CAS: 95-83-0; 4-Chlorobenzene-1,2-Diamine
该化合物是一种有机化合物,其特点是芳香结构,并有氨基和氯功能组,似乎是固体的,通常是晶状的,以其暗色著称,该化合物主要用于染色工业,特别是合成异种染料,因为它能够形成稳定的彩色复合体;还用于生产各种化学品和作为有机合成的中间体. 4-Crolo-1-2苯二苯二烯在有机溶剂中可溶性,但在水中溶性有限.重要的是要谨慎地处理该物质,因为它可能对健康造成危害,包括皮肤和呼吸刺激,以及潜在的致癌影响.建议在实验室或工业环境中与该化合物合作时采取适当的安全措施,包括使用个人防护设备.
- 相似结构搜索
- 产品信息参考
;;;; - InChIKey: BXIXXXYDDJVHDL-UHFFFAOYSA-N
- InChI=1S/C6H7ClN2/c7-4-1-2-5(8)6(9)3-4/h1-3H,8-9H2…
- 计算化学: 氢键受体数2.0氢键供体数2可旋转键数0
物理性质
MSDS等安全信息
- GHS象形图
- GHS符号GHS08 & GHS07;
注释: Health hazard & Exclamation mark - 危险类别致癌性 类别2
特定目标器官毒性 - 单次接触 类别3
皮肤腐蚀/刺激 类别2
严重眼刺激 类别2
急性毒性 类别4(经口)
致突变性 类别2
急性毒性 类别4(吸入)
急性毒性 类别4(经皮)
皮肤腐蚀 类别1B - 警示词Warning(警告)
- 危险描述H351 |怀疑致癌.
H335 |可能引起呼吸道刺激.
H315 |造成皮肤刺激.
H319 |造成严重眼刺激.
H302 |吞咽有害.
H341 |怀疑导致遗传缺陷.
H332 |吸入有害.
H312 |皮肤接触有害.
H314 |造成严重皮肤灼伤和眼损伤. - 防范说明P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P362+P364-P403+P233-P405-P501
- UN编号3143.0
- 危险品标志Xn
- 风险等级Irritant
- 安全声明26-36/37
- 危险类别码36/37/38-40
- WGK Germany3
欧盟法规
ECHA物质C&L通报REACH预注册上下游产品
CAS号89-63-4 邻硝基对氯苯胺 | CAS号1635-61-6 5-氯-2-硝基苯胺 | CAS号17348-69-5 5-氯苯并呋喃 | CAS号2207-32-1 5-氯苯并-2,1,3噻二唑 | CAS号610-40-2 3,4-二硝基氯苯 | CAS号7440-66-6 锌标准溶液 | CAS号881-51-6 N-(4-氯-2-硝基苯基)乙酰胺 | CAS号106-47-8 对氯苯胺 | CAS号52184-29-9 2-(2’-硝基-4’-氯苯偶... | CAS号5228-61-5 5-溴-2-硝基苯胺 | CAS号39811-14-8 6-氯-1H-苯并[d]咪唑-2-羧酸 | CAS号5448-43-1 6-氯喹喔啉 | CAS号3584-66-5 5-氯-2-(三氯甲基)苯并咪唑 | CAS号14225-75-3 5-氯-2-(2-氯苯基)-1... | CAS号144729-44-2 4-氯-3-硝基苯-1,2-二胺 | CAS号14537-47-4 6-氯-1,2-二甲基-1H-... | CAS号4887-82-5 5-氯苯并咪唑 | CAS号2818-69-1 5-氯-2-甲基苯并咪唑 | CAS号51-17-2 苯并咪唑 | CAS号94-97-3 5-氯代苯并三氮唑合成工艺路线路线简述
- 610-40-2 = 95-83-0
反应条件:1.1 Reagents: Sodium Borohydride Catalysts: Alumina,Silver Solvents: Water; Rt; 35 Min,Rt1.2 Solvents: Ethyl Acetate; Rt
标题:Morphologically Tailored Facet Dependent Silver Nanoparticles Supported α-Al2O3 Catalysts For Chemoselective Reduction Of Aromatic Nitro Compounds
作者:Rajendiran,Rajesh; Seelam,Prem Kumar; Patchaiyappan,Arunkumar; Balla,Putrakumar; Shankar,Harisingh; Et Al
参考文献:Chemical Engineering Journal (Amsterdam 日期:2023 卷标:451]
= 95-83-0
反应条件:1.1 Reagents: Sodium Pyrosulfite Solvents: Water; 2 H,Reflux
标题:Synthesis And Antimycobacterial Activity Of 2,5-Disubstituted And 1,2,5-Trisubstituted Benzimidazoles
作者:Jimenez-Juarez,Rogelio; Cruz-Chavez,Wendy; De Jesus-Ramirez,Nayeli; Castro-Ramirez,Guadalupe Ivonne; Uribe-Gonzalez,Itzel; Et Al
参考文献:Frontiers In Chemistry (Lausanne 日期:2020 卷标:8]
= 95-83-0
反应条件:1.1 Catalysts: Cobalt (Supported On Silica) Solvents: Ethanol; 80 Min,70 °C1.2 Reagents: Hydrazine Hydrate (1:1)
标题:In Situ Synthesized Silica-Supported Co@n-Doped Carbon As Highly Efficient And Reusable Catalysts For Selective Reduction Of Halogenated Nitroaromatics
作者:Sheng,Yao; Wang,Xueguang; Yue,Shengnan; Cheng,Gonglin; Zou,Xiujing; Et Al
参考文献:Chemcatchem 日期:2020 卷标:12(18) 页码:4632-4641]
= 95-83-0
反应条件:1.1 Catalysts: Carbon Solvents: Ethanol; 80 °C1.2 Reagents: Hydrazine Hydrate (1:1); 3 H,80 °C
标题:Renewable Soybean Pulp Derived N-Doped Carbon Materials For Efficient Chemoselective Hydrogenation Of Halogenated Nitrobenzenes
作者:Lv,Jing; Zheng,Yunfeng; Zhu,Yangyang; Yuan,Man; Chang,Yanlong; Et Al
参考文献:Chemistryselect 日期:2019 卷标:4(14) 页码:4083-4091]
= 95-83-0
反应条件:1.1 Reagents: Sodium Borohydride Catalysts: Cobalt Iron Manganese Oxide (Cofe1.8Mn0.2O4) Solvents: Methanol; 1 Min,Rt; 1 Min,Rt
标题:Comn0.2Fe1.8O4 Ferrite Nanoparticles Engineered By Sol-Gel Technology: An Expert And Versatile Catalyst For The Reduction Of Nitroaromatic Compounds
作者:Goyal,Ankita; Bansal,S.; Samuel,Pankaj; Kumar,Vinod; Singhal,Sonal
参考文献:Journal Of Materials Chemistry A: Materials For Energy And Sustainability 日期:2014 卷标:2(44) 页码:18848-18860]
1635-61-6 = 95-83-0
反应条件:1.1 Reagents: Stannous Chloride Solvents: Ethanol; Overnight,Reflux1.2 Reagents: Sodium Hydroxide Solvents: Water; Ph 11
标题:Terbenzimidazoles Useful As Antifungal Agents
参考文献:United States]
1635-61-6 = 95-83-0
反应条件:1.1 Reagents: Hydrazine Hydrate (1:1) Catalysts: Iron(Iii) Acetylacetonate Solvents: Methanol; 2 Min,180 °C
标题:Hydrazine-Mediated Reduction Of Nitro And Azide Functionalities Catalyzed By Highly Active And Reusable Magnetic Iron Oxide Nanocrystals
作者:Cantillo,David; Moghaddam,Mojtaba Mirhosseini; Kappe,C. Oliver
参考文献:Journal Of Organic Chemistry 日期:2013 卷标:78(9) 页码:4530-4542]
1635-61-6 = 95-83-0
反应条件:1.1 Reagents: Sodium Borohydride Catalysts: Guanidine,Iron Oxide (Fe3O4),Palladium Solvents: Water; 25 Min,Rt
标题:Pdii On Guanidine-Functionalized Fe3O4 Nanoparticles As An Efficient Heterogeneous Catalyst For Suzuki-Miyaura Cross-Coupling And Reduction Of Nitroarenes In Aqueous Media
作者:Halligudra,Guddappa; Paramesh,Chitrabanu C.; Mudike,Ravi; Ningegowda,Mallesha; Rangappa,Dinesh; Et Al
参考文献:Acs Omega 日期:2021 卷标:6(50) 页码:34416-34428]
1635-61-6 = 95-83-0
反应条件:1.1 Reagents: Hydrazine Hydrate (1:1) Catalysts: Nickel Solvents: Ethanol,Water; 35 Min,Rt
标题:Enhanced Reduction Of Nitrobenzene Derivatives Using Reusable Ni Nanoparticles Supported On Multi-Layered Poly(1,2-Phenylenediamine)-Coated Layered Double Hydroxides
作者:Babamoradi,Jamshid; Ghorbani-Vaghei,Ramin; Alavinia,Sedigheh
参考文献:Canadian Journal Of Chemistry 日期:2022 卷标:100(6) 页码:412-421]
= 95-83-0
反应条件:1.1 Reagents: Hydrazine Hydrate (1:1) Catalysts: Nickel,Cobalt Solvents: Ethanol; 80 °C; 1 H,80 °C
标题:Chemoselective Transfer Hydrogenation Of Nitroarenes By Highly Dispersed Ni-Co Bmnps
作者:Zhang,Jia-Wei; Lu,Guo-Ping; Cai,Chun
参考文献:Catalysis Communications 日期:2016 卷标:84 页码:25-29]
1635-61-6 = 95-83-0
反应条件:1.1 Reagents: Hydrogen Catalysts: Iron Oxide (Fe2O3) (Lignin Residue-Derived Carbon-Supported) Solvents: Tetrahydrofuran,Water; 24 H,35 Bar,120 °C
标题:Lignin Residue-Derived Carbon-Supported Nanoscale Iron Catalyst For The Selective Hydrogenation Of Nitroarenes And Aromatic Aldehydes
作者:Sarki,Naina; Kumar,Raju; Singh,Baint; Ray,Anjan; Naik,Ganesh; Et Al
参考文献:Acs Omega 日期:2022 卷标:7(23) 页码:19804-19815]
= 95-83-0
反应条件:1.1 Reagents: Potassium Carbonate,Sodium Borohydride Catalysts: Palladium,2866309-20-6 Solvents: Methanol,Water; Rt
标题:Intensified Hydrogenation In Flow Using A Poly(β-Cyclodextrin) Network-Supported Catalyst
作者:Davis,Bradley A.; Bennett,Jeffrey A.; Genzer,Jan; Efimenko,Kirill; Abolhasani,Milad
参考文献:Acs Sustainable Chemistry & Engineering 日期:2022 卷标:10(48) 页码:15987-15998]
1635-61-6 = 95-83-0
反应条件:1.1 Reagents: Sodium Hydride,Hydrazine Hydrate (1:1) Catalysts: Palladium Diacetate Solvents: Water; 20 H,50 °C
标题:Method For Preparing Arylamine By Reduction Of Aromatic Nitro Compound
参考文献:China]
610-40-2 = 95-83-0
反应条件:1.1 Reagents: Sodium Borohydride Catalysts: 1638504-95-6 Solvents: Water; 0.25 H,27 °C
标题:A Hydroquinone Based Palladium Catalyst For Room Temperature Nitro Reduction In Water
作者:Kumar,Alok; Purkait,Kallol; Dey,Suman Kr.; Sarkar,Amrita; Mukherjee,Arindam
参考文献:Rsc Advances 日期:2014 卷标:4(66) 页码:35233-35237]
= 95-83-0
反应条件:1.1 Catalysts: Samarium,1,1′-Dioctyl-4,4′-Bipyridinium Dibromide Solvents: Methanol
标题:Samarium(0) And 1,1'-Dioctyl-4,4'-Bipyridinium Dibromide: A Novel Electron-Transfer System For The Chemoselective Reduction Of Aromatic Nitro Groups
作者:Yu,Chengzhi; Liu,Bin; Hu,Longqin
参考文献:Journal Of Organic Chemistry 日期:2001 卷标:66(3) 页码:919-924]
610-40-2 = 95-83-0
反应条件:1.1 Reagents: Sodium Borohydride Catalysts: Iron Oxide (Fe3O4) (Guanidine-Conjugated),Cu2+,N-(3-Chloropropyl)Guanidine (Conjugated With Iron Oxide Nanoparticles) Solvents: Ethanol; 35 Min,Rt
标题:Cu(Ii) Immobilized On Guanidine Functionalized Fe3O4 Magnetic Substrate As A Heterogeneous Catalyst For Selective Reduction Of Nitroarenes
作者:Halligudra,Guddappa; Chikkanayakanahalli Paramesh,Chitrabanu; Shetty,Manjunath; Kachigere Bhadraiah,Harsha; Kambappa,Vinaya; Et Al
参考文献:Journal Of The Iranian Chemical Society 日期:2022 卷标:19(8) 页码:3697-3709]
= 95-83-0
反应条件:1.1 Reagents: Sodium Borohydride Catalysts: Iron Oxide (Fe3O4),Carbon (Acidified,Carboxylated),(Sp-4-3)-Dichloro(1,7-Phenanthroline-Kn7)[1,1′-(Sulfinyl-Ks)Bis[methane]]Platinu... Solvents: Water; 15 Min,25 °C
标题:Chemoselective Reduction Of Nitro And Nitrile Compounds With Magnetic Carbon Nanotubes-Supported Pt(Ii) Catalyst Under Mild Conditions
作者:Tabatabaei Rezaei,Seyed Jamal; Khorramabadi,Hossein; Hesami,Ali; Ramazani,Ali; Amani,Vahid; Et Al
参考文献:Industrial & Engineering Chemistry Research 日期:2017 卷标:56(43) 页码:12256-12266]
= 95-83-0
反应条件:1.1 Reagents: Hydrogen Catalysts: Alumina,Palladium Solvents: Ethanol; 8 H,25 Bar,125 °C
标题:Scalable Continuous Flow Hydrogenations Using Pd/al2O3-Coated Rectangular Cross-Section 3D-Printed Static Mixers
作者:Lebl,Rene; Zhu,Yutong; Ng,Derrick; Hornung,Christian H.; Cantillo,David; Et Al
参考文献:Catalysis Today 日期:2022 卷标:383 页码:55-63]
= 95-83-0
反应条件:1.1 Reagents: Hydrogen Catalysts: Nickel Solvents: Methanol; 1 H,30 - 35 °C
标题:A Process For The Preparation Of Tizanidine Hydrochloride
参考文献:India]
1635-61-6 = 95-83-0
反应条件:1.1 Reagents: Hydrogen Catalysts: Ruthenium (Pine Needle-Derived Char Supported) Solvents: Water; 24 H,10 Bar,80 °C
标题:Biorenewable Carbon-Supported Ru Catalyst For N-Alkylation Of Amines With Alcohols And Selective Hydrogenation Of Nitroarenes
作者:Goyal,Vishakha; Sarki,Naina; Poddar,Mukesh Kumar; Narani,Anand; Tripathi,Deependra; Et Al
参考文献:New Journal Of Chemistry 日期:2021 卷标:45(32) 页码:14687-14694
5-溴-2-硝基苯胺置于四(三苯基膦)钯,Palladium On Activated Charcoal,甲酸铵,Potassium Carbonate体系中,化学反应生成 4-氯-1,2-苯二胺
参考文献:Identification Of Novel Hdac Inhibitors Through Cell Based Screening And Their Evaluation As Potential Anticancer Agents
标题:Identification Of Novel Hdac Inhibitors Through Cell Based Screening And Their Evaluation As Potential Anticancer Agents
摘要:A Series Of Benzimidazole Based Hdac Inhibitors Have Been Rationally Designed,Synthesized And Screened. The Sar Of This New Chemotype Is Described. The Lead Compound,11E,Showed Strong Activity In Several Cellular Assays And Demonstrated In Vivo Efficacy In Mouse Xenograft Pancreatic Cancer Models. (C) 2013 Elsevier Ltd. All Rights Reserved.
DOI:10.1016/j.Bmcl.2013.07.001
海关参考信息
- 2903919090-氯苯
- 💡 提示：海关信息按照顺序优先匹配，如需确认的海关信息，请参考相关资料。
- 详情请参考：📖 海关编码查询和海关进出口税则
专利信息
专利号:US-4336383-A
优先权日:1980-05-07
标题:1-1-Binaphthyl-4,4',5,5',8,8'-hexacarboxylic acid compounds, method of preparation and use thereof for the synthesis of asymmetric derivatives of 3,4,9,10-perylenetetracarboxylic acid, and for dyeing and printing of textile materials
发明人：VOROZHTSOV GEORGY N; MASANOVA NATALIA N; FELDBLJUM NIKOLAI B; ALEXEEV VASILY I; SHIGALEVSKY VADIM A; SOLOMATIN GEORGY G; SHULEPOVA OLGA I; KHAITUN GALINA G; GORDEEVA NADEZHDA V
权利人:VOROZHTSOV GEORGY N; MASANOVA NATALIA N; FELDBLJUM NIKOLAI B; ALEXEEV VASILY I; SHIGALEVSKY VADIM A; SOLOMATIN GEORGY G; SHULEPOVA OLGA I; KHAITUN GALINA G; GORDEEVA NADEZHDA V
摘要:1,1'-Binaphthyl-4,4',5,5',8,8'-hexacarboxylic acid compounds having the following formula: ##STR1## wherein R 1 is hydrogen, halogen, or alkyl; when X is oxygen, Y is hydrogen, alkyl, a cycloalkyl, or an aryl containing at least one substituent from the group including: halogen, alkyl, or alkoxy, when X is nitrogen, Y is ##STR2## wherein R 2 is hydrogen, halogen, or alkyl; Y being linked to X with the formation of a benzimidazole cycle. n The method for preparing the compounds according to the present invention resides in the treatment of that 1,1'-binaphthyl-4,4',5,5',8,8'-hexacarboxylic acid anhydride with an alkali to give a corresponding salt which is condensed with orthophenylenediamines upon heating at reflux at a pH of from 6.3 to 6.8. The resulting benzimidazole-1,1'-binaphthyl-4,4',5,5',8,8'-hexacarboxylic acid anhydride having the formula: ##STR3## wherein R 1 is hydrogen, halogen, or alkyl, is isolated and condensed with an amine or ortho-phenylenediamines in an excess of the amine, in water or an organic solvent, followed by isolation of the desired product. n The compounds according to the present invention are employed for the synthesis of asymmetric compounds of 3,4,9,10-perylenetetracarboxylic acid, as well as for dyeing and printing of textile materials with the formation, on the material, of asymmetric compounds of 3,4,9,10-perylenetetracarboxylic acid having the following formula: ##STR4## wherein R 1 is hydrogen, halogen, or alkyl; when X is oxygen, Y is hydrogen, alkyl, cycloalkyl, or aryl containing at least one substituent from the group including; halogen, alkyl, or alkoxy, when X is nitrogen, Y is ##STR5## where R 2 is hydrogen, halogen, or alkyl; Y being linked with X to form a benzimidazole cycle. n The compounds according to the present invention dye textile materials to various shades of violet color.
专利号:US-9951049-B2
优先权日:2014-05-15
标题 :Pyrazole linked benzimidazole conjugates and a process for preparation thereof
发明人：KAMAL AHMED; SHAIK ANVER BASHA; KUMAR GAJJELA BHARATH; REDDY VANGALA SANTHOSH
权利人:COUNCIL OF SCIENT & INDUSTRIAL RESEACH; COUNCIL SCIENT IND RES
摘要:Pyrazole linked benzimidazole conjugates and a method for synthesis of one or more compounds having a pyrazole linked benzimidazole conjugate, particularly pyrazole linked benzimidazole conjugates that are useful as potential antitumor agents against human cancer cell lines, such as leukemia, non-small cell lung cancer, colon cancer, CNS cancer, melanoma, ovarian cancer, renal cancer, prostate cancer and breast cancer. The process comprises the step of oxidative cyclization of o-phenylenediamines and 3-phenyl-1H-pyrazole-5-carbaldehydes with sodium metabisulphite in ethanol/methanol solvent system at a desired temperature for a period of time to obtain the pyrazole linked benzimidazole conjugate.
专利号:US-11738328-B2
优先权日:2021-04-30
标题:Single-step synthesis of chemisorption fiber sorbents (CHEFS) for the capture of CO2 and removal of water contaminants
发明人：GRAY MCMAHAN L; SHI FAN; YI SHOULIANG; WILFONG WALTER CHRIS; WANG QIUMING
权利人:US ENERGY
摘要:One or more embodiments relates to method for generating CHEFS having the steps of generating the CHEFS from a dope. One or more embodiments relates to a method for generating CHEFS having amine functional groups having the steps of generating a dope containing a BIAS with amine groups, at least one polymer, and at least one solvent; and forming CHEFS from the dope, wherein the generated CHEFS have no more than 30% amine loss compared to the BIAS.
专利号:US-2013102730-A1
优先权日:2010-04-02
标 题:Polyamine-containing polymers and methods of synthesis and use
发明人：JOST ROBERT W; ULUDAG HASAN; BOLUK MEHMET YAMAN
权利人:JOST ROBERT W; ULUDAG HASAN; BOLUK MEHMET YAMAN; ALBERTA INNOVATES TECHNOLOGY FUTURES
摘要:The present invention relates to polyamine-containing polymers and methods of their synthesis and use. The polymer may be hydroxyethylcellulose, dextran, poly(vinyl alcohol) or poly(methyl acrylate).
专利号:US-6107409-A
优先权日:1998-05-06
标 题:Gels derived from extending grafted comb polymers and polypropylene via a solution synthesis
发明人：HOGAN TERRENCE E; FOLTZ VICTOR J; LAWSON DAVID F; WANG XIAORONG
权利人:BRIDGESTONE CORP
摘要:The present invention teaches a method for enabling the formation of a high damping, soft polymer gel. The method includes: reacting in a suitable solvent a poly(alkenyl benzene-co-maleic anhydride) and a primary amine to form a poly(alkenyl benzene-co-maleimide) polymer. The poly(alkenyl benzene-co-maleimide) polymer while remaining in solvent is grafted with a maleated polyalkylene through the use of a grafting agent such as an alkyl diamine to form a polyalkylene grafted poly(alkenyl benzene-co-maleimide) polymer product. The solvent is then removed from the polyalkylene grafted poly(alkenyl benzene-co-maleimide) polymer product and the polymer is mixed with extender such as oil sufficient to form the gel. During oil extension the graft copolymer is further crosslinked due to the presence of additional alkyl diamine.
专利号:US-2022347654-A1
优先权日:2021-04-30
标题 :Single-Step Synthesis of CHEmisorption Fiber Sorbents (CHEFS) for the Capture of CO2 and Removal of Water Contaminants
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供应商参考报价(招募中)
品牌试剂参考报价(招募中)
📌 第三方产品分析报告
主要参考文献
参考标题:Highly Chemoselective Reduction Of Nitroarenes Over Non-Noble Metal Nickel-Molybdenum Oxide Catalysts作者:Haigen Huang,Xueguang Wang,Xu Li,Chenju Chen,Xiujing Zou,Weizhong Ding,Xionggang Lu
摘要:Chemoselective Reduction Of Nitroarenes Is An Important Transformation For The Production Of Arylamines, Which Are The Primary Intermediates In The Synthesis Of Pharmaceuticals, Agrochemicals And Dyes. Heterogeneous Non-Noble Metal Nickel-Molybdenum...
合成参考文献
参考文献:10.1107/s1600536811014954
摘要:Yamin BM, Osman UM. 1,2-Bis(N'-benzoyl-thio-ureido)-4-chloro-benzene. Acta Crystallogr Sect E Struct Rep Online. 2011 Jun 01;67(Pt 6):o1286.
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