CAS: 122-98-5; 2-(Phenylamino)Ethanol

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CAS号591-50-4 碘苯 | CAS号141-43-5 2-氨基乙醇 | CAS号141-46-8 羟乙醛 | CAS号108-86-1 溴苯 | CAS号98-80-6 苯硼酸 | CAS号96-49-1 碳酸乙烯酯 | CAS号75-21-8 环氧乙烷 | CAS号624-76-0 2-碘-1-乙醇 | CAS号438056-69-0 4-(4-氨苯基)吗啉-3-酮 | CAS号480-93-3 3-羟基吲哚 | CAS号92-64-8 N-(2-氰乙基)-N-羟乙基苯胺 | CAS号92-53-5 4-苯基吗啉 | CAS号93-90-3 N-甲基-N-羟乙基苯胺 | CAS号446292-04-2 4-(3-氧代-4-吗啉基)硝基苯 | CAS号366789-02-8 利伐沙班 | CAS号446292-07-5 2-[(2R)-2-羟基-3-... | CAS号2166-93-0 2-[N-[2-[N-(2-h... | CAS号179930-11-1 (R,E)-2-((苯并[d]...

2-(N-Phenylformamido)Ethyl Formate置于sodium Hydroxide体系中,用 甲醇 用作溶剂,化学反应 12.0H,以95%的收率获得n-苯基乙醇胺
参考文献:使用 4Czipn 作为光催化剂的吗啉衍生物的可见光介导的有氧氧化 C(Sp3)-C(Sp3) 键裂解
标题:使用 4Czipn 作为光催化剂的吗啉衍生物的可见光介导的有氧氧化 C(Sp3)-C(Sp3) 键裂解
摘要:在此,开发了一种用于惰性 C( Sp 3 )-C( Sp 3 ) 键有氧氧化裂解的无金属策略.以可见光为能源,O 2为氧化剂,在温和条件下进行吗啉衍生物的解构.该程序证明了合适的选择性和官能团耐受性.此外,基于一系列机制探索和控制实验,提出了涉及激进过程的可能机制.
Doi:10.1002/adsc.202100455

专利信息

专利号:US-10040752-B2
优先权日:2015-08-24
标 题 :Synthesis of levomethadone hydrochloride or dextromethadone hydrochloride and methods for use thereof
发明人：MKRTCHYAN GNEL; YAO QINGWEI
权利人:CODY LABORATORIES INC
摘要:Highly efficient methods for synthesis of levomethadone hydrochloride or dextromethadone hydrochloride are provided starting from D-alanine, or L-alanine, respectively, with retention of configuration. Methods for treating a subject are provided comprising administering a composition comprising an effective amount of levomethadone hydrochloride having not more than 10 ppm dextromethadone.

专利号:US-6765117-B2
优先权日:1997-10-24
标题:Process for stereoselective synthesis of prostacyclin derivatives
发明人：MORIARTY ROBERT M; PENMASTA RAJU; GUO LIANG; RAO MUNAGALA S; STASZEWSKI JAMES P
权利人:UNITED THERAPEUTIC CORP
摘要:An improved method is described for making 9-deoxy-PGF 1 -type compounds. In contrast to the prior art, the method is stereoselective and requires fewer steps than the known methods for making these compounds. The invention also relates to novel intermediates prepared during the synthesis of the 9-deoxy-PGF 1 -type compounds.

专利号:US-2004053355-A1
优先权日:2000-05-26
标题:Modular approach to on-line synthesis, drug discovery and biochemical transformations using immobilized enzyme reactors
发明人：WAINER IRVING; MARKOGLOU NEKTARIA
摘要:A coupled system using extremely different enzymes with incompatible cofactors and reaction conditions has been constructed using standard liquid chromatographic formats and open tubular formats. One of the significant aspects of the present invention lies in the development of the liquid chromatographic on-line enzyme cascade. This has been illustrated by the biosynthetic pathway involving dopamine beta-hydroxylase and phenylethanolamine N-methyltransferase which encompass the synthesis of the key neurotransmitters, norepinephrine and epinephrine. The results demonstrate for the first time the immobilization of dopamine beta-hydroxylase and phenylethanolamine N-methyltransferase. The IMERs are active and can be used in a liquid chromatographic format for qualitative and quantitative determinations. The IMER-HPLC system can be used to carry out standard Michaelis-Menten enzyme kinetic studies and to quantitatively determine enzyme kinetic constants, identify specific enzyme inhibitors, provide information regarding the mode of inhibition and the inhibitor constants (K i ). A second significant aspect of the present invention lies in the ability of the immobilized enzyme reactors to be used independently or as a combination, thus providing a unique opportunity to explore the interrelationships between these enzymes, to investigate the source of diseases and to design new drug entities for identified clinical syndromes.

专利号:US-2003004337-A1
优先权日:2000-05-04
标 题 :Efficient lactam synthesis
发明人：JUNG KYUNG WOON; YOON CHEOL HWAN
摘要:Lactams, libraries of lactams, and an efficient method of synthesizing a lactam, including a γ-lactam, in which an a-diazoacetamide of the general structure (I) is reacted under conditions promoting intramolecular C-H insertion, for example in the presence of a rhodium salt such as Rh 2 (OAc) 4 , n n n by which means lactams that are precursors in the synthesis of diverse natural and synthetic products, including pyrrolidinone compounds such as lactacystin, pramanicin, kainic acid, statine, AHPPA, and rolipram, are produced.

专利号:US-4033949-A
优先权日:1976-04-14
标 题:Analogs of thromboxane B2 and processes for their synthesis
发明人：KELLY ROBERT C; NELSON NORMAN A
权利人:UPJOHN CO
摘要:The present specification provides novel intermediates and novel processes for the synthesis of various side chain and skeletal analogs of Thromboxane B 2 (11β-homo-11a-oxa-PGF 2 .sub.α). These analogs are particularly and especially useful as reproductive cycle control agents.

专利号:US-6689890-B2
优先权日:2000-05-04
标 题:Efficient lactam synthesis
发明人：JUNG KYUNG WOON; YOON CHEOL HWAN
权利人:UNIV SOUTH FLORIDA
摘要:Lactams, libraries of lactams, and an efficient method of synthesizing a lactam, including a gamma-lactam, in which an alpha-diazoacetamide of the general structure (I) is reacted under conditions promoting intramolecular C-H insertion, for example in the presence of a rhodium salt such as Rh2(OAc)4,by which means lactams that are precursors in the synthesis of diverse natural and synthetic products, including pyrrolidinone compounds such as lactacystin, pramanicin, kainic acid, statine, AHPPA, and rolipram, are produced.