CAS: 39828-35-8; 2,4-Dimethoxybenzoyl Chloride

上下游产品

2,4 dimethoxybenzoic acid 1-Bromo-2,4-dimethoxybenzene 2-diazo-1-(3,4-dimethoxyphenyl)ethanone 2,4,6-trihydroxy-2',4'-dimethoxy-benzophenone (2,4-dimethoxyphenyl)(3,4-dimethoxyphenyl)methanone 2-(2,4-dimethoxy-benzoyloxy)-4-methoxy-benzoic acid

2,4-二甲氧基溴苯置于正丁基锂,草酰氯,N,N-二甲基甲酰胺体系中,用 四氢呋喃,二氯甲烷 用作溶剂,化学反应 4.25H,反应生成2,4-二甲氧基苯甲酰氯
参考文献:补骨脂素衍生物的合成及其抗癌活性:Lespeflorin I 1的首次合成
标题:补骨脂素衍生物的合成及其抗癌活性:Lespeflorin I 1的首次合成
摘要:描述了用于制备许多不同的抗癌天然产物补骨脂素衍生物的合成方案.使用简单的起始原料,例如取代的苯基乙酸酯和苯甲酸,采用收敛的合成方法.发达的合成路线使我们完成了类似的天然产物莱斯佩弗洛林i 1(一种温和的黑色素合成抑制剂)的首次合成.针对两种常用的前列腺癌细胞系进行了合成化合物的初步生物活性研究.结果表明,可以通过对官能团的简单修饰来控制化合物的生物活性.
Doi:10.1016/j.Tet.2016.04.066

专利信息

专利号:US-11312696-B2
优先权日:2017-11-21
标 题:Synthesis of morin and morin derivatives
发明人：LINDEL THOMAS; MENDE STEFFEN
权利人:ORSATEC GMBH
摘要:The invention relates to a method for directly producing morin derivatives and high-purity morin of formula (I). The invention also relates to morin derivatives and high-purity morin that can be obtained using the claimed method.

专利号:US-5268423-A
优先权日:1992-02-28
标题 :Method for preparation of peptide synthesis resins and peptide synthesis resins
发明人：JORAN ALVIN D
权利人:UNIV NEW YORK
摘要:A solid phase resin useful as a support for peptide synthesis is synthesized stepwise from a solid phase polymer by reacting a solid phase phenyl ether resin with an alkoxy benzoyl halide to form a solid phase having (alkoxybenzoyl)phenoxymethyl groups bound thereto. The hydroxy group of the benzoyl moiety may be converted to a free amine by reacting with an ammonium salt of a carboxylic acid and then hydrolyzing with alkali. Novel resins produced by this method include those in which the solid phase phenyl ether resin is a resin having alkyl phenyl moieties linked to alkoxy phenyl groups by an ether linkage.

专利号:WO-2023207268-A1
优先权日:2022-04-26
标 题:Synthesis method of plant-derived deoxycholic acid
发明人：LI CHENCHEN; QIU WENWEI; LI JIE; WEN XINYI
权利人:SHANGHAI CLICK BIOTECH CO LTD
摘要:Provided is a synthesis method for deoxycholic acid, which synthesizes deoxycholic acid from plant-derived 9-OH-BA as the starting material by means of steps of side chain oxidation reaction, Wittig or Wittig-Horner reaction, dehydration reaction, hydrogenation reaction, esterification reaction, C epoxidation reaction, carbonyl reduction reaction, hydrolysis reaction, and the like.

专利号:US-2020308131-A1
优先权日:2017-11-21
标 题 :Synthesis of morin and morin derivatives

专利号:CN-111630041-A
优先权日:2017-11-21
标 题:Synthesis of morin and morin derivative

专利号:US-6664410-B1
优先权日:1999-07-15
标题 :Solid phase nitrile synthesis
发明人：KOBYLECKI RYSZARD; HONE NEAL DAVID; PAYNE LLOYD JAMES
权利人:MILLENNIUM PHARMACEUTICALS LTD
摘要:A nitrile compound is prepared by treating a solid supported amide to dehydrate it and cleave it from the support in one operation. The preparation involves acetylation of the amide compound in the presence of a base at a temperature of less than 100° C.