专利号:US-7247287-B2 优先权日:2003-06-11 标 题 :Synthesis of aluminophosphates and silicoaluminophosphates 发明人:CAO GUANG; SHAH MATU J 权利人:EXXONMOBIL CHEM PATENTS INC 摘要:The invention is directed to a method of synthesising silicoaluminophosphate and aluminophosphate molecular sieves using synthesis templates that contain at least one template of general formula R 1 R 2 N—R 3 , wherein R 1 and R 2 are independently selected from the group consisting of alkyl groups having from 1 to 3 carbon atoms and hydroxyalkyl groups having from 1 to 3 carbon atoms; R 3 is selected from the group consisting of 4- to 8-membered cycloalkyl groups, optionally substituted by 1 to 3 alkyl groups having from 1 to 3 carbon atoms, and 4- to 8-membered heterocyclic groups having from 1 to 3 heteroatoms, said heterocyclic groups being optionally substituted by 1 to 3 alkyl groups having from 1 to 3 carbon atoms and the heteroatoms in said heterocyclic groups being selected from the group consisting of O, N, and S. In particular, the present invention relates to the synthesis of silicoaluminophosphate molecular sieves of the CHA framework type having a low silicon to aluminium atomic ratio.
专利号:US-2014255328-A1 优先权日:2013-03-11 标 题:Hydrothermal Synthesis of Zinc Phlogopite 发明人:MCGUIRE MEAGHAN CLARK; BULL IVOR; JOHNSON GEOFFREY MARK 权利人:BASF SE 摘要:This invention relates to a synthetically derived zinc phlogopite platelets, of superior platelet diameter, effect pigments comprising such synthetically derived platelets and methods of forming said substrates. More specifically the disclosure describes an improved hydrothermal synthesis of zinc phlogopite suitable as a platelets for interference pigments, barrier and flame retardant applications.
专利号:US-8287715-B2 优先权日:2009-05-19 标题:Synthesis of boron using molten salt electrolysis 发明人:TAYLOR PATRICK R; GOMEZ JUDITH C 权利人:TAYLOR PATRICK R; GOMEZ JUDITH C; COLORADO SCHOOL OF MINES 摘要:The invention relates generally to elemental boron, particularly to elemental boron having a high purity level and to a method of recovering elemental boron by the electrolysis of a molten boron-containing electrolyte.
专利号:US-5228910-A 优先权日:1991-09-06 标题 :Mixed metal oxide crystalline powders and method for the synthesis thereof 发明人:JOYCE IVAN H; BLONSKI ROBERT P; MALONEY JOHN J; WELCH JOHN J; PIPOLY RICHARD A; BYRNE CHRISTINE J 权利人:FERRO CORP 摘要:A method for the synthesis of mixed metal oxide crystalline powders comprises the steps of preparing a raw material mixture containing at least two different metal cations; adding a template material to the mixture and blending it therewith; initiating formation of a mixed metal oxide by calcination of the mixture and the template material, whereby particles of the mixed metal oxides are formed; and thereafter recovering the mixed metal oxide particles. Mixed metal oxide crystalline powders comprise a template material; and metal oxides which form pigment classes of material containing the template material, the pigment classes being selected from the group consisting of borate, garnet, olivine, phenacite, phosphate, priderite, pyrochlore, sphene, spinel and zircon, as well as perovskite crystal classes of material containing the template, all of which have a uniform particle morphology and particle size ranging between about 0.2 to 100 mu with minimal comminution.
专利号:US-2006249072-A1 优先权日:2005-05-05 标 题 :Method of synthesizing a fluoride growth material for improved outgassing 发明人:CSILLAG FRANK J; JONES CHRISTOPHER D 权利人:CSILLAG FRANK J; JONES CHRISTOPHER D 摘要:Improved contaminant removal from alkaline- or alkali-earth metal fluoride crystal growth material can be obtained by coprecipitating an alkaline- or alkali-earth metal fluoride with a scavenging agent during synthesis of the fluoride growth material. The coprecipitation of the alkaline- or alkali-earth metal fluoride and scavenging agent can be performed using at least one of chloride, nitrate, hydroxide and carbonate salts of the alkaline- or alkali-earth metal fluoride and scavenging agent. This provides a more intimate mixture or dispersion of the scavenging agent in solid solution or as a mechanical mixture with the alkaline- or alkali-earth metal fluoride for improved outgassing and fewer trapped impurities, leading to improved radiation hardness and bulk absorption.
专利号:US-5648522-A 优先权日:1995-02-14 标题:Process for the synthesis of fluorinated sulphonic acids 发明人:HOMMELTOFT SVEN IVAR; EKELUND OLE; ZAVILLA JOHN 权利人:HALDOR TOPSOE AS 摘要:Process for the preparation of a fluorinated sulphonic acid compound by hydrolysis of a corresponding fluorinated sulphonyl fluoride, wherein the hydrolysis is carried out in the presence of a tertiary amine, comprising steps of recovering a mixture of a salt of hydrolysed fluorinated sulphonyl fluoride with the tertiary amine and an ammonium fluoride salt of the tertiary amine; n reacting the salt mixture with a sulphonyl compound of the general formula R--SO 2 X, wherein n n R=an alkyl group, Cl, F; n n and n n X=Br, Cl n n thereby exchanging fluoride of the ammonium fluoride salt in the mixture with the X atom of the sulphonyl compound and converting the sulphonyl compound to a sulphonyl fluoride; and n distilling off the sulphonyl fluoride from the reacted salt mixture.
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