazines 作者:Stevens,Malcolm F. G.; Mackenzie,Sheila M. 参考文献:Journal Of The Chemical Society [section] C: Organic 日期:1970 卷标:(17) 页码:2298-308
2-Amino-4-Phenyl-1,3,5-Triazine置于氨,Potassium Amide体系中,化学反应 24.0H,以60%的收率获得产物2,4-二氨基-6-苯基-1,3,5-三嗪 参考文献:Ring Transformations Of Heterocycles. 35. Potassium Amide Induced Ring Transformation Of 1,2,4-Triazines Into 1,2,4-Triazoles And 1,3,5-Triazines 标题:Ring Transformations Of Heterocycles. 35. Potassium Amide Induced Ring Transformation Of 1,2,4-Triazines Into 1,2,4-Triazoles And 1,3,5-Triazines 摘要: DOI:10.1021/jo00377A012
专利号:WO-9013609-A1 优先权日:1989-05-01 标题 :Novel fluorescent pigment compositions and a process for their preparation and use of same 发明人:MALLAVARAPU LEO X 权利人:MALLAVARAPU LEO X 摘要:A process is disclosed for producing novel fluorescent pigment compositions with no formaldehyde or para-formaldehyde during their synthesis. The synthesis of these compositions is, for example, achieved by using an in situ reaction of epoxy resins of preferably up to a molecular weight of 20,000 with a sulfonamide compound, e.g., toluene sulfonamide, in the presence of a Lewis acid catalyst, followed by, preferably, the further reaction with an isocyanate, e.g., aliphatic isocyanate and/or para-toluene sulfonyl isocyanate. During this reaction, a fluorescent dye is incorporated into the molten mass.
专利号:US-9703192-B2 优先权日:2012-09-15 标 题:Onium compounds and methods of synthesis thereof 发明人:LABEAUME PAUL J 权利人:ROHM & HAAS ELECT MAT 摘要:New onium salt compounds and methods for synthesis of such compounds are provided. Preferred methods of the invention include (a) providing an onium salt compound comprising a sulfonate component having an electron withdrawing group; and (b) treating the onium salt compound with a halide salt to form a distinct salt of the onium compound. The present onium compounds are useful as an acid generator component of a photoresist composition.
专利号:US-7351781-B2 优先权日:2001-04-24 标题 :Synthesis of vinyl polymers by controlled radical polymerization 发明人:WHITE DANIELA; O'DWYER JAMES B 权利人:PPG IND OHIO INC 摘要:A controlled free radical polymerization process, which includes the steps of: adding a monofunctional iniferter compound to an oxygen-free solvent; heating the solution to a temperature sufficient to allow the iniferter compound to form two carbon centered radical residues; adding a first monomer composition comprising one or more monomers to the solution containing the radical containing residues; polymerizing the first monomer composition to form a quasi-living polymer; and optionally polymerizing a second monomer composition comprising one or more monomers, which are different than the first monomer composition. The resulting non-random copolymer having the general formula:n nφ-[-A p -B s -] t -φn nwhere A and B are different compositions of ethylenically unsaturated monomers; p is an integer from 1 to 1,000; s is an integer from 0 to 1,000; t is an integer from 1 to 100; and φ is a residue from the iniferter.
专利号:WO-2005054219-A1 优先权日:2003-12-05 标 题:Process to modify non glycidyl functional impurities of glycidyl esters to be used in further radical polymerisation 发明人:HEYMANS DENIS MARIE CHARLES; HENRY NATHALIE SOLANGE JEANNE; UYTTERHOEVEN GRIET 权利人:RESOLUTION RES BELGIUM S A; HEYMANS DENIS MARIE CHARLES; HENRY NATHALIE SOLANGE JEANNE; UYTTERHOEVEN GRIET 摘要:The present invention relates to a process to modify the non glycidyl functional products occurring in industrially produced glycidyl esters, which are currently used in the synthesis of radical polymerisable acrylic or methacrylic acid derivatives, to be further reacted too resins for coating applications. The process to modify non glycidyl functional impurities in glycidyl esters of branched alkane carboxylic acids, by reacting the fraction of non-glycidyl functional products with ethylenically unsaturated anhydride. Another aspect of the present invention is formed by the cured coating films derived from the hereinbefore defined coating compositions and applied an a shaped substrate, and more in particular an automotives.
专利号:US-5753726-A 优先权日:1995-12-20 标 题:Synthesis of modified epoxy resins for cathodic electrodeposition with catalyst deactivation and diol modification 发明人:REUTER HARDY; JOUCK WALTER; OTT GUENTHER 权利人:BASF LACKE & FARBEN 摘要:Epoxy resins for preparing water-dispersible binders for cathodic electrodeposition coating materials, the epoxy resin being preparable by reacting a) polyepoxides having at least one glycidyl group per molecule b) and, optionally, up to 60% by weight, based on the overall epoxy resin reaction product, of aliphatic and/or alicyclic hydroxy compounds having preferably two or on average less than two hydroxyl groups per molecule and a molecular weight of less than 9000 g/mol, c) in the presence of a catalyst consisting of neutral metal salts, such as alkali metal salts and alkaline earth metal salts, zinc salts and nickel salts of tetrafluoroboric, tetrachloroboric, hexafluoro- antimonic,hexachloroantimonic,hexafluorophosphoric, perchlorate and periodic acid, and d) adding a deactivating agent which prevents the epoxy groups reacting further or effectively reduces the rate of such reaction as soon as the phenolic hydroxyl groups have already substantially reacted and at least 0.6% by weight of epoxy groups are still present, based on the overall weight of the epoxy resin reaction product.\\!
专利号:WO-2009115221-A1 优先权日:2008-03-18 标题:Composition for low colour of unsaturated glycidyl esters derivatives and the use thereof 发明人:HEYMANS DENIS MARIE CHARLES; UYTTERHOEVEN GRIET 权利人:HEXION SPECIALTY CHEMICALS RES; HEXION SPECIALTY CHEMICALS INC; HEYMANS DENIS MARIE CHARLES; UYTTERHOEVEN GRIET 摘要:The present invention relates to a composition comprising an aliphatic branched alcohol and glycidyl functional product esters, which are currently used in the synthesis of radical polymerisable acrylic or methacrylic acid derivatives, to be further reacted into resins for coating applications. Another aspect of the present invention is formed by the cured coating films derived from the hereinbefore defined coating compositions and applied on a shaped substrate, and more in particular on automotives.
摘要:Aggarwal, P.; Bebbington, M. W. P., Science of Synthesis Knowledge Updates, (2012) 2, 436. 摘要:Hansch, C., Leo, A., D. Hoekman. Exploring QSAR - Hydrophobic, Electronic, and Steric Constants. Washington, DC: American Chemical Society., 1995., p. 55 摘要:Kirk-Othmer Encyclopedia of Chemical Technology. 4th ed. Volumes 1: New York, NY. John Wiley and Sons, 1991-Present., p. V2 607 摘要:Franke C et al; Chemosphere 29: 1501-14 (1994) 摘要:Weast, R.C. and M.J. Astle. CRC Handbook of Data on Organic Compounds. Volumes I and II. Boca Raton, FL: CRC Press Inc. 1985., p. V1 253