CAS: 1651-41-8; 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoroundecan-1-Ol

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全氟辛基碘烷置于lithium Aluminium Tetrahydride,偶氮二异丁腈体系中,用 乙醚 用作溶剂,化学反应 5.75H,反应生成3-全氟辛基丙醇
参考文献:具有新的全氟烷基苯甲酸酯侧基的低润湿性液晶聚丙烯酸酯的中间相结构
标题:具有新的全氟烷基苯甲酸酯侧基的低润湿性液晶聚丙烯酸酯的中间相结构
摘要:研究了在侧基中带有间隔开的4-全氟己基丙基苯甲酸酯和4-全氟辛基丙基苯甲酸酯单元的新型聚丙烯酸酯的合成,热行为,本体微观结构和润湿性.X射线衍射分析证明形成了不同的近晶中间相(smi 2,Smf 2和smc 2)以及它们的结构和晶格参数随温度的变化.中间相的多晶型行为取决于重复单元中全氟化链段的长度.绘制了沿近晶层法线的电子密度分布图,并提供了对倾斜的双层结构中侧链堆积的更深入的了解.从溶液浇铸聚合物薄膜,并通过测量与不同探测液体的接触角来确定其低润湿性.我们认为,薄膜的疏水性和疏油性是由中间相表面结构增强的,中间相表面结构是由高阶中间相本体结构介导的.©2010 Wiley Periodicals,Inc. J Polym Sci A部分:Polym Chem 48:4128-4139,2010年
Doi:10.1002/pola.24207

专利信息

专利号:US-7858772-B2
优先权日:2006-12-22
标 题 :Compounds and methods for synthesis and purification of oligonucleotides
发明人：GUPTA AMAR; WILL STEPHEN
权利人:ROCHE MOLECULAR SYSTEMS INC
摘要:The present invention provides methods of extending nucleic acids and purifying target nucleic acids. The methods include the use of capping reagents to effect chain termination and provide a handle for purification via fluorous affinity methods.

专利号:ES-2399363-T3
优先权日:2006-12-22
标 题 :Compounds and methods for the synthesis and purification of oligonucleotides

专利号:US-2008161548-A1
优先权日:2006-12-22
标 题 :Compounds and methods for synthesis and purification of oligonucleotides

专利号:EP-2097427-A1
优先权日:2006-12-22
标题 :Compounds and methods for synthesis and purification of oligonucleotides

专利号:CN-101547928-A
优先权日:2006-12-22
标题:Compounds and methods for synthesis and purification of oligonucleotides

专利号:EP-2097427-B1
优先权日:2006-12-22
标题 :Compounds and methods for synthesis and purification of oligonucleotides