专利号:US-5817751-A 优先权日:1994-06-23 标 题 :Method for synthesis of diketopiperazine and diketomorpholine derivatives 发明人:SZARDENINGS ANNA KATRIN; CAMPBELL DAVID 权利人:AFFYMAX TECH NV 摘要:The present invention relates to the areas of organic and medicinal chemistry. More specifically, the present invention is concerned with combinatorial and solid phase methods for the synthesis of diverse diketopiperazine derivatives, and the use of such methods to create libraries of diverse diketopiperazine derivatives. The present invention has application in the areas of chemical synthesis, the screening for new diketopiperazine derivatives having beneficial medical properties and the use of such screening to provide compositions and methods including diketopiperazine derivatives for treating disease.
专利号:US-2024039038-A1 优先权日:2022-08-01 标 题:Solvent-reagent based synthesis of solid-state electrolytes 发明人:AYKOL MURATAHAN; CHINNAM PARAMESWARA RAO 权利人:RIVIAN IP HOLDINGS LLC 摘要:The present disclosure is directed to processes for the preparation of argyrodite type materials, use of such argyrodite type materials in synthesis of solid-state electrolytes, and inclusion in secondary rechargeable batteries such as lithium ion batteries (LIBs), solid state batteries (SSBs), and/or lithium metal batteries (LMBs). For example, in an aspect the present disclosure provides a process that includes contacting a lithium source with a phosphorus source in a solvent-reagent at a temperature from about 80° C. to about 120° C. to form a precipitate comprising the Li7-xPS6-xYx (where Y is Cl, Br, or I, and 0 专利号:US-2012184653-A1 优先权日:2011-01-18 标 题:Synthesis of linear phosphorus-containing functional fluorocopolymer 发明人:WANG LIANG; WANG VIKTORIA 权利人:WANG LIANG; WANG VIKTORIA 摘要:This invention relates to a synthesis of a linear fluorocopolymer having a plurality of pendant phosphorus-containing functional groups. The synthesized phosphorus-containing fluorocopolymer has chain linearity and narrow molecular weight distributions. It has applications as a lubricant additive that provides friction-reduction, anti-wear, and corrosion protection properties.
专利号:WO-2025132036-A1 优先权日:2023-12-21 标题 :Method for solution synthesis of sodium or lithium thiophosphate particles 发明人:POIRIER ROMAIN; GARNERO CYRIL; PASQUIER DAVID; LAMBERT ARNOLD; UZIO DENIS 权利人:IFP ENERGIES NOW 摘要:The present invention relates to a method for synthesis of thiophosphate particles Li3PS4 or Na3PS4 from a reagent A2S and a phosphorus reagent P2S5, where A is selected from Li or Na, the method comprising at least the following steps, carried out under an inert atmosphere: A) bringing the reagent A2S, previously suspended in at least one first polar solvent (solvent 1), into contact with a suspension containing at least the phosphorus reagent P2S5 in at least one second polar solvent and forming, in suspension under reflux, an intermediate compound in the form of a solvate-complex A3PS4-solvent; B) centrifuging, redispersing in a solvent, then filtering and washing the intermediate compound; C) drying the intermediate compound; d) optional heat treatment.
专利号:US-7619116-B2 优先权日:2003-12-17 标 题:Intermediates for the synthesis of (R)-tamsulosin and of its pharmaceutically acceptable salts and process for their preparation 发明人:DAMBRIN VALERY; LENOIR JEAN-YVES; SCHNEIDER JEAN-MARIE; GUILLAMOT GERARD; FOLLET MICHEL; BECKER ABRAM 权利人:PRODUCTS CHIMIQUES AUXILIAIRES 摘要:A subject matter of the present invention is novel intermediates for the synthesis of (R)-tamsulosin and of its pharmaceutically acceptable salts, and also the associated preparation process.
专利号:US-2022227624-A1 优先权日:2019-04-17 标 题:Method for Wet Chemical Synthesis of Lithium Argyrodites 发明人:WANG HUI; DRUFFEL THAD; BUCHBERGER DOMINIKA AGNIESZKA 权利人:BUCHBERGER DOMINIKA AGNIESZKA; UNIV LOUISVILLE RES FOUND INC; UNIV WARSZAWSKI; Uniwersy tet Warszawski 摘要:Methods for wet chemical synthesis of lithium argyrodites are provided, which in some embodiments include includes dissolving a stoichiometric mixture of precursors in a small quantity of solvent in an argon atmosphere, drying the mixture under vacuum or an inert gas atmosphere to evaporate the solvent, and then annealing to obtain a final lithium argyrodite product. Further embodiments comprise synthesizing the precursors, and excess halide doping to achieve higher ionic conductivity.
摘要:Baker, A.; Wirth, T., Science of Synthesis Knowledge Updates, (2017) 1, 198. 摘要:Stanforth, S. P., Science of Synthesis Knowledge Updates, (2014) 3, 137. 摘要:Koutentis, P. A.; Ioannidou, H. A., Science of Synthesis Knowledge Updates, (2010) 1, 272. 摘要:Silva, V. L. M.; Pinto, D. C. G. A.; Santos, C. M. M.; Rocha, D. H. A., Science of Synthesis Knowledge Updates, (2022) 3, 377. 摘要:Wang, M.; Jiang, X., Science of Synthesis Knowledge Updates, (2021) 2, 224.