CAS: 4549-31-9; 1,7-Dibromoheptane

相似化合物

3344-70-5 4101-68-2 4549-32-0

上下游产品

CAS号629-30-1 1,7-庚二醇 | CAS号123-99-9 壬二酸 | CAS号54509-73-8 ethene | CAS号74-95-3 二溴甲烷 | CAS号32038-97-4 1,7-dibenzoyl-1... | CAS号111-16-0 庚二酸 | CAS号2050-20-6 庚二酸二乙酯 | CAS号408339-08-2 bis-(7-bromo-he... | CAS号10035-10-6 氢溴酸 | CAS号111752-57-9 N-[7-(4-nitroph... | CAS号41059-02-3 9-溴壬酸 | CAS号4549-33-1 1,9-二溴壬烷 | CAS号21727-91-3 7-溴-1-庚醇乙酸酯 | CAS号52819-34-8 1,7-二乙酰氧基庚烷 | CAS号3937-56-2 1,9-壬二醇 | CAS号37688-96-3 1,14-二溴十四烷 | CAS号21964-48-7 1,12-Tridecadiene | CAS号592-76-7 1-庚烯 | CAS号29333-99-1 N,N,N',N'-tetra...

壬二酸置于溴,Mercury(II) Oxide体系中,用 Various Solvent(S) 作为反应溶剂,化学反应 3.0H,以78 G的收率获得产物1,7-二溴庚烷
参考文献:常春藤和相关植物的毒理学原理:漆酚,1,2-二羟基-3-[(z)-十五烷基-8-烯基]苯和1,2-二羟基-3-十五烷基苯的合成
标题:常春藤和相关植物的毒理学原理:漆酚,1,2-二羟基-3-[(z)-十五烷基-8-烯基]苯和1,2-二羟基-3-十五烷基苯的合成
摘要:1,2-二羟基-3-新合成-[(ż)-十五碳-8-烯基]苯(1)和1,2-二羟基-3-Pentadecylbenzene(4),毒葛(的发泡剂原则漆树radicans)和从1,2-二甲氧基苯(7)开始描述了其他种类的漆树科.已经重新检查了1,2-二甲氧基苯(7)的锂化并重新确定了产物2,3-二甲氧基苯基锂(8)的产率.使用三丁基氯化锡作为淬灭剂,已经通过气相色谱法研究了这种芳基锂与1,7-二溴庚烷的反应.anacardiaceae科的两株植物semecarpus Vitiensis Engl的提取物.和melanorrhoea Beccariengl.,已检查了漆酚的存在.已发现后者的树皮含有没食子酸.
DOI:10.1039/p19800002331

专利信息

专利号:US-7557099-B2
优先权日:2004-03-01
标题 :Pyrrolobenzodiazepines as key intermediates in the synthesis of dimeric cytotoxic pyrrolobenzodiazepines
发明人：HOWARD PHILIP WILSON; KANG GYOUNG-DONG
权利人:SPIROGEN LTD
摘要:Compounds and a method of synthesis of compounds of formula (Ia) or (Ib): and salts, solvates, and chemically protected forms thereof, wherein the dotted lines indicate the optional presence of a double bond between C1 and C2 or C2 and C3; R 2 and R 3 are independently selected from —H, â•?O, â•?CH 2 , —CN, —R, OR, halo, â•?CH—R, O—SO 2 —R, CO 2 R and COR; R 10 is a carbamate-based nitrogen protecting group; and R 11 is an oxygen protecting group.

专利号:US-4490342-A
优先权日:1983-04-29
标 题 :Synthesis of ZSM-23 zeolite
发明人：VALYOCSIK ERNEST W
权利人:MOBIL OIL CORP
摘要:An improved method of synthesizing ZSM-23 zeolitic material is disclosed and claimed. The method comprises preparing a reaction mixture which comprises sources of an alkali metal, an oxide of aluminum (Al 2 O 3 ), an oxide of silicon (SiO 2 ), water and a nitrogen-containing organic cation R + , and having the following composition, in terms of mole ratios: n n ______________________________________ n n n Broad Preferred n______________________________________ nSiO 2 /Al 2 O 3 n 40 to 5000 50 to 2000 nH 2 O/SiO 2 n 5 to 200 20 to 100 nOH - /SiO 2 n 0 to 0.60 0.10 to 0.40 nM + SiO 2 n 0.01 to 2.0 0.10 to 1.0 nR + /SiO 2 n 0.01 to 2.0 0.05 to 1.0 n______________________________________ n n wherein M + is a cation of an alkali or alkaline earth metal and R + is an organic cation of the formula (CH 3 ) 3 N + --R 1 --N + (CH 3 ) 3 wherein R 1 is a saturated or unsaturated straight chain hydrocarbon group having seven carbon atoms, and maintaining the mixture at crystallization conditions until crystals of the ZSM-23 zeolite are formed. Thereafter, the crystals are separated from the liquid and recovered.

专利号:US-4619820-A
优先权日:1984-10-17
标题:Synthesis of ZSM-23 zeolite and the product produced
发明人：VALYOCSIK ERNEST W
权利人:MOBIL OIL CORP
摘要:An improved method of synthesizing highly siliceous ZSM-23 zeolitic material is disclosed and claimed. The method comprises preparing a reaction mixture which comprises sources of an alkali metal, an oxide of aluminum (Al 2 O 3 ), an oxide of silicon (SiO 2 ), water and a nitrogen-containing organic cation R + , and having the following composition, in terms of mole ratios: n n ______________________________________ n n n Broad Preferred n______________________________________ nSiO 2 /Al 2 O 3 n 5,000 to ∞ n 10,000 to ∞ nH 2 O/SiO 2 n 5 to 200 20 to 100 nOH - /SiO 2 n 0 to 0.60 0.10 to 0.40 nM + /SiO 2 n 0.01 to 2.0 0.10 to 1.0 nR + /SiO 2 n 0.01 to 2.0 0.05 to 1.0 n______________________________________ n n wherein M + is a cation of an alkali or alkaline earth metal and R + is an organic cation of the formula (CH 3 ) 3 N + --R 1 --N + (CH 3 ) 3 wherein R 1 is a saturated or unsaturated straight chain hydrocarbon group having seven carbon atoms, and maintaining the mixture at crystallization conditions until crystals of the ZSM-23 zeolite are formed. Thereafter, the crystals are separated from the liquid and recovered.

专利号:US-5559228-A
优先权日:1995-03-30
标题 :Synthesis of bisindolylmaleimides
发明人：GILLIG JAMES R; JIROUSEK MICHAEL R
权利人:LILLY CO ELI
摘要:The present invention provides an efficient process of reacting a bis-indolyl acid of the Formula (II): (II) wherein R1 is a hydrogen or C1-C4 alkyl and R, X, and Y are optional substitutions; to produce a bis-indolyloxallic acid of the Formula (III): (III) Compounds of the Formula (III) are readily converted to the bis-indolylmaleimides.

专利号:US-4531012-A
优先权日:1983-04-29
标题:Organic template for synthesis of ZSM-23 zeolite
发明人：VALYOCSIK ERNEST W
权利人:MOBIL OIL CORP
摘要:There is disclosed an organic cation R + , designated Diquat-7, having the formula: n n (CH.sub.3).sub.3 --N.sup.+ --R.sub.1 --N.sup.+ --(CH.sub.3).sub.3 n n wherein R 1 is a saturated or unsaturated straight chain hydrocarbon group containing seven carbon atoms. There is also disclosed a method of preparing Diquat-7, and salts and hydroxide thereof.

专利号:US-2009111737-A1
优先权日:1999-05-24
标题:Novel antibacterial agents
发明人：CHRISTENSEN BURTON G; MORAN EDMUND J; GRIFFIN JOHN H; JUDICE J KEVIN; MU YONGQI; PACE JOHN L; MAMMEN MATHAI; AGGEN JAMES
权利人:CHRISTENSEN BURTON G; MORAN EDMUND J; GRIFFIN JOHN H; JUDICE J KEVIN; MU YONGQI; PACE JOHN L; MAMMEN MATHAI; AGGEN JAMES
摘要:This invention relates to novel multibinding compounds (agents) that are antibacterial agents. The multibinding compounds of the invention comprise from 2-10 ligands covalently connected by a linker or linkers, wherein each of said ligands in their monovalent (i.e., unlinked) state have the ability to bind to a an enzyme involved in cell wall biosynthesis and metabolism, a precursor used in the synthesis of the bacterial cell wall and/or the bacterial cell surface thereby interfere with the synthesis and/or metabolism of the cell wall. In particular the multibinding compounds of the invention comprise from 2-10 ligands covalently connected by a linker or linkers, wherein each of said ligands hasn a ligand domain capable of binding to penicillin binding proteins, a transpeptidase enzyme, a substrate of a transpeptidase enzyme, a beta-lactamase enzyme, pencillinase enzyme, cephalosporinase enzyme, a transglycoslase enzyme, or a transglycosylase enzyme substrate; Preferably, the ligands are selected from the beta lactam or glycopeptide class of antibacterial agents.