CAS: 1975-78-6; Decanonitrile

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334-48-5 112-31-2 2319-29-1

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癸酸乙酯置于sodium Diisobutyl-Tert-Butoxyaluminium Hydride,1,3-二碘-5,5-二甲基海因,氨体系中,用 四氢呋喃,水 用作溶剂,化学反应 5.0H,以79%的收率获得癸腈
参考文献:Facile Transformation Of Esters To Nitriles
标题:Facile Transformation Of Esters To Nitriles
摘要:Various Esters Were Efficiently Converted Into The Corresponding Nitriles In Good Yields By The Treatment With Sodium Diisobutyl-Tert-Butoxyaluminium Hydride (Sdbba-H),Followed By Treatment With Molecular Iodine In Aq Ammonia. The Present One-Pot Method Is Very Efficient And Practical For The Conversion Of Various Aromatic And Aliphatic Esters Into The Corresponding Nitrites. (C) 2011 Elsevier Ltd. All Rights Reserved.
Doi:10.1016/j.Tet.2011.08.028

专利信息

专利号:US-2024166514-A1
优先权日:2022-11-21
标题:Rapid synthesis of a sulfide-based solid electrolyte
发明人：FRANCISCO BRIAN E; OBERWETTER SAMUEL
权利人:SOLID POWER OPERATING INC
摘要:Provided herein are methods for synthesizing sulfide-based solid electrolytes, including those with an Argyrodite phase. The methods generally comprise mixing electrolyte precursors in a blend of solvents comprising a catalytic solvent and a spectator solvent.

专利号:US-8729283-B2
优先权日:2009-01-29
标 题 :Chain-selective synthesis of fuel components and chemical feedstocks
发明人：OLSON EDWIN S
权利人:ENERGY & ENVIRON RES CT FOUND
摘要:A method comprising providing a starting composition comprising a polyunsaturated fatty acid, a polyunsaturated fatty ester, a carboxylate salt of a polyunsaturated fatty acid, a polyunsaturated triglyceride, or a mixture thereof; self-metathesizing the starting composition or cross-metathesizing the starting composition with at least one short-chain olefin in the presence of a metathesis catalyst to form self-/cross-metathesis products comprising: cyclohexadiene; at least one olefin; and one or more acid-, ester-, or salt-functionalized alkene; and reacting cyclohexadiene to produce at least one cycloalkane or cycloalkane derivatives. A method for producing cycloalkanes for jet fuel by providing a starting composition comprising at least one selected from the group consisting of algal and polyunsaturated vegetable oils, subjecting the starting composition to metathesis to produce metathesis product comprising at least one olefin, cyclohexadiene, and at least one acid-, ester-, or salt-functionalized alkene, and reacting the at least one olefin and cyclohexadiene to form cycloalkane(s).

专利号:US-4219684-A
优先权日:1979-04-02
标 题 :Synthesis of alcohols by hydroformylation with nitrile promoter
发明人：IMAI TAMOTSU
权利人:UOP INC
摘要:Alcohols may be synthesized by reacting an olefinic compound, carbon monoxide and hydrogen in the presence of a Group VIII organometallic complex catalyst at reaction conditions which include a temperature in the range of from about 50° to about 250° C. and a pressure in the range of from about 10 to about 300 atmospheres. In addition, the reaction is also effected in the presence of a promoter compound comprising a nitrile.

专利号:US-5747180-A
优先权日:1995-05-19
标题 :Electrochemical synthesis of quasi-periodic quantum dot and nanostructure arrays
发明人：MILLER ALBERT E; BANDYOPADHYAY SUPRIYO
权利人:UNIV NOTRE DAME DU LAC
摘要:A method of fabricating two-dimensional regimented and quasi periodic arrays of metallic and semiconductor nanostructures (quantum dots) with diameters of Ëœ100 â„«(10 nm) includes the steps of polishing and anodizing a substrate to form a regimented quasi-periodic array of nanopits. The array forms a template for metallic or semiconductor material. The desired material is deposited in the nanopits by immersing the substrate in an appropriate solution and using the substrate as one cathode and inserting a second cathode in the solution.

专利号:WO-2010123589-A2
优先权日:2009-01-29
标题:Chain-selective synthesis of fuel components and chemical feedstocks

专利号:US-8137525-B1
优先权日:2003-01-13
标 题:Colloidal sphere templates and sphere-templated porous materials
发明人：HARRELD JOHN H; STUCKY GALEN D; MITCHELL NATHAN L; SAKAMOTO JEFF S
权利人:HARRELD JOHN H; STUCKY GALEN D; MITCHELL NATHAN L; SAKAMOTO JEFF S; UNIV CALIFORNIA
摘要:A method of making colloidal sphere templates and the sphere-templated porous materials made from the templates. The templated porous materials or thin films comprise micron and submicron-scaled spheres in ordered, disordered, or partially ordered arrays. The invention is useful in the synthesis of submicron porous, metallic tin-based and other high capacity anode materials with controlled pore structures for application in rechargeable lithium-ion batteries. The expected benefits of the resulting nanostructured metal films include a large increase in lithium storage capacity, rate capability, and improved stability with electrochemical cycling.