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N-Fmoc-N'-Boc-L-2,3-二氨基丙酸置于4-二甲氨基吡啶,二乙胺体系中,用 甲醇,二氯甲烷 作为反应溶剂,化学反应 21.17H,反应生成 L-3-N-Boc-2,3-二氨基丙酸甲酯
参考文献:具有极性胺的铱催化的不对称烯丙基胺化:获得具有铅样分子特性的结构单元
标题:具有极性胺的铱催化的不对称烯丙基胺化:获得具有铅样分子特性的结构单元
摘要:空气稳定的铱催化剂和偶极非质子传递溶剂二甲基亚砜(dmso)的组合首次允许在不对称的烯丙基取代中系统性地利用高极性,官能化的胺:低分子量,富含sp 3的手性体系获得具有理化性质的嵌段,这对于合成铅样小分子将是有价值的.
DOI:10.1002/adsc.201000721

专利信息

专利号:US-9115102-B2
优先权日:2009-09-17
标题 :N-[2-hydroxycarbamoyl-2-(piperazinyl) ethyl] benzamide compounds, their preparation and their use as TACE inhibitors
发明人：CHAMBON SANDRINE; CLARY LAURENCE; SCHUPPLI MARLENE
权利人:CHAMBON SANDRINE; CLARY LAURENCE; SCHUPPLI MARLENE; GALDERMA RES & DEV
摘要:The present invention relates to novel benzene-carboxamide compounds having a structure that corresponds to the general formula (I), and also to their method of synthesis and to their use in pharmaceutical compositions intended for use in human or veterinary medicine or else to their use in cosmetic compositions.