溴代十二烷 在 Sodium Sulfite体系中,用 乙醇,水作为反应溶剂,以92%的收率获得sodium Dodecyl Sulfate 参考文献:[En] Hormone Receptor Modulators For Treating Metabolic Conditions And Disorders[Fr] Modulateurs Du Récepteur Hormonal Pour Le Traitement D'états Et De Troubles Métaboliques 标题:[En] Hormone Receptor Modulators For Treating Metabolic Conditions And Disorders[Fr] Modulateurs Du Récepteur Hormonal Pour Le Traitement D'états Et De Troubles Métaboliques 摘要:这项发明涉及fxr的激活剂,可用于治疗自身免疫性疾病,肝病,肠道疾病,肾脏疾病,癌症以及fxr在其中发挥作用的其他疾病,其化学式为(I):(I),其中l1,A,X1,X2,R1,R2和r3如本文所述.
专利号:US-2012190064-A1 优先权日:2004-10-01 标题 :Feeding buffers, systems, and methods for in vitro synthesis of biomolecules 发明人:KUDLICKI WIESLAW ANTONI; KEPPETIPOLA SHIRANTHI; FLETCHER JULIA; GETBEHEAD ASHLEY ELAINE; KATZEN FEDERICO; VOZZA-BROWN LAURA 权利人:KUDLICKI WIESLAW ANTONI; KEPPETIPOLA SHIRANTHI; FLETCHER JULIA; GETBEHEAD ASHLEY ELAINE; KATZEN FEDERICO; VOZZA-BROWN LAURA; LIFE TECHNOLOGIES CORP 摘要:Compositions, methods and kits for in vitro systems for synthesis of biomolecules such as polypeptides, are provided herein. Cell extracts that provide enhanced yields of soluble proteins using in vitro protein synthesis methods are provided. The invention also includes methods for producing high yields of proteins by the addition of a feeding solution that includes amino acids and an energy source to an ongoing in vitro synthesis system. The invention also includes methods of using a high-yield in vitro synthesis system to produce large quantities of proteins with incorporated labeled amino acids for analysis by methods such as by NMR. The invention further includes vectors for enhanced production of proteins from nucleic acid templates using in vitro synthesis systems.
专利号:WO-2019158576-A1 优先权日:2018-02-16 标题 :Direct synthesis of alkane sulfonic acids from alkane and sulfur trioxide employing heterogeneous catalysis 发明人:OTT TIMO 权利人:GRILLO WERKE AG 摘要:The present invention relates to a process for the direct synthesis of alkanesulfonic acids, particularly methanesulfonic acid, from sulfur trioxide and alkanes employing heterogeneous catalysts, particularly transition metals such as rhodium. Particularly the synthesis is carried out in a tube furnace and the resultant product is isolated by quenching the resultant gas mixture in aqueous concentrated sulfuric acid at room temperature.
专利号:US-11643336-B2 优先权日:2019-10-24 标 题 :Precursor materials for Li-ion battery cathode synthesis 发明人:PULLEN ADRIAN W; SRIRAMULU SURESH 权利人:CAMX POWER LLC 摘要:Provided are processes for the production of particles for use as a precursor material for synthesis of Li-ion cathode active material of a lithium-ion cell comprising: a non-lithiated nickel oxide particle of the formula MOx wherein M comprises 80 at % Ni or greater and wherein x is 0.7 to 1.2, M optionally excluding boron in the MOx crystal structure; and a modifier oxide intermixed with, coated on, present within, or combinations thereof the non-lithiated nickel oxide particle, wherein the modifier oxide is associated with the non-lithiated nickel oxide such that a calcination at 500 degrees Celsius for 2 hours results in crystallite growth measured by XRD of 2 nanometers or less.
专利号:WO-2020064466-A1 优先权日:2018-09-25 标 题:Catalyst for the synthesis of alkanesulfonic acids 发明人:OTT TIMO; BIERTUEMPEL INGO 权利人:BASF SE 摘要:The present invention relates to novel uses of organic peroxoacids comprising functional groups as catalysts in the preparation of alkane sulfonic acids from alkanes and sulfur trioxide, methods for the production of alkane sulfonic acids employing said catalysts as well as reaction mixtures comprising said catalysts. The invention particularly relates to the production of methane sulfonic acid from methane and sulfur trioxide employing organic peroxoacids comprising functional groups as catalysts.
专利号:WO-2020064573-A1 优先权日:2018-09-25 标 题:Catalysts for the synthesis of alkanesulfonic acids 发明人:OTT TIMO; BIERTUEMPEL INGO 权利人:BASF SE 摘要:The present invention relates to novel uses of compounds comprising heterolytically cleavable bonds as catalysts in the preparation of alkanesulfonic acids from alkanes and sulfur trioxide, methods for the production of alkanesulfonic acids employing said catalysts as well as reaction mixtures comprising said catalysts. The invention particularly relates to the production of methanesulfonic acid from methane and sulfur trioxide employing compounds comprising heterolytically cleavable bonds as catalysts.
专利号:US-4097522-A 优先权日:1975-06-05 标 题:Synthesis of m-benzoyl-hydratropic acid 发明人:BAIOCCHI LEANDRO 权利人:ACRAF 摘要:A process is provided for the production of m-benzoyl-hydratropic acid which comprises heating the reaction mixture obtained from the condensation of 2-benzoyl-cyclohexanone and pyruvic acid, its esters or salts, at a temperature of 200° to 230° and in the presence of an acid catalyst.
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合成参考文献
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