合成目标产物 Dinonyl Phthalate 主要起始原料 O-Xylene And 1-Nonanol
143-08-8 = 84-76-4 反应条件:1.1 Catalysts: 12-Tungstophosphoric Acid,Tetrabutyltitanium,Sulfuric Acid; 150 Min,453 °C 标题:Effect Of The Catalyst On The Rate Of Formation Of High Molecular Weight Aliphatic Phthalates 作者:Kulawska,Maria 参考文献:Przemysl Chemiczny 日期:2012 卷标:91(9) 页码:1851-1853]
143-08-8 = 84-76-4 [标题:Reaction Conditions 标题:Identification Of Some New Generation Additives For Polymers Obtained In The Catalytic Hydrogenation Process 作者:Dziwinski,Euzebiusz Jan; Bereska,Bartlomiej; Ilowska,Jolanta; Lach,Jozef; Bereska,Agnieszka; Et Al 参考文献:New Advances In Hydrogenation Processes: Fundamentals And Applications 日期:2017 卷标:227 页码:227-245]
143-08-8 = 84-76-4 反应条件:1.1 Catalysts: Sulfuric Acid Solvents: Water; 360 Min,443 K 标题:Kinetic Investigations On The Esterification Of Phthalic Anhydride With N-Heptyl,N-Nonyl Or N-Undecyl Alcohol Over Sulfuric Acid Catalyst 作者:Kulawska,Maria; Moroz,Henryk; Kasprzyk,Aleksandra 参考文献:Reaction Kinetics 日期:2011 卷标:104(1) 页码:9-15
辛烯置于phosphine Modified Cobalt Catalyst 甲烷磺酸,氢气体系中,用 甲苯 作为反应溶剂,50.0~200.0 °C,6.89 Mpa 条件下,反应 19.0H,反应生成 邻苯二甲酸二壬酯 参考文献:Nonyl Alcohols With A Low Degree Of Branching And Their Derivatives 标题:Nonyl Alcohols With A Low Degree Of Branching And Their Derivatives 摘要:该发明涉及低程度分支的壬醇及使用它们生产的衍生物.具体来说,本发明涉及主要壬醇混合物,其中至少80%的烷基链是直链,至少15%的烷基链在2-碳位置分支,以及其衍生物.低程度的分支产生的衍生物比使用更高度分支醇类产生的类似衍生物更加纤长且不那么臃肿.
专利号:US-9896523-B2 优先权日:2015-06-26 标题 :Ziegler-Natta catalyst synthesis and process thereof 发明人:SINGH GURMEET; KUMAR NARESH; KAUR SUKHDEEP; BANTU BHASKER; KAPUR GURPREET SINGH; SHASHIKANT 权利人:INDIAN OIL CORP LTD 摘要:The present invention describes a process of preparing a catalyst for olefin polymerization comprising: (i) treating a magnesium metal with an organohalide along with an internal donor to obtain a reaction mixture having solid component (A); (ii) treating the reaction mixture having solid component (A) with an acyl halide to obtain a reaction mixture having solid component (B); and (iii) treating the reaction mixture having solid component (B) of step (ii) with a transition metal compound to obtain the catalyst. The present invention also relates to a process for preparation of a catalyst system from said catalyst and preparation of a polyolefins from the catalyst system.
专利号:US-5194469-A 优先权日:1991-02-28 标题:Latex for coatings having improved flexibility 发明人:SRAIL RICHARD E; BURROWAY GARY L 权利人:GOODYEAR TIRE & RUBBER 摘要:This invention relates to the synthesis of a latex which can be formulated into coatings having improved flexibility and good water resistance. Coatings of this type are particularly useful in roof coating applications because they offer excellent flexibility, excellent ultra-violet light resistance, and good water resistance. The subject invention more specifically discloses a process for producing a neutralized latex that is useful in the manufacture of water reducible coatings which comprises: n (1) free radical aqueous emulsion polymerizing, at a pH of less than about 3.5, a monomer mixture which comprises, based on 100 weight percent monomers: (a) from about 30 to about 70 weight percent vinyl aromatic monomers, (b) from about 25 to about 65 weight percent of at least one alkyl acrylate monomer, (c) from about 1 to about 5 weight percent of acrylic acid, and (d) about 0.4 to about 3 weight percent methacrylic acid, in the presence of about 0.2 to 0.4 phm at least one sulfonate surfactant and in the presence of about 4 to 8 phm of at least one nonionic surface active agent having a hydrophile-lipophile balance number which is within the range of about 12 to about 20 to produce a latex; and n (2) neutralizing the latex with ammonia to a pH which is within the range of about 7 to about 10.5 to produce the neutralized latex.
专利号:US-5122566-A 优先权日:1989-10-06 标 题 :Latex for coatings having reduced blushing characteristics 发明人:BURROWAY GARY L; GESENHUES ALBERT M; BRADEN JENNIFER T 权利人:GOODYEAR TIRE & RUBBER 摘要:This invention relates to the synthesis of a latex which can be formulated into coatings having improved water resistance for both moisture vapor transmission and water spotting. Coatings which are formulated with the latex of this invention are particularly useful for coating metal substrates because they provide excellent rust and corrosion resistance. The subject invention more specifically discloses a process for producing a neutralized latex that is useful in the manufacture of water reducible coatings which comprises: (1) free radical aqueous emulsion polymerizing at a pH of less than about 3.5 a monomer mixture which comprises, based on 100 weight percent monomers: (a) from about 45 to about 85 weight percent vinyl aromatic monomers, (b) from about 15 to about 50 weight percent of at least one alkyl acrylate monomer, and (c) from about 1 to about 6 weight percent of at least one unsaturated carbonyl compound; in the presence of about 0.5 to 4.0 phm at least one phosphate ester surfactant and in the presence of about 0.5 to 4.0 phm of at least one water insoluble nonionic surface active agent to produce a latex; and (2) neutralizing the latex with ammonia to a pH which is within the range of about 7 to a bout 10.5 to produce the neutralized latex.
专利号:US-4968741-A 优先权日:1989-10-06 标题:Latex for coatings having reduced blushing characteristics 发明人:BURROWAY GARY L; GESENHUES ALBERT M; BRADEN JENNIFER T 权利人:GOODYEAR TIRE & RUBBER 摘要:This invention relates to the synthesis of a latex which can be formulated into coatings having improved water resistance for both moisture vapor transmission and water spotting. Coatings which are formulated with the latex of this invention are particularly useful for coating metal substrates because they provide excellent rust and corrosion resistance. The subject invention more specifically discloses a process for producing a neutralized latex that is useful in the manufacture of water reducible coatings which comprises: n (1) free radical aqueous emulsion polymerizing at a pH of less than about 3.5 a monomer mixture which comprises, based on 100 weight percent monomers: (a) from about 45 to about 85 weight percent vinyl aromatic monomers, (b) from about 15 to about 50 weight percent of at least one alkyl acrylate monomer, and (c) from about 1 to about 6 weight percent of at least one unsaturated carbonyl compound; in the presence of about 0.5 to 4.0 phm at least one phosphate ester surfactant and in the presence of about 0.5 to 4.0 phm of at least one water insoluble nonionic surface active agent to produce a latex; and n (2) neutralizing the latex with ammonia to a pH which is within the range of about 7 to about 10.5 to produce the neutralized latex.
专利号:NZ-587672-A 优先权日:2005-04-28 标 题:Intermediates suitable for the synthesis of lactam compounds
专利号:US-6770586-B2 优先权日:2000-04-24 标题 :Solid catalyst component and catalyst for olefins polymerization 发明人:TASHINO KUNIHIKO; SUZUKI YUKIHIRO; NISHIYAMA ISA; OGAWA HAYASHI; YOSHIDA TAKUMA; HOSAKA MOTOKI; SATO MAKI 权利人:TOHO TITANIUM CO LTD 摘要:Solid catalyst components and catalysts which contain (a) magnesium compound, (b) titanium tetrachloride, and (c) a phthalic acid diester or its derivative are useful in the synthesis of olefin polymers in high yields. Particularly, propylene polymers can be obtain in very high yields while retaining high stereoregularity.
摘要:Bingham, E.; Cohrssen, B.; Powell, C.H.; Patty's Toxicology Volumes 1-9 5th ed. John Wiley & Sons. New York, N.Y. (2001)., p. V6 849 摘要:40 CFR 716.120 (USEPA); U.S. National Archives and Records Administration's Electronic Code of Federal Regulations. Available from, as of April 16, 2008: 摘要:Brown VK H et al; Arch Toxicol 26 (1): 84-90 (1970) 摘要:Raymond MD et al; Patty's Toxicology. (2007). NY, NY: John Wiley & Sons, Inc. Esters of Aromatic Mono-, Di-, and Tricarboxylic Acids, Aromatic Diacids and Di-, Tri- or Polyalcohols. On-line posting date: Apr 16, 2001. 摘要:Lyman WJ et al; Handbook of Chemical Property Estimation Methods. Washington, DC: Amer Chem Soc pp. 7-4, 7-5, 8-12 (1990)