合成目标产物 Sulfur Hexafluoride 主要起始原料 Fluorine And Sulfur
(文献来源)合成步骤主要原料 Fluorine 和 Sulfur
Silver Fluoride置于氯,Sulfur体系中,用 Neat (No Solvent) 用作溶剂,化学反应生成六氟化硫 参考文献:Gmelin Handbuch Der Anorganischen Chemie,Gmelin Handbook: Ag: Mvol.B1,5.3.8.2,Page 298-299 标题:Gmelin Handbuch Der Anorganischen Chemie,Gmelin Handbook: Ag: Mvol.B1,5.3.8.2,Page 298-299
专利信息
专利号:US-9896336-B2 优先权日:2008-06-11 标 题:Bromine-facilitated synthesis of fluoro-sulfur compounds 发明人:WINTER ROLF 权利人:AVANTBIO CORP 摘要:Described herein are methods for the bromine-facilitated synthesis of fluoro-sulfur compounds, that include SF 4 , SF 5 Cl, SF 5 Br and SF 6 . The methods described herein generally require lower temperature and pressure, produce higher yields, require less time, do not use corrosive or costly reactants and solvents that are commonly used in the synthesis of the fluoro-sulfur compounds, and do not produce deleterious waste products when compared to previously-used methods.
专利号:US-2023286918-A1 优先权日:2020-07-02 标 题:Manufacturing process for 3,5-dichloropicolinonitrile for synthesis of vadadustat 发明人:JURKAUSKAS VALDAS; JUNG YOUNG CHUN; KWON TAESOO; KANNAN ARUNACHALAM; GONDI VIJAYA BHASKER 权利人:AKEBIA THERAPEUTICS INC 摘要:Disclosed herein are methods and processes of preparing vadadustat or a pharmaceutically acceptable salts thereof, and intermediates (e.g., a compound of Formula (I), (I-F), (II), or (IV), or a pharmaceutically acceptable salts thereof) useful for the synthesis of vadadustat.
专利号:US-2010173100-A1 优先权日:2006-01-16 标题 :Method for the synthesis of product molecules 发明人:WEISS HORST; GERBER GUSTAV; NUERNBERGER PATRICK HENNING; WOLPERT DANIEL STEPHAN 权利人:BASF AG 摘要:The invention relates to a method for the synthesis of product molecules, wherein ultrashort laser pulses shaped with the aid of a pulse shaper are generated and a gas which contains educt molecules is fed onto a surface, on which the educt molecules are at least partially adsorbed, the shaped ultrashort laser pulses being directed onto the surface in order to control a reaction process for synthesis of the product molecules from educts adsorbed on the surface.
专利号:US-10199177-B2 优先权日:2014-07-15 标 题:Method for the synthesis of nanocomposites based on TiO2 and carbonated nanostructures 发明人:HERLIN NATHALIE; WANG JIN; PINAULT MATHIEU; BOUCLE JOHANN 权利人:COMMISSARIAT ENERGIE ATOMIQUE; CENTRE NAT RECH SCIENT; UNIV LIMOGES 摘要:The invention relates to a method for the synthesis of a nanocomposite compound comprising TiO2 nanoparticles bound to carbon nanostructures, characterized in that it comprises the following steps: a) mixing carbon nanostructures and at least one TiO2 precursor in a first liquid in order to form a stock suspension; b) nebulizing said stock suspension and transporting it into a reaction chamber by means of a gaseous flow; and c) carrying out laser pyrolysis of said stock suspension in said reaction chamber in order to simultaneously form TiO2 nanoparticles and graft them onto the nano structures.
专利号:US-4886921-A 优先权日:1988-04-18 标题 :Synthesis of carbon fluoride and carbon fluoride chloride 发明人:NALEWAJEK DAVID 权利人:ALLIED SIGNAL INC 摘要:An improved synthesis of carbon fluoride CFx, and carbon fluoride chloride, (CyFxClz)n, is described. Direct fluorination of the intermediate (CyFxClz)n (x=0.7, y=1 and z=0.1) in the absence of chlorine produces, either CFx (x>/=1) or (CyFxClz)n (x>/=0.9, y=1, z=0.01) in as brief a period as 1 hour. The final CFx product is novel and exhibits improved properties compared to CFx made via conventional methods. The novel process for producing carbon fluoride chloride is more economical than prior art methods.
专利号:US-7015176-B2 优先权日:2003-06-03 标题 :Process for the synthesis of aryl sulfurpentafluorides 发明人:BAILEY III WADE H; CASTEEL JR WILLIAM J; PESARESI RENO J; PROZONIC FRANK M 权利人:AIR PROD & CHEM 摘要:A process is described for the synthesis of an aryl sulfur pentafluoride compound. In one embodiment of the present invention, there is provided a process for preparing an aryl sulfurpentafluoride compound comprising: combining an at least one aryl sulfur compound with a fluorinating agent to at least partially react and form an intermediate aryl sulfurtrifluoride product; and exposing the intermediate aryl sulfurtrifluoride product to the fluorinating agent and optionally a fluoride source to at least partially react and form the aryl sulfurpentafluoride compound.
1: Yuan M, Li R, Zhang Y, Yang L, Zhang X, Tang C, Guo D. Enhancement Patterns of Intrahepatic Cholangiocarcinoma on Contrast-Enhanced Ultrasound: Correlation with Clinicopathologic Findings and Prognosis. Ultrasound Med Biol. 2018 Oct 3. pii: S0301-5629(18)30364-8. doi: 10.1016/j.ultrasmedbio.2018.08.014. [Epub ahead of print] doi: 10.1159/000492746. eCollection 2018 May-Aug. 3: Couch MJ, Ball IK, Li T, Fox MS, Biman B, Albert MS. (19) F MRI of the Lungs Using Inert Fluorinated Gases: Challenges and New Developments. J Magn Reson Imaging. 2018 Sep 24. doi: 10.1002/jmri.26292. [Epub ahead of print] Review. doi: 10.1021/acs.jpca.8b07189. Epub 2018 Sep 18. doi: 10.1097/ICO.0000000000001705. doi: 10.1364/AO.57.006004. doi: 10.1016/j.jcrs.2018.06.024. Epub 2018 Jul 27. doi: 10.3168/jds.2018-14456. Epub 2018 Jul 25. doi: 10.2147/COPD.S164285. eCollection 2018. 14: Li D, Akiyama H, Kishi S. Optical coherence tomography patterns and outcomes of contusion maculopathy caused by impact of sporting equipment. BMC Ophthalmol. 2018 Jul 16;18(1):174. doi: 10.1186/s12886-018-0843-x.
合成参考文献
参考文献:10.1007/s00417-009-1236-x 摘要:Weichel ED, Bower KS, Colyer MH. Chorioretinectomy for perforating or severe intraocular foreign body injuries. Graefe's Archive for Clinical and Experimental Ophthalmology. 2009 Nov 22;248(3):319–30. doi: 10.1007/s00417-009-1236-x. 参考文献:10.1055/s-0028-1110030 摘要:Mostbeck G. Real-time ultrasound (US) and contrast-enhanced US for suspicious axillary lymph nodes in breast cancer - a love and hate relationship Ultraschall Med. 2010 Feb;31(1):4–7. doi: 10.1055/s-0028-1110030. 参考文献:10.1161/circulationaha.110.006668 摘要:Giordana P, Baqué-Juston MC, Jeandel PY, Mondot L, Hirlemann J, Padovani B, Raffaelli C. Contrast-enhanced ultrasound of carotid artery wall in Takayasu disease: first evidence of application in diagnosis and monitoring of response to treatment. Circulation. 2011 Jul 12;124(2):245–7. doi: 10.1161/circulationaha.110.006668. 参考文献:10.1007/s10792-011-9453-9 摘要:Yanyali A, Horozoglu F, Macin A, Bozkurt KT, Aykut V, Acar BT, Nohutcu AF. Corneal topographic changes after transconjunctival 23-gauge sutureless vitrectomy. Int Ophthalmol. 2011 Aug;31(4):277–82. doi: 10.1007/s10792-011-9453-9. 参考文献:10.1111/j.1464-410x.2011.10199.x 摘要:Taverna G, Morandi G, Seveso M, Giusti G, Benetti A, Colombo P, Minuti F, Grizzi F, Graziotti P. Colour Doppler and microbubble contrast agent ultrasonography do not improve cancer detection rate in transrectal systematic prostate biopsy sampling. BJU Int. 2011 Dec;108(11):1723–7. doi: 10.1111/j.1464-410x.2011.10199.x.