CAS: 832-53-1; Pentafluorobenzenesulfonyl Chloride

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CAS号363-72-4 五氟苯 | CAS号879-06-1 3-indole acetamide | CAS号27918-31-6 五氟苯磺酰氯 | CAS号7722-84-1 过氧化氢 | CAS号344-07-0 氯五氟苯 | CAS号771-62-0 五氟硫酚 | CAS号7782-50-5 氯气 | CAS号64-19-7 冰醋酸 | CAS号195533-53-0 Batabulin | CAS号434-90-2 全氟联苯 | CAS号793-73-7 pentafluorophen... | CAS号142-04-1 苯胺盐酸盐 | CAS号344-07-0 氯五氟苯 | CAS号363-72-4 五氟苯 | CAS号711-55-7 1,2,3,4-tetrafl... | CAS号108-20-3 异丙醚 | CAS号784-14-5 2,3,4,5,6-五氟联苯 | CAS号4400-84-4 2,3,4,5,6-penta...

氯五氟苯置于氯磺酸体系中,用 Neat (No Solvent) 作为反应溶剂,化学反应生成 2,3,4,5,6-五氟苯磺酰氯
参考文献:Development Of Hdac Inhibitors Exhibiting Therapeutic Potential In T-Cell Prolymphocytic Leukemia
标题:Development Of Hdac Inhibitors Exhibiting Therapeutic Potential In T-Cell Prolymphocytic Leukemia
摘要:
DOI:10.1021/acs.Jmedchem.1C00420

专利信息

专利号:EP-0364340-B1
优先权日:1988-10-05
标题:Method for the synthesis of sulfonyl imides
摘要:Method for the synthesis of sulfonylimidides having the formula M((RSO2)2N)y, whrein M is a metal or an ammonium radical quaternary or not, the Rs, which may be identical or similar are organic monovalent radicals, particularly hydrocarbyles and preferably perfluorohydrocarbyles, in C1 to C12, and y is the valence of M. On the one hand, a silazane component selected amongst the silazane compounds M(((R2)3Si)2N)y or the associations of a silazane derivative A((R2)3Si)2N or a fluoride M1Fz of low cross-linking energy is reacted with, on the other hand, at least one sulfonic halogenite component consisting of a sulfonyl fluoride RSO2F or in the association of a sulfonyl chloride RSO2Cl with a fluoride M1Fz, M, R and y having the above-mentionned significations, M1 being selected amongst the Ms and being optionally identical to M, z being the valence of M1 and R2 representing an alkyl in C1 to C4. The imidides obtained for which the R2 are perfluorated radicals and M is an alkaline metal such as Li are usable in association with polyethers for the production of materials of the ionic conduction type for all solid generators in thin films.

专利号:US-5256821-A
优先权日:1988-10-05
标题:Method of synthesis of sulphonylimides
发明人：ARMAND MICHEL B
权利人:ELF AQUITAINE; HYDRO QUEBEC
摘要:Method for the synthesis of sulfonylimidides having the formula M((RSO 2 ) 2 N) y , wherein M is a metal or an ammonium radical quaternary or not, the Rs, which may be identical or similar are organic monovalent radicals, particularly hydrocarbyles and preferably perfluorohydrocarbyles, in C 1 to C 12 , and y is the valence of M. On the one hand, silazane component selected amongst the silazane compounds M(((R 2 ) 3 Si) 2 N) y or the associations of a silazane derivative A((R 2 ) 3 Si) 2 N or a fluoride M 1 F z of low cross-linking energy is reacted with, on the other hand, at least one sulfonic halogenite component consisting of a sulfonyl fluoride RSO 2 F or in the association of a sulfonyl chloride RSO 2 Cl with a fluoride M 1 F z , M, R and y having the above-mentioned significations, M being selected amongst the Ms and being optionally identical to M, z being the valence of M 1 and R 2 representing an alkyl in C 1 to C 4 . The imidides obtained for which the R 2 are perfluorated radicals and M is an alkaline metal such as Li are usable in association with polyethers for the production of materials of the ionic conduction type for all solid generators in thin films.

专利号:US-2010150835-A1
优先权日:2007-02-27
标题:Synthesis of [18F] Fluoromethyl Benzene Using Benzyl Pentafluorobenzenesulfonate
发明人：LANGSTROM BENGT; KARIMI FARHAD; BLOM ELISABETH
权利人:LANGSTROM BENGT; KARIMI FARHAD; BLOM ELISABETH
摘要:The present invention discloses the reactivity of ponytail (“PTâ€?) sulfonates as leaving groups in nucleophilic fluorination reactions. The results showed that using a pentafluorobenzenesulfonate precursor is a suitable leaving group for n. c. a. nucleophilic 18 F-fluorination in synthesis of [ 18 F]fluoromethyl benzene, wherein this is a suitable leaving group for 18F-labeling with moderate reactivity. The PT-precursor seems to be quite stable. In an attempt to purify the crude 18F-labeled product using fluorous solid phase extraction (F-SPE), the radio labeled impurities decreased significantly. This provides an opportunity for utilizing PT methodology in both simple and fast purification methods.

专利号:US-5214218-A
优先权日:1992-05-04
标题 :One step synthesis of methyl t-butyl ether from t-butanol using haloacid-modified clay catalysts
发明人：KNIFTON JOHN F
权利人:TEXACO CHEMICAL
摘要:A method is disclosed wherein t-butanol is reacted with methanol in a reaction zone in one step to provide methyl tert-butyl ether and the improvement of accomplishing the reaction which comprises: n a. Using a catalyst comprising a montmorillonite clay treated with a haloacid; n b. continuously contacting said t-butanol and methanol in a molar amount of about 0.1 to 10 moles of methanol per mole of t-butanol with said catalyst at a temperature of about 20° C. to about 250° C. and a pressure of about atmospheric to about 1000 psig to obtain the methyl tert-butyl ether product.

专利号:EP-2883866-A1
优先权日:2012-08-13
标题 :INTERMEDIATE FOR SYNTHESIS OF 1-(2-DEOXY-2-FLUORO-4-THIO-beta-D-ARABINOFURANOSYL) CYTOSINE, INTERMEDIATE FOR SYNTHESIS OF THIONUCLEOSIDE, AND METHODS FOR PRODUCING THESE INTERMEDIATES

专利号:WO-2014027658-A1
优先权日:2012-08-13
标题 :INTERMEDIATE FOR SYNTHESIS OF 1-(2-DEOXY-2-FLUORO-4-THIO-β-D-ARABINOFURANOSYL) CYTOSINE, INTERMEDIATE FOR SYNTHESIS OF THIONUCLEOSIDE, AND METHODS FOR PRODUCING THESE INTERMEDIATES