CAS: 51661-19-9; 1,2-Bis(O-Nitrophenoxy)Ethane

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potassium 4-nitrophenolate 1,2-dichloro-ethane ethylene dibromide sodium o-nitrophenate N-Ethyl-2-nitroaniline 2-nitro-N-methylaniline 1,2-bis(2-aminophenoxy)ethane-N,N,N'N'-tetraacetic acid tetraethyl ester 5,5'-diformyl-1,2-bis(2-aminophenoxy)ethane-N,N,N',N'-tetraacetic ethyl ester

硝苯酚置于potassium Carbonate体系中,用 N,N-二甲基甲酰胺 作为反应溶剂,化学反应 9.0H,反应生成 1,2-双(2-硝基苯氧基)乙烷
参考文献:Structural Study And Fluorescent Property Of A Novel Organic Microporous Crystalline Material
标题:Structural Study And Fluorescent Property Of A Novel Organic Microporous Crystalline Material
摘要:A Novel Microporous Organic Material [(2-{2-[2-(Bis-Methoxycarbonylmethylamino) Phenoxy] Ethoxy}-4-Benzimidazole-Phenyl) Methoxycarbonylmethylamino] Acetic Acid Methyl Ester 6 Was Synthesized And Characterized By Single Crystal X-Ray Diffraction,Fourier Transform Infrared Spectroscopy (Ft-Ir),Electron Spray Ionization-Mass Spectrometry (Esi-Hrms),X-Ray Powder Diffraction (Pxrd),H-1 And C-13 NMR. 6 Crystallizes In The Centrosymmetric Monoclinic Space Group C2/c,With Unit Cell Parameters A = 35.648(3) Angstrom,B = 14.3240(12) Angstrom,C = 15.3693(13) Angstrom,Alpha = 90.00,Beta = 94.8190(10),Gamma = 90.00,V = 7820.16 Angstrom(3) And Z = 8 At 296(2) K. As Indicated By Crystal Packing,The Molecular Conjugation Planes Arrange Along The C Axis To Form Micropores Due To The Hydrogen Bonds. In Addition,The Fluorescent Spectrum And Luminescence Lifetime Were Studied For 6.
DOI:10.5935/0103-5053.20130276