CAS: 86209-51-0; Primisulfuron-Methyl
该化合物是一种选择性的除草剂,主要用于控制各种作物,特别是玉米和大豆的宽叶草和某些草,它属于磺酰胺类除草剂,其作用是抑制对植物中基本氨基酸合成至关重要的酶乙酸合成,这种抑制导致目标杂草停止生长并最终死亡.Primisulfon的特点是其系统性行动,允许其被叶子和根部吸收,甚至在具有挑战性的条件下提供有效控制.它通常应用后乳液,其效力可能受到温度和湿度等环境因素的影响.该化合物对哺乳动物和鸟类毒性较低,因此对综合虫害管理是一个相对安全的选择.然而,必须注意防止径流,保护非目标杂草种,如同所有除草剂一样.适当的应用技术和遵守所建议的准则对于最大限度地其功效和尽量减少环境影响至关重要.
- 英文名称Primisulfuron-Methyl
- 中文名称氟嘧磺隆
- IUPAC名称methyl 2-(N-((4,6-bis(difluoromethoxy)pyrimidin-2-yl)carbamoyl)sulfamoyl)benzoate
- 其它别名Methyl 2-[4,6-bis(difluoromethoxy)pyrimidin-2-ylcarbamoylsulfamoyl]benzoate
- CAS编号86209-51-0
- MFCD编号:MFCD00337169
- EINECS号:617-814-2
- FDA UNII编号:3TN6B6S8JP
- 分子式:C15H12F4N4O7S
- 分子量:468.34
- 产品CID: 1863066
- 产品分类化学农药原药 → 除草剂 → 取代脲类除草剂
物理性质
- 熔点203.1 °C
- 沸点203.1°C
- 闪点203 °C
- 密度1.582g/cm3
- pKa:3.78±0.10(预测)
- PSA:154.19
- LogP:3.5211
- 折射率1.535
- 蒸汽压<5X10-3 mPa (<3.75X10-8 mm Hg) @ 25 °C
- 溶解性Solubility in acetone 35,000 mg/l, ethanol 1000 mg/l, toluene 570 mg/l, n-octanol 7.7 mg/l, n-hexane 1.5 mg/l (all measured at 25 °C)
- 敏感性水解反应半衰期为pH值3～5约10h，pH值7～9为>300h；土壤中半衰期为10～60h。≤100°C稳定。
- 外观形态Colorless crystals | Fine white powder
- 储存条件2-8°C
- 产品应用用于玉米田除草.外观:白色晶体
MSDS等安全信息
欧盟法规
ECHA物质C&L通报REACH预注册上下游产品
2-异氰酸磺酰基苯甲酸甲酯 2-(Methoxycarbonyl)Benzenesulfonyl Isocyanate 74222-95-0合成工艺路线路线简述
- 86209-44-1 + 74222-95-0 = 86209-51-0
反应条件:1.1 6 H,Reflux
标题:Synthesis And Herbicidal Activity Of Primisulfuron-Methyl
作者:Huang,Mingzhi
参考文献:Nongyao 日期:2003 卷标:42(10) 页码:15-16]
86209-44-1 + 74222-95-0 = 86209-51-0
反应条件:1.1 Solvents: 1,4-Dioxane; 3 H,Rt -> 80 °C
标题:Synthesis Of 2-[[[[[4,6-Bis(Difluoromethoxy)-2-Pyrimidinyl]Amino]Carbonyl]Amino]Sulfonyl]Benzoic Acid Methyl Ester (Primisulfuron)
作者:Wang,Jin-Ling; Et Al
参考文献:Yingyong Huaxue 日期:2009 卷标:26(4) 页码:486-488]
86209-44-1 + 153567-95-4 = 86209-51-0
反应条件:1.1 Solvents: Acetonitrile
标题:Synthesis Of Ultrahigh Effective Herbicide Primisulfuron-Methyl
作者:Xiao,Shenchu; Et Al
参考文献:Huaxue Shijie 日期:2001 卷标:42(7) 页码:391-392]
100478-26-0 = 86209-51-0
反应条件:1.1 Reagents: Ammonia Solvents: Dichloromethane,Water2.1 Solvents: Dichloromethane
标题:The Synthesis Of Herbicide Primisulfuron-Methyl
作者:Xiang,Dong; Et Al
参考文献:Nongyao 日期:2000 卷标:39(7)]
56-09-7 + 1717-59-5 = 86209-51-0
反应条件:1.1 Solvents: Acetonitrile; 3 H,50 °C2.1 Solvents: Acetonitrile
标题:Process For Preparation Of Fluorine-Containing Herbicides
参考文献:China]
56-09-7 = 86209-51-0
反应条件:1.1 Reagents: Sodium Hydroxide Solvents: 1,4-Dioxane,Water2.1 Solvents: Acetonitrile
标题:Synthesis Of Ultrahigh Effective Herbicide Primisulfuron-Methyl
作者:Xiao,Shenchu; Et Al
参考文献:Huaxue Shijie 日期:2001 卷标:42(7) 页码:391-392]
100478-25-9 = 86209-51-0
反应条件:1.1 Reagents: Hydrogen Peroxide Solvents: Acetic Acid,Water2.1 Reagents: Ammonia Solvents: Dichloromethane,Water3.1 Solvents: Dichloromethane
标题:The Synthesis Of Herbicide Primisulfuron-Methyl
作者:Xiang,Dong; Et Al
参考文献:Nongyao 日期:2000 卷标:39(7)]
113-00-8 + 105-53-3 = 86209-51-0
反应条件:1.1 Reagents: Sodium Ethoxide Solvents: Ethanol2.1 Reagents: Sodium Hydroxide Solvents: 1,4-Dioxane,Water3.1 Solvents: Acetonitrile
标题:Synthesis Of Ultrahigh Effective Herbicide Primisulfuron-Methyl
作者:Xiao,Shenchu; Et Al
参考文献:Huaxue Shijie 日期:2001 卷标:42(7) 页码:391-392]
1979-98-2 = 86209-51-0
反应条件:1.1 Reagents: Sodium Hydroxide Solvents: 1,4-Dioxane,Water; 4 H,Rt -> 65 °C1.2 Reagents: Hydrochloric Acid Solvents: Water; Ph 6,Rt1.3 2 H,Rt -> 65 °C2.1 Reagents: Hydrogen Peroxide Solvents: Acetic Acid,Water; Rt -> 85 °C; 80 - 85 °C; 2 H,80 - 85 °C2.2 Reagents: Water3.1 Reagents: Ammonium Hydroxide Solvents: Dichloromethane,Water; Rt; 3 H,Rt4.1 Solvents: 1,4-Dioxane; 3 H,Rt -> 80 °C
标题:Synthesis Of 2-[[[[[4,6-Bis(Difluoromethoxy)-2-Pyrimidinyl]Amino]Carbonyl]Amino]Sulfonyl]Benzoic Acid Methyl Ester (Primisulfuron)
作者:Wang,Jin-Ling; Et Al
参考文献:Yingyong Huaxue 日期:2009 卷标:26(4) 页码:486-488]
108-59-8 = 86209-51-0
反应条件:1.1 Reagents: Sodium Methoxide Solvents: Methanol2.1 Reagents: Sodium Hydroxide3.1 Catalysts: Tetrabutylammonium Chloride Solvents: Acetonitrile4.1 Reagents: Hydrogen Peroxide Solvents: Acetic Acid,Water5.1 Reagents: Ammonia Solvents: Dichloromethane,Water6.1 Solvents: Dichloromethane
标题:The Synthesis Of Herbicide Primisulfuron-Methyl
作者:Xiang,Dong; Et Al
参考文献:Nongyao 日期:2000 卷标:39(7)]
86209-44-1 + 74222-95-0 = 86209-51-0
反应条件:1.1 Solvents: Acetonitrile
标题:Process For Preparation Of Fluorine-Containing Herbicides
参考文献:China]
57683-71-3 + 116367-42-1 = 86209-51-0
反应条件:1.1 Solvents: Acetonitrile; 6 H,Reflux
标题:Study On The Synthesis Of Herbicide Primisulfuron-Methyl For Corn Farmland
作者:Lu,Yang; Et Al
参考文献:Jingxi Yu Zhuanyong Huaxuepin 日期:2006 卷标:14(15) 页码:13-14]
100478-26-0 = 86209-51-0
反应条件:1.1 Reagents: Ammonium Hydroxide Solvents: Dichloromethane,Water; Rt; 3 H,Rt2.1 Solvents: 1,4-Dioxane; 3 H,Rt -> 80 °C
标题:Synthesis Of 2-[[[[[4,6-Bis(Difluoromethoxy)-2-Pyrimidinyl]Amino]Carbonyl]Amino]Sulfonyl]Benzoic Acid Methyl Ester (Primisulfuron)
作者:Wang,Jin-Ling; Et Al
参考文献:Yingyong Huaxue 日期:2009 卷标:26(4) 页码:486-488]
86209-44-1 = 86209-51-0
反应条件:1.1 Reagents: Triethylamine Solvents: 1,2-Dichloroethane; 30 Min,70 °C; 70 °C -> 80 °C; 2 H,80 °C2.1 Solvents: Acetonitrile; 6 H,Reflux
标题:Study On The Synthesis Of Herbicide Primisulfuron-Methyl For Corn Farmland
作者:Lu,Yang; Et Al
参考文献:Jingxi Yu Zhuanyong Huaxuepin 日期:2006 卷标:14(15) 页码:13-14]
56-09-7 = 86209-51-0
反应条件:1.1 Reagents: Sodium Hydroxide Solvents: 1,4-Dioxane,Water; 1 H,60 - 70 °C2.1 6 H,Reflux
标题:Synthesis And Herbicidal Activity Of Primisulfuron-Methyl
作者:Huang,Mingzhi
参考文献:Nongyao 日期:2003 卷标:42(10) 页码:15-16]
56-09-7 = 86209-51-0
反应条件:1.1 Reagents: Sodium Hydroxide Solvents: 1,4-Dioxane,Water; 70 - 80 °C1.2 4 H,70 - 80 °C2.1 Reagents: Triethylamine Solvents: 1,2-Dichloroethane; 30 Min,70 °C; 70 °C -> 80 °C; 2 H,80 °C3.1 Solvents: Acetonitrile; 6 H,Reflux
标题:Study On The Synthesis Of Herbicide Primisulfuron-Methyl For Corn Farmland
作者:Lu,Yang; Et Al
参考文献:Jingxi Yu Zhuanyong Huaxuepin 日期:2006 卷标:14(15) 页码:13-14]
81-07-2 = 86209-51-0
反应条件:1.1 Reagents: Sulfuric Acid Solvents: Methanol; 6 H,Reflux2.1 Solvents: Acetonitrile; 6 H,Reflux
标题:Study On The Synthesis Of Herbicide Primisulfuron-Methyl For Corn Farmland
作者:Lu,Yang; Et Al
参考文献:Jingxi Yu Zhuanyong Huaxuepin 日期:2006 卷标:14(15) 页码:13-14]
100478-25-9 = 86209-51-0
反应条件:1.1 Reagents: Hydrogen Peroxide Solvents: Acetic Acid,Water; Rt -> 85 °C; 80 - 85 °C; 2 H,80 - 85 °C1.2 Reagents: Water2.1 Reagents: Ammonium Hydroxide Solvents: Dichloromethane,Water; Rt; 3 H,Rt3.1 Solvents: 1,4-Dioxane; 3 H,Rt -> 80 °C
标题:Synthesis Of 2-[[[[[4,6-Bis(Difluoromethoxy)-2-Pyrimidinyl]Amino]Carbonyl]Amino]Sulfonyl]Benzoic Acid Methyl Ester (Primisulfuron)
作者:Wang,Jin-Ling; Et Al
参考文献:Yingyong Huaxue 日期:2009 卷标:26(4) 页码:486-488]
113-00-8 + 105-53-3 = 86209-51-0
反应条件:1.1 Reagents: Sodium Ethoxide Solvents: Toluene; Rt -> Reflux1.2 Reflux; 4 - 5 H,Reflux1.3 Reagents: Hydrochloric Acid Solvents: Water; Neutralized2.1 Reagents: Sodium Hydroxide Solvents: 1,4-Dioxane,Water; 70 - 80 °C2.2 4 H,70 - 80 °C3.1 Reagents: Triethylamine Solvents: 1,2-Dichloroethane; 30 Min,70 °C; 70 °C -> 80 °C; 2 H,80 °C4.1 Solvents: Acetonitrile; 6 H,Reflux
标题:Study On The Synthesis Of Herbicide Primisulfuron-Methyl For Corn Farmland
作者:Lu,Yang; Et Al
参考文献:Jingxi Yu Zhuanyong Huaxuepin 日期:2006 卷标:14(15) 页码:13-14]
127697-72-7 = 86209-51-0
反应条件:1.1 Catalysts: Tetrabutylammonium Chloride Solvents: Acetonitrile2.1 Reagents: Hydrogen Peroxide Solvents: Acetic Acid,Water3.1 Reagents: Ammonia Solvents: Dichloromethane,Water4.1 Solvents: Dichloromethane
标题:The Synthesis Of Herbicide Primisulfuron-Methyl
作者:Xiang,Dong; Et Al
参考文献:Nongyao 日期:2000 卷标:39(7)]
31645-12-2 = 86209-51-0
反应条件:1.1 Reagents: Sodium Hydroxide Solvents: Water; Rt -> 10 °C; 0 - 10 °C; 4 H,0 - 10 °C1.2 Reagents: Hydrochloric Acid Solvents: Water; Ph 2,0 - 10 °C; 1 H,0 - 10 °C2.1 Reagents: Sodium Hydroxide Solvents: 1,4-Dioxane,Water; 4 H,Rt -> 65 °C2.2 Reagents: Hydrochloric Acid Solvents: Water; Ph 6,Rt2.3 2 H,Rt -> 65 °C3.1 Reagents: Hydrogen Peroxide Solvents: Acetic Acid,Water; Rt -> 85 °C; 80 - 85 °C; 2 H,80 - 85 °C3.2 Reagents: Water4.1 Reagents: Ammonium Hydroxide Solvents: Dichloromethane,Water; Rt; 3 H,Rt5.1 Solvents: 1,4-Dioxane; 3 H,Rt -> 80 °C
标题:Synthesis Of 2-[[[[[4,6-Bis(Difluoromethoxy)-2-Pyrimidinyl]Amino]Carbonyl]Amino]Sulfonyl]Benzoic Acid Methyl Ester (Primisulfuron)
作者:Wang,Jin-Ling; Et Al
参考文献:Yingyong Huaxue 日期:2009 卷标:26(4) 页码:486-488]
504-17-6 = 86209-51-0
反应条件:1.1 Reagents: Sodium Hydroxide2.1 Catalysts: Tetrabutylammonium Chloride Solvents: Acetonitrile3.1 Reagents: Hydrogen Peroxide Solvents: Acetic Acid,Water4.1 Reagents: Ammonia Solvents: Dichloromethane,Water5.1 Solvents: Dichloromethane
标题:The Synthesis Of Herbicide Primisulfuron-Methyl
作者:Xiang,Dong; Et Al
参考文献:Nongyao 日期:2000 卷标:39(7)]
105-53-3 = 86209-51-0
反应条件:1.1 Reagents: Sodium Methoxide Solvents: Methanol,Water; 30 Min,Rt; 5 H,Rt -> 70 °C; 70 °C -> Rt2.1 Reagents: Sodium Hydroxide Solvents: Water; Rt -> 10 °C; 0 - 10 °C; 4 H,0 - 10 °C2.2 Reagents: Hydrochloric Acid Solvents: Water; Ph 2,0 - 10 °C; 1 H,0 - 10 °C3.1 Reagents: Sodium Hydroxide Solvents: 1,4-Dioxane,Water; 4 H,Rt -> 65 °C3.2 Reagents: Hydrochloric Acid Solvents: Water; Ph 6,Rt3.3 2 H,Rt -> 65 °C4.1 Reagents: Hydrogen Peroxide Solvents: Acetic Acid,Water; Rt -> 85 °C; 80 - 85 °C; 2 H,80 - 85 °C4.2 Reagents: Water5.1 Reagents: Ammonium Hydroxide Solvents: Dichloromethane,Water; Rt; 3 H,Rt6.1 Solvents: 1,4-Dioxane; 3 H,Rt -> 80 °C
标题:Synthesis Of 2-[[[[[4,6-Bis(Difluoromethoxy)-2-Pyrimidinyl]Amino]Carbonyl]Amino]Sulfonyl]Benzoic Acid Methyl Ester (Primisulfuron)
作者:Wang,Jin-Ling; Et Al
参考文献:Yingyong Huaxue 日期:2009 卷标:26(4) 页码:486-488
2-异氰酸磺酰基苯甲酸甲酯,2-氨基-4,6-双(二氟甲氧基)嘧啶 以 1,4-二氧六环 作为反应溶剂,以affording The Title Compound With A Melting Point Of 186°-188oc.的收率获得产物甲基氟嘧磺隆
参考文献:N-Arylsulfonyl-N'-Pyrimidinylureas
标题:N-Arylsulfonyl-N'-Pyrimidinylureas
摘要:本发明涉及一般式为##str1##的n-芳基磺酰-N'-嘧啶基脲及其与胺,碱金属氢氧化物或碱土金属氢氧化物或季铵碱基的盐.这些化合物具有非常好的前后除草和生长调节性能.在该式中,R.Sub.18是氢,烷基或烷氧基,X是未取代或取代的苯基基团或未取代或取代的萘基基团,Y是c.Sub.1-C.Sub.3烷基,C.Sub.1-C.Sub.3卤代烷基,C.Sub.1-C.Sub.3烷氧基,C.Sub.1-C.Sub.3卤代烷氧基,C.Sub.1-C.Sub.3烷基硫基,C.Sub.2-C.Sub.3烷氧基烷基,卤素或未取代的氨基团,Z是氧或硫.
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专利信息
专利号:WO-2021130756-A1
优先权日:2019-12-25
标题:Combinations of non-protein amino acids and acetolactate synthase enzyme inhibitors
发明人：KLIPCAN LIRON; VAN-OSS PINHASI RUTH
权利人:THE STATE OF ISRAEL MINISTRY OF AGRICULTURE & RURAL DEVELOPMENT AGRICULTURAL RES ORGANIZATION ARO VO
摘要:The present invention provides compositions and methods for disrupting protein synthesis in plant cells.
专利号:US-11919928-B2
优先权日:2016-03-16
标题 :Method for producing dihydrotentoxin
发明人：KUBO TAKASHI; MACHIDA MASAYUKI; FUJIOKA TOMONORI; YAMAGUCHI Shigenari; KAWAI KIYOSHI
权利人:KUMIAI CHEMICAL INDUSTRY CO
摘要:An object of the present invention is to identify an enzyme having activity of synthesizing dihydrotentoxin that is a tentoxin precursor and an enzyme having activity of synthesizing tentoxin using dihydrotentoxin as a substrate. The present invention concerns a tentoxin synthesis-related gene encoding a protein comprising the amino acid sequence of SEQ ID NO: 16 and having activity of nonribosomal peptide synthesis of dihydrotentoxin and a tentoxin synthesis-related gene encoding a protein comprising the amino acid sequence of SEQ ID NO: 18 and having activity of converting dihydrotentoxin to tentoxin.
专利号:ES-2717283-T3
优先权日:2012-07-24
标 题:Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6- (4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and herbicides inhibitors of VLCFA synthesis and synthesis of fatty acids / lipids
专利号:TW-I655905-B
优先权日:2012-07-24
标题 :Contains 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl)pyridine-2-carboxylic acid or a derivative thereof and very long chain fatty acid (VLCFA) Synthesis of herbicidal compositions with fatty acid/fat synthesis inhibiting herbicides
专利号:US-9644469-B2
优先权日:2012-07-24
标题 :Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and VLCFA and lipid synthesis inhibiting herbicides
发明人：YERKES CARLA N; MANN RICHARD K; SHIRAISHI IKUO; YANAGIYAMA SHINGO; SATCHIVI NORBERT M
权利人:DOW AGROSCIENCES LLC
摘要:A synergistic herbicidal composition containing (a) a compound of formula (I): n nor an agriculturally acceptable salt or ester thereof and (b) VLCFA and fatty acid/lipid synthesis inhibiting herbicides, including but not limited to, acetochlor, alachlor, anilofos, benfuresate, cafenstrole, dimethenamid-P, fentrazamide, indanofan, flufenacet, mefenacet, s-metolachlor, molinate, pethoxamid, pretilachlor, prosulfocarb, pyroxasulfone, thenylchlor and thiobencarb, or a salt or ester thereof, provide synergistic weed control of undesirable vegetation in direct-seeded, water-seeded and transplanted rice, cereals, wheat, barley, oats, rye, sorghum, corn or maize, sugarcane, sunflower, oilseed rape, canola, sugar beet, soybean, cotton, pineapple, pastures, grasslands, rangelands, fallowland, turf, tree and vine orchards, aquatics, plantation crops, vegetables, industrial vegetation management (IVM) or rights-of-way (ROW).
专利号:US-2010190794-A1
优先权日:2007-06-12
标 题:Herbicidally Active Composition
发明人：HUPE EIKE; MOBERG WILLIAM KARL; REINHARD ROBERT; SIEVERNICH BERND; KIBLER ELMAR
权利人:BASF SE
摘要:The present invention relates to herbicidally active compositions comprising at least one piperazinedione compound of the formula I n n n n n n n n n n n n in which: n R x , R y are each hydrogen or together are a chemical bond; n R 1 is cyano or nitro; n R 2 is hydrogen, fluorine, chlorine, C 1 -C 2 -alkyl, ethenyl or C 1 -C 2 -alkoxy; n R 3 is fluorine or hydrogen; n R 4 is methyl; n R 5 is hydrogen, methyl or ethyl; n R 6 is hydrogen, methyl or ethyl; and n R 7 is hydrogen or halogen; n and at least one further active compound selected from the group consisting of n b1) lipid biosynthesis inhibitors; n b2) acetolactate synthase inhibitors (ALS inhibitors); n b3) photosynthesis inhibitors; n b4) protoporphyrinogen-IX oxidase inhibitors, n b5) bleacher herbicides; n b6) enolpyruvyl shikimate 3-phosphate synthase inhibitors (EPSP inhibitors); n b7) glutamine synthetase inhibitors; n b8) 7,8-dihydropteroate synthase inhibitors (DHP inhibitors); n b9) mitose inhibitors; n b10) inhibitors of the synthesis of very long chain fatty acids (VLCFA inhibitors); n b11) cellulose biosynthesis inhibitors; n b12) decoupler herbicides; n b13) auxin herbicides; n b14) auxin transport inhibitors; n b15) other herbicides, and n C) safeners.
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供应商参考报价(招募中)
品牌试剂参考报价(招募中)
📌 第三方产品分析报告
合成参考文献
摘要:USEPA; Tolerance Reassessment Progess and Risk management Decision. (TRED) database on Primisulfuron-methyl (86209-51-0). Available from, as of March 31, 2003:
摘要:Franke C et al; Chemosphere 29: 1501-14 (1994)
摘要:Weber JB, Keller KE; in Mechanisms of Pesticide Movement into Ground Water, Chp 3: 43-62, Honeycutt RC, Schabacker DJ, eds. Ann Arbor, MI: Lewis Pub (1994)
📝 需求与反馈
尽可能描述清楚需求与问题信息
