CAS: 51851-37-7; Triethoxy(3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctyl)Silane

相似化合物

101947-16-4 102390-98-7 83048-65-1

三乙氧基硅烷,1H,1H,2H-全氟-1-辛烯置于chloroplatinic Acid体系中,用 异丙醇 作为反应溶剂,化学反应 0.12H,以97.7%的收率获得产物1H,1H,2H,2H-全氟辛基三乙氧基硅烷
参考文献:连续性流微反应器合成氟硅化合物的方法
标题:连续性流微反应器合成氟硅化合物的方法
摘要:本发明属于含氟材料技术领域,具体涉及一种连续性流微反应器合成氟硅化合物的方法.所述的合成方法,以连续性流微反应器为反应装置,包括以下步骤:1)将氟代烯烃通过物料通道a,烷氧基硅烷通过物料通道b,溶于有机溶剂的催化剂通过物料通道c分别经计量泵p1,P2和p3流入预设温度为t的混合反应模块m内进行混合反应;2)待混合反应结束后,反应液从出口d流出,对流出的反应液进行后处理,得到氟硅化合物.本发明提供的合成方法,科学合理,简单易行,能够克服现有的氯硅烷硅氢加成中存在的放热剧烈,操作控制难,设备要求苛刻,收率低,反应时间长等问题.

专利信息

专利号:US-2023313255-A1
优先权日:2020-07-15
标题:Massively Parallel Enzymatic Synthesis of Polynucleotides
发明人：HORGAN ADRIAN; LACHAIZE HENRI; VERARDO DOMIANO; GODRON XAVIER
权利人:DNA SCRIPT
摘要:The invention is directed to methods and compositions for inkjet assisted synthesis of a plurality of polynucleotides at reaction sites on a substrate using template-free polymerases, such as, terminal deoxynucleotidyl transferases (TdTs). Compositions of the invention include formulations of synthesis reagents for inkjet delivery including, but not limited to, TdT coupling reaction buffers and 3′-O-protected dNTP monomers.

专利号:US-11945957-B2
优先权日:2017-10-17
标题 :Aqueous composition and a method of producing durable and extremely efficient water repelling superhydrophobic materials at ambient condition thereof
发明人：THALAPPIL PRADEEP; BAIDYA AVIJIT; GANAYEE MOHD AZHARDIN; RAVINDRAN SWATHY JAKKA
权利人:INDIAN INSTITUTE OF TECH MADRAS; INDIAN INST TECH MADRAS
摘要:The present invention relates to a durable and multifunctional superhydrophobic coating composition and water based fabrication method of producing the durable and multifunctional superhydrophobic coating composition via chemical modification and functionalization of hydrophilic material by silanes under room temperature without any organic solvents. Synthesis of chemically modified cellulose nanofibers or clay in water forms excellent water repelling thin films upon coating over various substrates. The super hydrophobic materials are used as additive for paints, pigments, paper, varnish and, textile and used for various industrial applications such as construction of buildings and other super structures.

专利号:US-6384210-B1
优先权日:1997-03-20
标题:Solvent for biopolymer synthesis, solvent microdroplets and methods of use
发明人：BLANCHARD ALAN P
权利人:UNIV WASHINGTON
摘要:The present invention provides a method of biopolymer, esp. oligonucleotide, synthesis. The method consists of coupling a first nucleotide to a second nucleotide in a high surface tension solvent. The invention also provides microdroplets of a soln. comprising a solvent having a b.p. of 150 degree. C. or above, a surface tension of 30 dynes/cm or above, and a viscosity of 0.015 g/(cm)(sec), e.g., propylene carbonate. Such microdroplets are useful for the synthesis of chem. species, particularly biopolymers such as oligonucleotides and peptides, as well as arrays of chem. species. An automated system for oligonucleotide synthesis is described, which comprises delivery of microdroplets by inkjet technol. and computer control of the process. The high surface tension solvent used is selected for compatibility with the inkjet technol.

专利号:US-9981239-B2
优先权日:2015-04-21
标题:Devices and methods for oligonucleic acid library synthesis
发明人：BANYAI WILLIAM; PECK BILL JAMES; FERNANDEZ ANDRES; CHEN SIYUAN; INDERMUHLE PIERRE; MARSH EUGENE P
权利人:TWIST BIOSCIENCE CORP
摘要:Devices and methods for de novo synthesis of large and highly accurate libraries of oligonucleic acids are provided herein. Devices include structures having a main channel and microchannels, where the microchannels have a high surface area to volume ratio. Devices disclosed herein provide for de novo synthesis of oligonucleic acids having a low error rate.

专利号:US-6419883-B1
优先权日:1998-01-16
标题 :Chemical synthesis using solvent microdroplets
发明人：BLANCHARD ALAN P
权利人:UNIV WASHINGTON
摘要:The present invention relates to microdroplets of a solution comprising a solvent having a boiling point of 150° C. or above, a surface tension of 30 dynes/cm or above, and a viscosity of 0.015 g/(cm)(sec). Such microdroplets are useful for the synthesis of chemical species, particularly biopolymers such as oligonucleotides and peptides, as well as arrays of chemical species. Preferably, the solvent has the formula (I):whereinA=O or S;X=O, S or N (C1-C4 alkyl)Y=O, S, N(C1-C4 alkyl) or CH2; andR=C1-C20 straight or branched chain alkyl.

专利号:US-2006000773-A1
优先权日:2003-03-07
标题:Process for the synthesis of a chromatographic phase
发明人：GLENNON JEREMY; HEALY LIAM
权利人:GLENNON JEREMY; HEALY LIAM
摘要:A process for the synthesis, delivery or deposition or localisation of a chromatographic phase, especially for chromatographic separation or solid phase extraction, comprises introducing a chemical moiety to a support using a supercritical fluid such as supercritical carbon dioxide.